Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.
Oil palm fronds biomass was used as a source for isolation of cellulose nanowhiskers (CNW), and its subsequent characterization was done. Non-cellulosic components such a lignin, hemicellulose, and pectin were removed from the biomass by chemimechanical alkaline hydrogen peroxide method followed by...
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| Format: | Article |
| Language: | English English |
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NC State University
2016
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| Online Access: | http://irep.iium.edu.my/53855/ http://irep.iium.edu.my/53855/1/BioRes_11_3_6742_Saurabh_DOSZASK_Effect_Hydroly_Treat_CNW_Oil_Palm_Fronds_9745.pdf http://irep.iium.edu.my/53855/7/53855_Effect%20of%20hydrolysis%20treatment%20on%20cellulose_wos.pdf |
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| author | K. Saurabh, Chaturbhuj Dungani, Rudi A.F., Owolabi N.S., Atiqah Ashaari, Zaidon N. A., Sri Aprilia Sarker, Md. Zaidul Islam H. P. S., Abdul Khalil |
| author_facet | K. Saurabh, Chaturbhuj Dungani, Rudi A.F., Owolabi N.S., Atiqah Ashaari, Zaidon N. A., Sri Aprilia Sarker, Md. Zaidul Islam H. P. S., Abdul Khalil |
| author_sort | K. Saurabh, Chaturbhuj |
| building | IIUM Repository |
| collection | Online Access |
| description | Oil palm fronds biomass was used as a source for isolation of cellulose nanowhiskers (CNW), and its subsequent characterization was done. Non-cellulosic components such a lignin, hemicellulose, and pectin were removed from the biomass by chemimechanical alkaline hydrogen peroxide method followed by sulphuric acid hydrolysis having different time duration of hydrolysis. Apart from the progressive reduction in peaks characteristic of hemicellulose and lignin dissolution, FTIR spectroscopy analysis showed that the hydrolysis did not affect the chemical structure of CNW was revealed by TEM. XRD analysis revealed that the natural structural of cellulose I polymorph was mantained irrespective of the hydrolysis time. High thermal stability and aspect ratio of the extracted CNW demostrated its suitability as a reinforcement material in nanocomposites. |
| first_indexed | 2025-11-14T16:35:07Z |
| format | Article |
| id | iium-53855 |
| institution | International Islamic University Malaysia |
| institution_category | Local University |
| language | English English |
| last_indexed | 2025-11-14T16:35:07Z |
| publishDate | 2016 |
| publisher | NC State University |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | iium-538552017-04-13T07:03:00Z http://irep.iium.edu.my/53855/ Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. K. Saurabh, Chaturbhuj Dungani, Rudi A.F., Owolabi N.S., Atiqah Ashaari, Zaidon N. A., Sri Aprilia Sarker, Md. Zaidul Islam H. P. S., Abdul Khalil R Medicine (General) Oil palm fronds biomass was used as a source for isolation of cellulose nanowhiskers (CNW), and its subsequent characterization was done. Non-cellulosic components such a lignin, hemicellulose, and pectin were removed from the biomass by chemimechanical alkaline hydrogen peroxide method followed by sulphuric acid hydrolysis having different time duration of hydrolysis. Apart from the progressive reduction in peaks characteristic of hemicellulose and lignin dissolution, FTIR spectroscopy analysis showed that the hydrolysis did not affect the chemical structure of CNW was revealed by TEM. XRD analysis revealed that the natural structural of cellulose I polymorph was mantained irrespective of the hydrolysis time. High thermal stability and aspect ratio of the extracted CNW demostrated its suitability as a reinforcement material in nanocomposites. NC State University 2016 Article PeerReviewed application/pdf en http://irep.iium.edu.my/53855/1/BioRes_11_3_6742_Saurabh_DOSZASK_Effect_Hydroly_Treat_CNW_Oil_Palm_Fronds_9745.pdf application/pdf en http://irep.iium.edu.my/53855/7/53855_Effect%20of%20hydrolysis%20treatment%20on%20cellulose_wos.pdf K. Saurabh, Chaturbhuj and Dungani, Rudi and A.F., Owolabi and N.S., Atiqah and Ashaari, Zaidon and N. A., Sri Aprilia and Sarker, Md. Zaidul Islam and H. P. S., Abdul Khalil (2016) Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. BioResources, 11 (3). pp. 6742-6755. ISSN 1930-2126 http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_3_6742_Saurabh_Hydrolysis_Cellulose_Nanowhiskers |
| spellingShingle | R Medicine (General) K. Saurabh, Chaturbhuj Dungani, Rudi A.F., Owolabi N.S., Atiqah Ashaari, Zaidon N. A., Sri Aprilia Sarker, Md. Zaidul Islam H. P. S., Abdul Khalil Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. |
| title | Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. |
| title_full | Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. |
| title_fullStr | Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. |
| title_full_unstemmed | Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. |
| title_short | Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. |
| title_sort | effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. |
| topic | R Medicine (General) |
| url | http://irep.iium.edu.my/53855/ http://irep.iium.edu.my/53855/ http://irep.iium.edu.my/53855/1/BioRes_11_3_6742_Saurabh_DOSZASK_Effect_Hydroly_Treat_CNW_Oil_Palm_Fronds_9745.pdf http://irep.iium.edu.my/53855/7/53855_Effect%20of%20hydrolysis%20treatment%20on%20cellulose_wos.pdf |