GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans

GC–MS metabolomics was used to discriminate the phytochemicals profile of Indonesian white, red, and black rice brans, and Japanese white rice brans. This technique was used for the first time to identify compounds in rice brans having cytotoxic activity against WiDr colon cancer cells. Orthogonal P...

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Main Authors: Yuliana, Nancy Dewi, Tuarita, Mirna Zena, Khatib, Alfi, Laila, Farida, Sukarno, Sukarno
Format: Article
Language:English
English
English
Published: The Korean Society of Food Science and Technology 2020
Subjects:
Online Access:http://irep.iium.edu.my/82261/
http://irep.iium.edu.my/82261/15/82261_GC%E2%80%93MS%20metabolomics%20revealed.pdf
http://irep.iium.edu.my/82261/2/82261_GC%E2%80%93MS%20metabolomics%20revealed_SCOPUS.pdf
http://irep.iium.edu.my/82261/3/82261_GC%E2%80%93MS%20metabolomics%20revealed_WOS.pdf
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author Yuliana, Nancy Dewi
Tuarita, Mirna Zena
Khatib, Alfi
Laila, Farida
Sukarno, Sukarno
author_facet Yuliana, Nancy Dewi
Tuarita, Mirna Zena
Khatib, Alfi
Laila, Farida
Sukarno, Sukarno
author_sort Yuliana, Nancy Dewi
building IIUM Repository
collection Online Access
description GC–MS metabolomics was used to discriminate the phytochemicals profile of Indonesian white, red, and black rice brans, and Japanese white rice brans. This technique was used for the first time to identify compounds in rice brans having cytotoxic activity against WiDr colon cancer cells. Orthogonal Projection to the Latent Structure (OPLS) analysis showed that protocatechuic acid (PA) was a discriminating factor found in black rice brans which strongly correlated with its cytotoxicity (IC50 8.53 ± 0.26 µM). Real time-PCR data demonstrated that PA cytotoxicity at different concentrations (1, 5, 10, 25 and 50 µg/mL) was mediated through different pathways. Bcl-2 expression was downregulated at all tested concentrations indicating apoptosis stimulation. At 1–10 ppm concentration, PA activated both intrinsic and extrinsic apoptosis pathways since the expression of p53, Bax, caspase-8, and caspase-9 were upregulated. At a higher dose (25 and 50 µg/mL), PA possibly involved in pyroptosis-mediated pro-inflammatory cell death by upregulating the expression of caspase-1 and caspase-7.
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institution International Islamic University Malaysia
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language English
English
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publishDate 2020
publisher The Korean Society of Food Science and Technology
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spelling iium-822612020-08-18T07:11:54Z http://irep.iium.edu.my/82261/ GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans Yuliana, Nancy Dewi Tuarita, Mirna Zena Khatib, Alfi Laila, Farida Sukarno, Sukarno Q Science (General) QK Botany GC–MS metabolomics was used to discriminate the phytochemicals profile of Indonesian white, red, and black rice brans, and Japanese white rice brans. This technique was used for the first time to identify compounds in rice brans having cytotoxic activity against WiDr colon cancer cells. Orthogonal Projection to the Latent Structure (OPLS) analysis showed that protocatechuic acid (PA) was a discriminating factor found in black rice brans which strongly correlated with its cytotoxicity (IC50 8.53 ± 0.26 µM). Real time-PCR data demonstrated that PA cytotoxicity at different concentrations (1, 5, 10, 25 and 50 µg/mL) was mediated through different pathways. Bcl-2 expression was downregulated at all tested concentrations indicating apoptosis stimulation. At 1–10 ppm concentration, PA activated both intrinsic and extrinsic apoptosis pathways since the expression of p53, Bax, caspase-8, and caspase-9 were upregulated. At a higher dose (25 and 50 µg/mL), PA possibly involved in pyroptosis-mediated pro-inflammatory cell death by upregulating the expression of caspase-1 and caspase-7. The Korean Society of Food Science and Technology 2020-06-01 Article PeerReviewed application/pdf en http://irep.iium.edu.my/82261/15/82261_GC%E2%80%93MS%20metabolomics%20revealed.pdf application/pdf en http://irep.iium.edu.my/82261/2/82261_GC%E2%80%93MS%20metabolomics%20revealed_SCOPUS.pdf application/pdf en http://irep.iium.edu.my/82261/3/82261_GC%E2%80%93MS%20metabolomics%20revealed_WOS.pdf Yuliana, Nancy Dewi and Tuarita, Mirna Zena and Khatib, Alfi and Laila, Farida and Sukarno, Sukarno (2020) GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans. Food Science and Biotechnology, 29 (6). pp. 825-835. ISSN 1226-7708 E-ISSN 2092-6456 https://link.springer.com/article/10.1007/s10068-019-00725-2 10.1007/s10068-019-00725-2
spellingShingle Q Science (General)
QK Botany
Yuliana, Nancy Dewi
Tuarita, Mirna Zena
Khatib, Alfi
Laila, Farida
Sukarno, Sukarno
GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans
title GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans
title_full GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans
title_fullStr GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans
title_full_unstemmed GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans
title_short GC–MS metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans
title_sort gc–ms metabolomics revealed protocatechuic acid as a cytotoxic and apoptosis-inducing compound from black rice brans
topic Q Science (General)
QK Botany
url http://irep.iium.edu.my/82261/
http://irep.iium.edu.my/82261/
http://irep.iium.edu.my/82261/
http://irep.iium.edu.my/82261/15/82261_GC%E2%80%93MS%20metabolomics%20revealed.pdf
http://irep.iium.edu.my/82261/2/82261_GC%E2%80%93MS%20metabolomics%20revealed_SCOPUS.pdf
http://irep.iium.edu.my/82261/3/82261_GC%E2%80%93MS%20metabolomics%20revealed_WOS.pdf