Toward more realistic viscosity measurements of tyre rubber–bitumen blends

The measurement of rheological properties of the tyre rubber bitumen blends is often challenging due to presence of suspended tyre rubber’s crumbs. Furthermore, the phase separation during the course of measurements makes the viscosity of these non-homogeneous blends difficult to ascertain. In this...

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Main Authors: Lo Presti, Davide, Fecarotti, Claudia, Clare, Adam T., Airey, Gordon
Format: Article
Published: Elsevier 2014
Online Access:https://eprints.nottingham.ac.uk/3125/
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author Lo Presti, Davide
Fecarotti, Claudia
Clare, Adam T.
Airey, Gordon
author_facet Lo Presti, Davide
Fecarotti, Claudia
Clare, Adam T.
Airey, Gordon
author_sort Lo Presti, Davide
building Nottingham Research Data Repository
collection Online Access
description The measurement of rheological properties of the tyre rubber bitumen blends is often challenging due to presence of suspended tyre rubber’s crumbs. Furthermore, the phase separation during the course of measurements makes the viscosity of these non-homogeneous blends difficult to ascertain. In this study, a new dual helical impeller was designed and manufactured to be used with a rotational viscometer in order to have a real-time control of the viscosity while performing a laboratory mixing of the blends. Layer based manufacturing techniques showed to be a convenient method to produce complex shaped impeller prototypes before manufacturing the more expensive stainless steel assembly. Impeller geometry was optimised to create a convective like flow within the sample and so minimise phase separation. Shear rate constant is geometry dependent and a calibration exercise was carried out to ascertain this. Results of both calibration and validation phases showed that the new impeller provides reliable viscosity measurements of homogenous fluids such as neat bitumen. With regards to complex fluids the new impeller showed a more stable and realistic trend than that obtained by using a standard spindle. In fact, it was demonstrated that the new impeller significantly decreases phase separation within the blend and in turns provides a more realistic measurement of the viscosity. This system represents a feasible and improved solution for optimising the laboratory modification process of tyre rubber bitumen blends by adapting the rotational viscometer as a low-shear mixer.
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spelling nottingham-31252020-05-04T16:46:42Z https://eprints.nottingham.ac.uk/3125/ Toward more realistic viscosity measurements of tyre rubber–bitumen blends Lo Presti, Davide Fecarotti, Claudia Clare, Adam T. Airey, Gordon The measurement of rheological properties of the tyre rubber bitumen blends is often challenging due to presence of suspended tyre rubber’s crumbs. Furthermore, the phase separation during the course of measurements makes the viscosity of these non-homogeneous blends difficult to ascertain. In this study, a new dual helical impeller was designed and manufactured to be used with a rotational viscometer in order to have a real-time control of the viscosity while performing a laboratory mixing of the blends. Layer based manufacturing techniques showed to be a convenient method to produce complex shaped impeller prototypes before manufacturing the more expensive stainless steel assembly. Impeller geometry was optimised to create a convective like flow within the sample and so minimise phase separation. Shear rate constant is geometry dependent and a calibration exercise was carried out to ascertain this. Results of both calibration and validation phases showed that the new impeller provides reliable viscosity measurements of homogenous fluids such as neat bitumen. With regards to complex fluids the new impeller showed a more stable and realistic trend than that obtained by using a standard spindle. In fact, it was demonstrated that the new impeller significantly decreases phase separation within the blend and in turns provides a more realistic measurement of the viscosity. This system represents a feasible and improved solution for optimising the laboratory modification process of tyre rubber bitumen blends by adapting the rotational viscometer as a low-shear mixer. Elsevier 2014-04-13 Article PeerReviewed Lo Presti, Davide, Fecarotti, Claudia, Clare, Adam T. and Airey, Gordon (2014) Toward more realistic viscosity measurements of tyre rubber–bitumen blends. Construction and Building Materials . ISSN 0950-0618 (In Press) http://www.sciencedirect.com/science/article/pii/S0950061814003018 doi:10.1016/j.conbuildmat.2014.03.038 doi:10.1016/j.conbuildmat.2014.03.038
spellingShingle Lo Presti, Davide
Fecarotti, Claudia
Clare, Adam T.
Airey, Gordon
Toward more realistic viscosity measurements of tyre rubber–bitumen blends
title Toward more realistic viscosity measurements of tyre rubber–bitumen blends
title_full Toward more realistic viscosity measurements of tyre rubber–bitumen blends
title_fullStr Toward more realistic viscosity measurements of tyre rubber–bitumen blends
title_full_unstemmed Toward more realistic viscosity measurements of tyre rubber–bitumen blends
title_short Toward more realistic viscosity measurements of tyre rubber–bitumen blends
title_sort toward more realistic viscosity measurements of tyre rubber–bitumen blends
url https://eprints.nottingham.ac.uk/3125/
https://eprints.nottingham.ac.uk/3125/
https://eprints.nottingham.ac.uk/3125/