Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites

The use of thermoplastic composites based on poly(lactic) acid and phosphate glass fibres over metallic alloys for clinical restorative treatment is highly beneficial due to their biocompatibility and biodegradability. However, difficulties in achieving a thorough melt impregnation at high fibre con...

Full description

Bibliographic Details
Main Authors: Barrera Betanzos, Fernando, Gimeno-Fabra, Miquel, Segal, Joel, Grant, David, Ahmed, Ifty
Format: Article
Published: Elsevier 2016
Subjects:
Online Access:https://eprints.nottingham.ac.uk/32820/
_version_ 1848794497094254592
author Barrera Betanzos, Fernando
Gimeno-Fabra, Miquel
Segal, Joel
Grant, David
Ahmed, Ifty
author_facet Barrera Betanzos, Fernando
Gimeno-Fabra, Miquel
Segal, Joel
Grant, David
Ahmed, Ifty
author_sort Barrera Betanzos, Fernando
building Nottingham Research Data Repository
collection Online Access
description The use of thermoplastic composites based on poly(lactic) acid and phosphate glass fibres over metallic alloys for clinical restorative treatment is highly beneficial due to their biocompatibility and biodegradability. However, difficulties in achieving a thorough melt impregnation at high fibre contents while limiting polymer degradation is one of the main issues encountered during their manufacture. This paper reports for the first time on the effects of pressure cycling on the mechanical properties of compression moulded polylactic acid-phosphate glass fibre composites. The strength of the composites consolidated under pressure cycling were at least 30% higher than those in which conventional static pressure was used. The marked disparity was attributed to the influence of pressure cycling on the fibre preform permeability, the melt viscosity and the capillary pressure, leading to improved fibre wet-out with respect to static pressure. Implementation of a cyclic pressure appeared to promote the occurrence of transcrystallinity in the polymer matrix as suggested by DSC traces. The fibre content influenced PLA thermal degradation since the matrix molecular weight decreased as the fibre content increased on account of the moisture adsorbed by the glass surface. However, this extent of degradation did not impair the matrix mechanical performance in the composites.
first_indexed 2025-11-14T19:17:08Z
format Article
id nottingham-32820
institution University of Nottingham Malaysia Campus
institution_category Local University
last_indexed 2025-11-14T19:17:08Z
publishDate 2016
publisher Elsevier
recordtype eprints
repository_type Digital Repository
spelling nottingham-328202020-05-04T17:56:27Z https://eprints.nottingham.ac.uk/32820/ Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites Barrera Betanzos, Fernando Gimeno-Fabra, Miquel Segal, Joel Grant, David Ahmed, Ifty The use of thermoplastic composites based on poly(lactic) acid and phosphate glass fibres over metallic alloys for clinical restorative treatment is highly beneficial due to their biocompatibility and biodegradability. However, difficulties in achieving a thorough melt impregnation at high fibre contents while limiting polymer degradation is one of the main issues encountered during their manufacture. This paper reports for the first time on the effects of pressure cycling on the mechanical properties of compression moulded polylactic acid-phosphate glass fibre composites. The strength of the composites consolidated under pressure cycling were at least 30% higher than those in which conventional static pressure was used. The marked disparity was attributed to the influence of pressure cycling on the fibre preform permeability, the melt viscosity and the capillary pressure, leading to improved fibre wet-out with respect to static pressure. Implementation of a cyclic pressure appeared to promote the occurrence of transcrystallinity in the polymer matrix as suggested by DSC traces. The fibre content influenced PLA thermal degradation since the matrix molecular weight decreased as the fibre content increased on account of the moisture adsorbed by the glass surface. However, this extent of degradation did not impair the matrix mechanical performance in the composites. Elsevier 2016-06-15 Article PeerReviewed Barrera Betanzos, Fernando, Gimeno-Fabra, Miquel, Segal, Joel, Grant, David and Ahmed, Ifty (2016) Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites. Materials & Design, 100 . pp. 141-150. ISSN 0261-3069 Bioresorbable composites; Phosphate glass fibre; Polylactic acid; Cyclic pressure http://www.sciencedirect.com/science/article/pii/S0264127516303914 doi:10.1016/j.matdes.2016.03.108 doi:10.1016/j.matdes.2016.03.108
spellingShingle Bioresorbable composites; Phosphate glass fibre; Polylactic acid; Cyclic pressure
Barrera Betanzos, Fernando
Gimeno-Fabra, Miquel
Segal, Joel
Grant, David
Ahmed, Ifty
Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites
title Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites
title_full Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites
title_fullStr Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites
title_full_unstemmed Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites
title_short Cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites
title_sort cyclic pressure on compression-moulded bioresorbable phosphate glass fibre reinforced composites
topic Bioresorbable composites; Phosphate glass fibre; Polylactic acid; Cyclic pressure
url https://eprints.nottingham.ac.uk/32820/
https://eprints.nottingham.ac.uk/32820/
https://eprints.nottingham.ac.uk/32820/