Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method

Gold nanoparticles supported on zinc oxide nanoparticles were synthesized at several pH levels via the deposition-precipitation (DP) method. The effects of pH on gold loading, particle size, and particle size distribution on the support were studied at the iso-electric point (IEP) as well as below...

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Main Authors: Yazid, Hanani, Adnan, Rohana, Abd Hamid, Shafida, Farrukh, Muhammad Akhyar
Format: Article
Language:English
Published: The Scientific and Technological Research Council of Turkey 2010
Subjects:
Online Access:http://irep.iium.edu.my/5345/
http://irep.iium.edu.my/5345/1/goldnano.pdf
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author Yazid, Hanani
Adnan, Rohana
Abd Hamid, Shafida
Farrukh, Muhammad Akhyar
author_facet Yazid, Hanani
Adnan, Rohana
Abd Hamid, Shafida
Farrukh, Muhammad Akhyar
author_sort Yazid, Hanani
building IIUM Repository
collection Online Access
description Gold nanoparticles supported on zinc oxide nanoparticles were synthesized at several pH levels via the deposition-precipitation (DP) method. The effects of pH on gold loading, particle size, and particle size distribution on the support were studied at the iso-electric point (IEP) as well as below and above the IEP of ZnO. The addition of the support significantly changed the pH of the solution. The effects of adjusting the pH before and after the addition of the support into the gold chloride solution were also investigated. Gold particles with diameters of less than 5 nm were obtained. The results revealed that gold loading depends on the pH, while gold particle size and distribution are independent of pH adjustment. Structural and elemental characterizations of the gold nanorods were carried out using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy-dispersive X-rays (EDX), atomic absorption spectrometry (AAS), and ultraviolet-visible spectrophotometry (UV-Vis).
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spelling iium-53452011-11-22T08:54:14Z http://irep.iium.edu.my/5345/ Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method Yazid, Hanani Adnan, Rohana Abd Hamid, Shafida Farrukh, Muhammad Akhyar QD Chemistry Gold nanoparticles supported on zinc oxide nanoparticles were synthesized at several pH levels via the deposition-precipitation (DP) method. The effects of pH on gold loading, particle size, and particle size distribution on the support were studied at the iso-electric point (IEP) as well as below and above the IEP of ZnO. The addition of the support significantly changed the pH of the solution. The effects of adjusting the pH before and after the addition of the support into the gold chloride solution were also investigated. Gold particles with diameters of less than 5 nm were obtained. The results revealed that gold loading depends on the pH, while gold particle size and distribution are independent of pH adjustment. Structural and elemental characterizations of the gold nanorods were carried out using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy-dispersive X-rays (EDX), atomic absorption spectrometry (AAS), and ultraviolet-visible spectrophotometry (UV-Vis). The Scientific and Technological Research Council of Turkey 2010 Article PeerReviewed application/pdf en http://irep.iium.edu.my/5345/1/goldnano.pdf Yazid, Hanani and Adnan, Rohana and Abd Hamid, Shafida and Farrukh, Muhammad Akhyar (2010) Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method. Turkish Journal of Chemistry, 34. pp. 639-650. ISSN 1300-0527(P), 1303-6130(O) http://journals.tubitak.gov.tr/chem/index.php doi:10.3906/kim-0912-379
spellingShingle QD Chemistry
Yazid, Hanani
Adnan, Rohana
Abd Hamid, Shafida
Farrukh, Muhammad Akhyar
Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
title Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
title_full Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
title_fullStr Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
title_full_unstemmed Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
title_short Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
title_sort synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
topic QD Chemistry
url http://irep.iium.edu.my/5345/
http://irep.iium.edu.my/5345/
http://irep.iium.edu.my/5345/
http://irep.iium.edu.my/5345/1/goldnano.pdf