Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber

In this study, the microcrystalline cellulose (MCC) was extracted via a non-acidic method from the oil palm empty fruit bunch (EFB) cellulose. The extraction was conducted through Ammonium Persulfate (APS) oxidation treatment, which was followed by the ball milling process. The effects of varied tem...

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Main Authors: Samat, Noorasikin, Ghazali, Nurul Najihah, Ahmad, Zuraida, Ali, Fathilah
Format: Article
Language:English
Published: International Journal of Engineering and Technology(UAE) 2018
Subjects:
Online Access:http://irep.iium.edu.my/70900/
http://irep.iium.edu.my/70900/1/70900_Non-Acidic%20Method%20for%20Isolation.pdf
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author Samat, Noorasikin
Ghazali, Nurul Najihah
Ahmad, Zuraida
Ali, Fathilah
author_facet Samat, Noorasikin
Ghazali, Nurul Najihah
Ahmad, Zuraida
Ali, Fathilah
author_sort Samat, Noorasikin
building IIUM Repository
collection Online Access
description In this study, the microcrystalline cellulose (MCC) was extracted via a non-acidic method from the oil palm empty fruit bunch (EFB) cellulose. The extraction was conducted through Ammonium Persulfate (APS) oxidation treatment, which was followed by the ball milling process. The effects of varied temperature levels from APS oxidation treatment (60, 80 and 90oC) and different milling time (1, 4 hours) were investigated. APS oxidation treatment at 90oC was found to produce the most optimum results. The size of the MCC was less than 20μm and had demonstrated the highest degree of crystallinity index and thermal stability. The high crystallinity index is associated with the removal of non-cellulosic components as seen from FTIR analysis, where a decrease was observed in the characteristic peak intensity of 1735 and 1510 cm-1. The milling time had also affected the formation of MCC. Although a relatively longer milling time had produced smaller MCC with narrow size distribution, it had, however, given rise to a slight adverse effect on the crystallinity index and thermal stability.
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spelling iium-709002019-07-12T08:35:00Z http://irep.iium.edu.my/70900/ Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber Samat, Noorasikin Ghazali, Nurul Najihah Ahmad, Zuraida Ali, Fathilah TP248.13 Biotechnology TP368 Food processing and manufacture In this study, the microcrystalline cellulose (MCC) was extracted via a non-acidic method from the oil palm empty fruit bunch (EFB) cellulose. The extraction was conducted through Ammonium Persulfate (APS) oxidation treatment, which was followed by the ball milling process. The effects of varied temperature levels from APS oxidation treatment (60, 80 and 90oC) and different milling time (1, 4 hours) were investigated. APS oxidation treatment at 90oC was found to produce the most optimum results. The size of the MCC was less than 20μm and had demonstrated the highest degree of crystallinity index and thermal stability. The high crystallinity index is associated with the removal of non-cellulosic components as seen from FTIR analysis, where a decrease was observed in the characteristic peak intensity of 1735 and 1510 cm-1. The milling time had also affected the formation of MCC. Although a relatively longer milling time had produced smaller MCC with narrow size distribution, it had, however, given rise to a slight adverse effect on the crystallinity index and thermal stability. International Journal of Engineering and Technology(UAE) 2018 Article PeerReviewed application/pdf en http://irep.iium.edu.my/70900/1/70900_Non-Acidic%20Method%20for%20Isolation.pdf Samat, Noorasikin and Ghazali, Nurul Najihah and Ahmad, Zuraida and Ali, Fathilah (2018) Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber. International Journal of Engineering & Technology, 7 (4014). pp. 339-342. ISSN 2227-524X https://www.sciencepubco.com/index.php/ijet/article/view/27670
spellingShingle TP248.13 Biotechnology
TP368 Food processing and manufacture
Samat, Noorasikin
Ghazali, Nurul Najihah
Ahmad, Zuraida
Ali, Fathilah
Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber
title Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber
title_full Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber
title_fullStr Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber
title_full_unstemmed Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber
title_short Non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber
title_sort non-acidic method for isolation of microcrystalline cellulose from oil palm empty fruit bunch fiber
topic TP248.13 Biotechnology
TP368 Food processing and manufacture
url http://irep.iium.edu.my/70900/
http://irep.iium.edu.my/70900/
http://irep.iium.edu.my/70900/1/70900_Non-Acidic%20Method%20for%20Isolation.pdf