Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography

We used X-ray computed tomography (CT), microscopy and hardness measurements to study Al–Si10–Mg produced by selective laser melting (SLM). Specimens were subject to a series of heat treatments including annealing and precipitation hardening. The specimen interiors were imaged with X-ray CT, allowin...

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Main Authors: Maskery, Ian, Aboulkhair, N.T., Corfield, M.R., Tuck, Christopher, Clare, A.T., Leach, Richard K., Wildman, Ricky D., Ashcroft, Ian, Hague, Richard J.M.
Format: Article
Published: Elsevier 2016
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Online Access:https://eprints.nottingham.ac.uk/31972/
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author Maskery, Ian
Aboulkhair, N.T.
Corfield, M.R.
Tuck, Christopher
Clare, A.T.
Leach, Richard K.
Wildman, Ricky D.
Ashcroft, Ian
Hague, Richard J.M.
author_facet Maskery, Ian
Aboulkhair, N.T.
Corfield, M.R.
Tuck, Christopher
Clare, A.T.
Leach, Richard K.
Wildman, Ricky D.
Ashcroft, Ian
Hague, Richard J.M.
author_sort Maskery, Ian
building Nottingham Research Data Repository
collection Online Access
description We used X-ray computed tomography (CT), microscopy and hardness measurements to study Al–Si10–Mg produced by selective laser melting (SLM). Specimens were subject to a series of heat treatments including annealing and precipitation hardening. The specimen interiors were imaged with X-ray CT, allowing the non-destructive quantification and characterisation of pores, including their spatial distribution. The specimens had porosities less than 0.1%, but included some pores with effective cross-sectional diameters up to 260 μm. The largest pores were highly anisotropic, being flat and lying in the plane normal to the build direction. Annealing cycles caused significant coarsening of the microstructure and a reduction of the hardness from (114 ± 3) HV, in the as-built state, to (45 ± 1) HV, while precipitation hardening increased this to a final hardness of (59 ± 1) HV. The pore size and shape distributions were unaffected by the heat treatments. We demonstrate the applicability of CT measurements and quantitative defect analysis for the purposes of SLM process monitoring and refinement.
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publishDate 2016
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spelling nottingham-319722020-05-04T20:04:41Z https://eprints.nottingham.ac.uk/31972/ Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography Maskery, Ian Aboulkhair, N.T. Corfield, M.R. Tuck, Christopher Clare, A.T. Leach, Richard K. Wildman, Ricky D. Ashcroft, Ian Hague, Richard J.M. We used X-ray computed tomography (CT), microscopy and hardness measurements to study Al–Si10–Mg produced by selective laser melting (SLM). Specimens were subject to a series of heat treatments including annealing and precipitation hardening. The specimen interiors were imaged with X-ray CT, allowing the non-destructive quantification and characterisation of pores, including their spatial distribution. The specimens had porosities less than 0.1%, but included some pores with effective cross-sectional diameters up to 260 μm. The largest pores were highly anisotropic, being flat and lying in the plane normal to the build direction. Annealing cycles caused significant coarsening of the microstructure and a reduction of the hardness from (114 ± 3) HV, in the as-built state, to (45 ± 1) HV, while precipitation hardening increased this to a final hardness of (59 ± 1) HV. The pore size and shape distributions were unaffected by the heat treatments. We demonstrate the applicability of CT measurements and quantitative defect analysis for the purposes of SLM process monitoring and refinement. Elsevier 2016-01 Article PeerReviewed Maskery, Ian, Aboulkhair, N.T., Corfield, M.R., Tuck, Christopher, Clare, A.T., Leach, Richard K., Wildman, Ricky D., Ashcroft, Ian and Hague, Richard J.M. (2016) Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography. Materials Characterization, 111 . pp. 193-204. ISSN 1873-4189 Selective laser melting; Aluminium alloy; Additive manufacture; X-ray computed tomography; Non-destructive testing http://www.sciencedirect.com/science/article/pii/S1044580315300711 doi:10.1016/j.matchar.2015.12.001 doi:10.1016/j.matchar.2015.12.001
spellingShingle Selective laser melting; Aluminium alloy; Additive manufacture; X-ray computed tomography; Non-destructive testing
Maskery, Ian
Aboulkhair, N.T.
Corfield, M.R.
Tuck, Christopher
Clare, A.T.
Leach, Richard K.
Wildman, Ricky D.
Ashcroft, Ian
Hague, Richard J.M.
Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography
title Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography
title_full Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography
title_fullStr Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography
title_full_unstemmed Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography
title_short Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using x-ray computed tomography
title_sort quantification and characterisation of porosity in selectively laser melted al–si10–mg using x-ray computed tomography
topic Selective laser melting; Aluminium alloy; Additive manufacture; X-ray computed tomography; Non-destructive testing
url https://eprints.nottingham.ac.uk/31972/
https://eprints.nottingham.ac.uk/31972/
https://eprints.nottingham.ac.uk/31972/