Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds

Other than grain coarsening, the loss of corrosion resistance in ferritic stainless steel (FSS) welds due to intergranular precipitation of chromium carbides restricts the use of the alloy for structural application. The use of cryogenic cooling offers dual opportunities for the control of weld geom...

Full description

Bibliographic Details
Main Authors: Amuda, Muhammed Olawale Hakeem, Mridha, Shahjahan
Format: Proceeding Paper
Language:English
Published: 2011
Subjects:
Online Access:http://irep.iium.edu.my/6063/
http://irep.iium.edu.my/6063/1/Carbide_precipitation_in_FSS_welds.pdf
_version_ 1848776608315342848
author Amuda, Muhammed Olawale Hakeem
Mridha, Shahjahan
author_facet Amuda, Muhammed Olawale Hakeem
Mridha, Shahjahan
author_sort Amuda, Muhammed Olawale Hakeem
building IIUM Repository
collection Online Access
description Other than grain coarsening, the loss of corrosion resistance in ferritic stainless steel (FSS) welds due to intergranular precipitation of chromium carbides restricts the use of the alloy for structural application. The use of cryogenic cooling offers dual opportunities for the control of weld geometry and grain structure in FSS. This results in improved mechanical properties but the effect on carbide precipitation was not investigated. In this paper, the effect of heat flux, welding speed and flow rate of cryogenic liquid on carbide precipitation in 16% chromium FSS welds are discussed. The use of cryogenic cooling reduces the size of the sensitized zone but this is not significantly affected by the flow rate of the cryogenic fluid. Compared to the conventional welding, the cryogenic cooling increases the cooling rate and reduces the martensite content in the high temperature heat affected zone (HTHAZ) by about 20%. This results in wider ditched-structure in welds made with flow rates lower than 0.052L/min. Cryogenic cooling produces more ditched weld microstructure revealed by electrolytic etching in oxalic acid; however, the structure is acceptable since no single grain boundary is completely surrounded by ditches.
first_indexed 2025-11-14T14:32:48Z
format Proceeding Paper
id iium-6063
institution International Islamic University Malaysia
institution_category Local University
language English
last_indexed 2025-11-14T14:32:48Z
publishDate 2011
recordtype eprints
repository_type Digital Repository
spelling iium-60632011-11-21T21:19:08Z http://irep.iium.edu.my/6063/ Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds Amuda, Muhammed Olawale Hakeem Mridha, Shahjahan TN600 Metallurgy Other than grain coarsening, the loss of corrosion resistance in ferritic stainless steel (FSS) welds due to intergranular precipitation of chromium carbides restricts the use of the alloy for structural application. The use of cryogenic cooling offers dual opportunities for the control of weld geometry and grain structure in FSS. This results in improved mechanical properties but the effect on carbide precipitation was not investigated. In this paper, the effect of heat flux, welding speed and flow rate of cryogenic liquid on carbide precipitation in 16% chromium FSS welds are discussed. The use of cryogenic cooling reduces the size of the sensitized zone but this is not significantly affected by the flow rate of the cryogenic fluid. Compared to the conventional welding, the cryogenic cooling increases the cooling rate and reduces the martensite content in the high temperature heat affected zone (HTHAZ) by about 20%. This results in wider ditched-structure in welds made with flow rates lower than 0.052L/min. Cryogenic cooling produces more ditched weld microstructure revealed by electrolytic etching in oxalic acid; however, the structure is acceptable since no single grain boundary is completely surrounded by ditches. 2011 Proceeding Paper NonPeerReviewed application/pdf en http://irep.iium.edu.my/6063/1/Carbide_precipitation_in_FSS_welds.pdf Amuda, Muhammed Olawale Hakeem and Mridha, Shahjahan (2011) Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds. In: 14th International Conference on Advances in Material and Processing Technologies (AMPT 2011), 13-16 July 2011, Istanbul, Turkey. (Unpublished) http://www.ampt2011.org/en/
spellingShingle TN600 Metallurgy
Amuda, Muhammed Olawale Hakeem
Mridha, Shahjahan
Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds
title Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds
title_full Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds
title_fullStr Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds
title_full_unstemmed Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds
title_short Parametric study of carbide precipitation in 16% chromium ferritic stainless steel (FSS) welds
title_sort parametric study of carbide precipitation in 16% chromium ferritic stainless steel (fss) welds
topic TN600 Metallurgy
url http://irep.iium.edu.my/6063/
http://irep.iium.edu.my/6063/
http://irep.iium.edu.my/6063/1/Carbide_precipitation_in_FSS_welds.pdf