Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media

The main purpose of this work is to experimentally investigate the concentration yields of exfoliated Graphene in organic solvents with the variation of different centrifugation speeds (rpm). Graphene was effectively fabricated by one of the most convenient chemical processing approach liquid-pha...

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Main Authors: Arifutzzaman, Abul, Ismail, Ahmad Faris, Yaacob, Iskandar Idris, Alam, Md Zahangir, Khan, Ahsan Ali
Format: Proceeding Paper
Language:English
English
Published: IOP Publishing Ltd 2019
Subjects:
Online Access:http://irep.iium.edu.my/72438/
http://irep.iium.edu.my/72438/1/72438%20Experimental%20investigation%20of%20concentration.pdf
http://irep.iium.edu.my/72438/2/72438%20Experimental%20investigation%20of%20concentration%20SCOPUS.pdf
_version_ 1848787614449008640
author Arifutzzaman, Abul
Ismail, Ahmad Faris
Yaacob, Iskandar Idris
Alam, Md Zahangir
Khan, Ahsan Ali
author_facet Arifutzzaman, Abul
Ismail, Ahmad Faris
Yaacob, Iskandar Idris
Alam, Md Zahangir
Khan, Ahsan Ali
author_sort Arifutzzaman, Abul
building IIUM Repository
collection Online Access
description The main purpose of this work is to experimentally investigate the concentration yields of exfoliated Graphene in organic solvents with the variation of different centrifugation speeds (rpm). Graphene was effectively fabricated by one of the most convenient chemical processing approach liquid-phase exfoliation (LPE) of graphite in two different organic solvent N-Methyl-2-Pyrrolidone (NMP) and N, N-dimethylformamide (DMF). After exfoliation separated supernatant dispersions were preserved into the other tube as product. Similar procedure was repeated with same parameter and same graphite for both of the solvents. FESEM analyses of the exfoliated Graphene samples revealed the presence of few layers of Graphene flakes stacking. Analysis of the Raman spectrum of the samples it was revealed that the precursor graphite flakes was converted to Graphene sheets. Concentrations of graphene suspensions in both solvents were measured from separately prepared standard graphs using Beer’s law with the aid of UV-vis absorbance spectroscopy. Estimated exfoliated graphene concentration was acquired higher for lower centrifugation (rpm) for both of the solvent. It was also seen that for the same rpm concentration of Graphene was higher in NMP than that of in DMF.
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format Proceeding Paper
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institution International Islamic University Malaysia
institution_category Local University
language English
English
last_indexed 2025-11-14T17:27:44Z
publishDate 2019
publisher IOP Publishing Ltd
recordtype eprints
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spelling iium-724382019-10-11T07:41:57Z http://irep.iium.edu.my/72438/ Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media Arifutzzaman, Abul Ismail, Ahmad Faris Yaacob, Iskandar Idris Alam, Md Zahangir Khan, Ahsan Ali T Technology (General) The main purpose of this work is to experimentally investigate the concentration yields of exfoliated Graphene in organic solvents with the variation of different centrifugation speeds (rpm). Graphene was effectively fabricated by one of the most convenient chemical processing approach liquid-phase exfoliation (LPE) of graphite in two different organic solvent N-Methyl-2-Pyrrolidone (NMP) and N, N-dimethylformamide (DMF). After exfoliation separated supernatant dispersions were preserved into the other tube as product. Similar procedure was repeated with same parameter and same graphite for both of the solvents. FESEM analyses of the exfoliated Graphene samples revealed the presence of few layers of Graphene flakes stacking. Analysis of the Raman spectrum of the samples it was revealed that the precursor graphite flakes was converted to Graphene sheets. Concentrations of graphene suspensions in both solvents were measured from separately prepared standard graphs using Beer’s law with the aid of UV-vis absorbance spectroscopy. Estimated exfoliated graphene concentration was acquired higher for lower centrifugation (rpm) for both of the solvent. It was also seen that for the same rpm concentration of Graphene was higher in NMP than that of in DMF. IOP Publishing Ltd 2019-03-20 Proceeding Paper PeerReviewed application/pdf en http://irep.iium.edu.my/72438/1/72438%20Experimental%20investigation%20of%20concentration.pdf application/pdf en http://irep.iium.edu.my/72438/2/72438%20Experimental%20investigation%20of%20concentration%20SCOPUS.pdf Arifutzzaman, Abul and Ismail, Ahmad Faris and Yaacob, Iskandar Idris and Alam, Md Zahangir and Khan, Ahsan Ali (2019) Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media. In: 4th International Conference on Mechanical, Automotive and Aerospace Engineering (ICMAAE 2018), 19th-20th September 2018, Kuala Lumpur, Malaysia. https://iopscience.iop.org/article/10.1088/1757-899X/488/1/012001/pdf 10.1088/1757-899X/488/1/012001
spellingShingle T Technology (General)
Arifutzzaman, Abul
Ismail, Ahmad Faris
Yaacob, Iskandar Idris
Alam, Md Zahangir
Khan, Ahsan Ali
Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media
title Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media
title_full Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media
title_fullStr Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media
title_full_unstemmed Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media
title_short Experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media
title_sort experimental investigation of concentration yields of liquid phase exfoliated graphene in organic solvent media
topic T Technology (General)
url http://irep.iium.edu.my/72438/
http://irep.iium.edu.my/72438/
http://irep.iium.edu.my/72438/
http://irep.iium.edu.my/72438/1/72438%20Experimental%20investigation%20of%20concentration.pdf
http://irep.iium.edu.my/72438/2/72438%20Experimental%20investigation%20of%20concentration%20SCOPUS.pdf