Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system

Human hexokinase II (HKII) is one of the key enzymes in the glycolytic pathway. It has been postulated that HKII is a potential target for anti-dengue (DENV) drug development, as well as involved in cancer and tumor cell growth. In this work, the human hexokinase II (HKII) gene was cloned into p...

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Main Authors: Tanbin, Suriyea, Ahmad Fuad, Fazia Adyani
Format: Proceeding Paper
Language:English
English
Published: Association for Computing Machinery 2019
Subjects:
Online Access:http://irep.iium.edu.my/79728/
http://irep.iium.edu.my/79728/9/79728_Expression%20and%20Purification%20of%20Soluble_new_complete.pdf
http://irep.iium.edu.my/79728/2/79728_Expression%20and%20Purification%20of%20Soluble%20Bacterially-Expressed_scopus.pdf
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author Tanbin, Suriyea
Ahmad Fuad, Fazia Adyani
author_facet Tanbin, Suriyea
Ahmad Fuad, Fazia Adyani
author_sort Tanbin, Suriyea
building IIUM Repository
collection Online Access
description Human hexokinase II (HKII) is one of the key enzymes in the glycolytic pathway. It has been postulated that HKII is a potential target for anti-dengue (DENV) drug development, as well as involved in cancer and tumor cell growth. In this work, the human hexokinase II (HKII) gene was cloned into pETite N-His SUMO vector and transformed into the E.coli strain HI-control 10G for the propagation of clones. Two different expression hosts, E.coli HI-controlTM BL21 (DE3) and BL21 (DE3) pLysS were used to optimize HKII expression. In order to obtain the soluble recombinant HKII in a functional form, we optimized protein expression at three different temperatures; 17°C, 25°C and 37°C, at 24 hours incubation time. The soluble protein was expressed in the presence of 0.5 mM isopropyl-2-Dthiogalactopyranoside (IPTG) in TB media at 17°C for 24 hrs. The expressed protein was then purified to homogeneity by a combination of Immobilized Metal Ion Affinity Chromatography (IMAC), size exclusion chromatography (SEC) and ion-exchange chromatography (IEX), resulting in pure bacterially-expressed HK2. Taken together, this study has successfully produced soluble bacterially-expressed human HKII that can be utilized for further therapeutic studies.
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format Proceeding Paper
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institution International Islamic University Malaysia
institution_category Local University
language English
English
last_indexed 2025-11-14T17:47:01Z
publishDate 2019
publisher Association for Computing Machinery
recordtype eprints
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spelling iium-797282022-03-17T08:08:19Z http://irep.iium.edu.my/79728/ Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system Tanbin, Suriyea Ahmad Fuad, Fazia Adyani QH Natural history TP248.13 Biotechnology Human hexokinase II (HKII) is one of the key enzymes in the glycolytic pathway. It has been postulated that HKII is a potential target for anti-dengue (DENV) drug development, as well as involved in cancer and tumor cell growth. In this work, the human hexokinase II (HKII) gene was cloned into pETite N-His SUMO vector and transformed into the E.coli strain HI-control 10G for the propagation of clones. Two different expression hosts, E.coli HI-controlTM BL21 (DE3) and BL21 (DE3) pLysS were used to optimize HKII expression. In order to obtain the soluble recombinant HKII in a functional form, we optimized protein expression at three different temperatures; 17°C, 25°C and 37°C, at 24 hours incubation time. The soluble protein was expressed in the presence of 0.5 mM isopropyl-2-Dthiogalactopyranoside (IPTG) in TB media at 17°C for 24 hrs. The expressed protein was then purified to homogeneity by a combination of Immobilized Metal Ion Affinity Chromatography (IMAC), size exclusion chromatography (SEC) and ion-exchange chromatography (IEX), resulting in pure bacterially-expressed HK2. Taken together, this study has successfully produced soluble bacterially-expressed human HKII that can be utilized for further therapeutic studies. Association for Computing Machinery 2019-03-28 Proceeding Paper NonPeerReviewed application/pdf en http://irep.iium.edu.my/79728/9/79728_Expression%20and%20Purification%20of%20Soluble_new_complete.pdf application/pdf en http://irep.iium.edu.my/79728/2/79728_Expression%20and%20Purification%20of%20Soluble%20Bacterially-Expressed_scopus.pdf Tanbin, Suriyea and Ahmad Fuad, Fazia Adyani (2019) Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system. In: "9th International Conference on Biomedical Engineering and Technology, ICBET 2019", 28 - 30 Mar 2019, Meiji UniversityTokyo, Japan. https://dl.acm.org/doi/pdf/10.1145/3326172.3326219 10.1145/3326172.3326219
spellingShingle QH Natural history
TP248.13 Biotechnology
Tanbin, Suriyea
Ahmad Fuad, Fazia Adyani
Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system
title Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system
title_full Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system
title_fullStr Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system
title_full_unstemmed Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system
title_short Expression and purification of soluble bacterially-expressed human hexokinase II in E.coli system
title_sort expression and purification of soluble bacterially-expressed human hexokinase ii in e.coli system
topic QH Natural history
TP248.13 Biotechnology
url http://irep.iium.edu.my/79728/
http://irep.iium.edu.my/79728/
http://irep.iium.edu.my/79728/
http://irep.iium.edu.my/79728/9/79728_Expression%20and%20Purification%20of%20Soluble_new_complete.pdf
http://irep.iium.edu.my/79728/2/79728_Expression%20and%20Purification%20of%20Soluble%20Bacterially-Expressed_scopus.pdf