2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate
In the main molecule of the title compound, C22H20N2O4·1.13CH4O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent molecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13) and 0.249 (...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2009
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| Online Access: | http://irep.iium.edu.my/4369/ http://irep.iium.edu.my/4369/1/2-%5B1-%282-Hydr-oxy-3-methoxy-benz-yl%29.pdf |
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| author | Al-Douh, Mohammed H. Osman, Hasnah Abd Hamid, Shafida Kia, Reza Fun, Hoong-Kun |
| author_facet | Al-Douh, Mohammed H. Osman, Hasnah Abd Hamid, Shafida Kia, Reza Fun, Hoong-Kun |
| author_sort | Al-Douh, Mohammed H. |
| building | IIUM Repository |
| collection | Online Access |
| description | In the main molecule of the title compound, C22H20N2O4·1.13CH4O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent molecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13) and 0.249 (5). The crystal structure is stabilized by intermolecular O-HO, O-HN and C-HO hydrogen bonds. The crystal studied was a merohedral twin [BASF ratio of 0.917 (1)/0.083 (1)].
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| first_indexed | 2025-11-14T14:28:11Z |
| format | Article |
| id | iium-4369 |
| institution | International Islamic University Malaysia |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-14T14:28:11Z |
| publishDate | 2009 |
| publisher | International Union of Crystallography |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | iium-43692011-12-16T00:16:29Z http://irep.iium.edu.my/4369/ 2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate Al-Douh, Mohammed H. Osman, Hasnah Abd Hamid, Shafida Kia, Reza Fun, Hoong-Kun QD Chemistry In the main molecule of the title compound, C22H20N2O4·1.13CH4O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent molecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13) and 0.249 (5). The crystal structure is stabilized by intermolecular O-HO, O-HN and C-HO hydrogen bonds. The crystal studied was a merohedral twin [BASF ratio of 0.917 (1)/0.083 (1)]. International Union of Crystallography 2009-04 Article PeerReviewed application/pdf en http://irep.iium.edu.my/4369/1/2-%5B1-%282-Hydr-oxy-3-methoxy-benz-yl%29.pdf Al-Douh, Mohammed H. and Osman, Hasnah and Abd Hamid, Shafida and Kia, Reza and Fun, Hoong-Kun (2009) 2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate. Acta Crystallographica Section E Structure Reports Online, 65 (4). o925-o926. ISSN 1600-5368 http://dx.doi.org/10.1107/S1600536809011192 doi:10.1107/S1600536809011192 |
| spellingShingle | QD Chemistry Al-Douh, Mohammed H. Osman, Hasnah Abd Hamid, Shafida Kia, Reza Fun, Hoong-Kun 2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate |
| title | 2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate |
| title_full | 2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate |
| title_fullStr | 2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate |
| title_full_unstemmed | 2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate |
| title_short | 2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate |
| title_sort | 2-[1-(2-hydroxy-3-methoxybenzyl)-1h-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate |
| topic | QD Chemistry |
| url | http://irep.iium.edu.my/4369/ http://irep.iium.edu.my/4369/ http://irep.iium.edu.my/4369/ http://irep.iium.edu.my/4369/1/2-%5B1-%282-Hydr-oxy-3-methoxy-benz-yl%29.pdf |