Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths

Cobalt-platinum (Co-Pt) nanocrystalline alloy films were electrodeposited using a novel stable single-bath system containing a complex forming additive which stabilised the Co+2 ions and enhanced codeposition with platinum complexes. The compositions of the electrodeposits was controlled by adjustin...

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Main Authors: Teh, Seohhian, Johan, Mohd Rafie, Yaacob, Iskandar Idris
Format: Article
Language:English
English
Published: Maney Publishing 2014
Subjects:
Online Access:http://irep.iium.edu.my/58535/
http://irep.iium.edu.my/58535/1/58535_ynthesis%20and%20characterisatio_article.pdf
http://irep.iium.edu.my/58535/2/58535_ynthesis%20and%20characterisatio_scopus.pdf
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author Teh, Seohhian
Johan, Mohd Rafie
Yaacob, Iskandar Idris
author_facet Teh, Seohhian
Johan, Mohd Rafie
Yaacob, Iskandar Idris
author_sort Teh, Seohhian
building IIUM Repository
collection Online Access
description Cobalt-platinum (Co-Pt) nanocrystalline alloy films were electrodeposited using a novel stable single-bath system containing a complex forming additive which stabilised the Co+2 ions and enhanced codeposition with platinum complexes. The compositions of the electrodeposits was controlled by adjusting the metal ions ratio in the electrolytic bath and by varying the current density. X-ray diffraction results showed that the as-deposited films contained face-centred cubic CoPt3 phase and the calculated crystallite sizes were in nanoscale dimension in a range of 3-10 nm. Scanning electron microscopy results showed formation of granules and clusters. Atomic force microscopy and infinite focus microscopy results showed granular surface morphology and approximately similar surface roughness value on Co43-Pt57 film. Magnetic force microscopy characterisation on Co43-Pt57 showed existence of correlation between magnetic force and surface topography. The saturation magnetisation values of as-synthesised nanostructured Co-Pt films increased with increasing of Co content.
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language English
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publishDate 2014
publisher Maney Publishing
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spelling iium-585352017-09-26T05:37:41Z http://irep.iium.edu.my/58535/ Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths Teh, Seohhian Johan, Mohd Rafie Yaacob, Iskandar Idris QC Physics TA Engineering (General). Civil engineering (General) Cobalt-platinum (Co-Pt) nanocrystalline alloy films were electrodeposited using a novel stable single-bath system containing a complex forming additive which stabilised the Co+2 ions and enhanced codeposition with platinum complexes. The compositions of the electrodeposits was controlled by adjusting the metal ions ratio in the electrolytic bath and by varying the current density. X-ray diffraction results showed that the as-deposited films contained face-centred cubic CoPt3 phase and the calculated crystallite sizes were in nanoscale dimension in a range of 3-10 nm. Scanning electron microscopy results showed formation of granules and clusters. Atomic force microscopy and infinite focus microscopy results showed granular surface morphology and approximately similar surface roughness value on Co43-Pt57 film. Magnetic force microscopy characterisation on Co43-Pt57 showed existence of correlation between magnetic force and surface topography. The saturation magnetisation values of as-synthesised nanostructured Co-Pt films increased with increasing of Co content. Maney Publishing 2014-12 Article PeerReviewed application/pdf en http://irep.iium.edu.my/58535/1/58535_ynthesis%20and%20characterisatio_article.pdf application/pdf en http://irep.iium.edu.my/58535/2/58535_ynthesis%20and%20characterisatio_scopus.pdf Teh, Seohhian and Johan, Mohd Rafie and Yaacob, Iskandar Idris (2014) Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths. Materials Research Innovations, 18. S6-286-S6-290. ISSN 1432-8917 E-ISSN 1433-075X http://www.tandfonline.com/doi/abs/10.1179/1432891714Z.000000000969 10.1179/1432891714Z.000000000969
spellingShingle QC Physics
TA Engineering (General). Civil engineering (General)
Teh, Seohhian
Johan, Mohd Rafie
Yaacob, Iskandar Idris
Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths
title Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths
title_full Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths
title_fullStr Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths
title_full_unstemmed Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths
title_short Synthesis and characterisation of nanostructured Co-Pt magnetic films electrodeposited from tartrate-stabilised chloride baths
title_sort synthesis and characterisation of nanostructured co-pt magnetic films electrodeposited from tartrate-stabilised chloride baths
topic QC Physics
TA Engineering (General). Civil engineering (General)
url http://irep.iium.edu.my/58535/
http://irep.iium.edu.my/58535/
http://irep.iium.edu.my/58535/
http://irep.iium.edu.my/58535/1/58535_ynthesis%20and%20characterisatio_article.pdf
http://irep.iium.edu.my/58535/2/58535_ynthesis%20and%20characterisatio_scopus.pdf