Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions

The separation of water-in-oil emulsions made with Azeri crude was investigated using natural gravity settling and microwave heating techniques. Separation times could be reduced by an order of magnitude compared with untreated emulsions. Increasing the salinity of the water phase leads to a 15% ave...

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Main Authors: Binner, Eleanor, Robinson, John P., Silvester, S.A., Kingman, S.W., Lester, Edward
Format: Article
Published: Elsevier 2014
Subjects:
Online Access:https://eprints.nottingham.ac.uk/31942/
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author Binner, Eleanor
Robinson, John P.
Silvester, S.A.
Kingman, S.W.
Lester, Edward
author_facet Binner, Eleanor
Robinson, John P.
Silvester, S.A.
Kingman, S.W.
Lester, Edward
author_sort Binner, Eleanor
building Nottingham Research Data Repository
collection Online Access
description The separation of water-in-oil emulsions made with Azeri crude was investigated using natural gravity settling and microwave heating techniques. Separation times could be reduced by an order of magnitude compared with untreated emulsions. Increasing the salinity of the water phase leads to a 15% average decrease in the settling time for untreated emulsions compared with over 90% for microwave-heated emulsions. An image analysis technique showed that the observed increases in settling time could not be attributed to changes in viscosity alone. Significant coalescence of water droplets occurs during microwave heating, however the effects of coalescence and viscosity reduction cannot be completely decoupled. Despite this, it is clear that it is the thermal effect of microwave heating that leads to improvements in settling times, and that any advantages in microwave heating over conventional heating can be explained by selective heating of the aqueous phase rather than so-called non-thermal effects.
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spelling nottingham-319422020-05-04T16:41:41Z https://eprints.nottingham.ac.uk/31942/ Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions Binner, Eleanor Robinson, John P. Silvester, S.A. Kingman, S.W. Lester, Edward The separation of water-in-oil emulsions made with Azeri crude was investigated using natural gravity settling and microwave heating techniques. Separation times could be reduced by an order of magnitude compared with untreated emulsions. Increasing the salinity of the water phase leads to a 15% average decrease in the settling time for untreated emulsions compared with over 90% for microwave-heated emulsions. An image analysis technique showed that the observed increases in settling time could not be attributed to changes in viscosity alone. Significant coalescence of water droplets occurs during microwave heating, however the effects of coalescence and viscosity reduction cannot be completely decoupled. Despite this, it is clear that it is the thermal effect of microwave heating that leads to improvements in settling times, and that any advantages in microwave heating over conventional heating can be explained by selective heating of the aqueous phase rather than so-called non-thermal effects. Elsevier 2014-01-15 Article PeerReviewed Binner, Eleanor, Robinson, John P., Silvester, S.A., Kingman, S.W. and Lester, Edward (2014) Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions. Fuel, 116 . pp. 516-521. ISSN 1873-7153 Water-in-oil emulsion Microwave Coalescence Viscosity Interfacial tension Selective heating http://www.sciencedirect.com/science/article/pii/S0016236113007709 doi:10.1016/j.fuel.2013.08.042 doi:10.1016/j.fuel.2013.08.042
spellingShingle Water-in-oil emulsion
Microwave
Coalescence
Viscosity
Interfacial tension
Selective heating
Binner, Eleanor
Robinson, John P.
Silvester, S.A.
Kingman, S.W.
Lester, Edward
Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions
title Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions
title_full Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions
title_fullStr Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions
title_full_unstemmed Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions
title_short Investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions
title_sort investigation into the mechanisms by which microwave heating enhances separation of water-in-oil emulsions
topic Water-in-oil emulsion
Microwave
Coalescence
Viscosity
Interfacial tension
Selective heating
url https://eprints.nottingham.ac.uk/31942/
https://eprints.nottingham.ac.uk/31942/
https://eprints.nottingham.ac.uk/31942/