Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology
Response surface methodology (RSM) was used to determine the effects of high pressure homogenization (HPH) parameters (pressure and number of cycles) on the isolated yield, crystallinity, and diameter of kenaf bast cellulose nanofibers (CNF). Central composite design of experiments was utilized to...
| Main Authors: | , , , , , , |
|---|---|
| Format: | Article |
| Language: | English English |
| Published: |
Elsevier
2015
|
| Subjects: | |
| Online Access: | http://irep.iium.edu.my/43424/ http://irep.iium.edu.my/43424/1/industrial_crops.pdf http://irep.iium.edu.my/43424/4/43424_Optimization%20of%20high%20pressure%20homogenization%20parameters.pdf |
| _version_ | 1848782447281438720 |
|---|---|
| author | Davoudpour, Yalda Hossain (Md.), Sohrab Abdul Khalil, H.P.S. Mohamad Haafiz, M.K. Mohd Ishak, Z.A. Hassan, Azman Sarker, Md. Zaidul Islam |
| author_facet | Davoudpour, Yalda Hossain (Md.), Sohrab Abdul Khalil, H.P.S. Mohamad Haafiz, M.K. Mohd Ishak, Z.A. Hassan, Azman Sarker, Md. Zaidul Islam |
| author_sort | Davoudpour, Yalda |
| building | IIUM Repository |
| collection | Online Access |
| description | Response surface methodology (RSM) was used to determine the effects of high pressure homogenization
(HPH) parameters (pressure and number of cycles) on the isolated yield, crystallinity, and diameter of
kenaf bast cellulose nanofibers (CNF). Central composite design of experiments was utilized to determine
the optimal pressure and number of cycles of HPS for the highest CNF yield, crystallinity, and lowest CNF
diameter. The linear terms for the pressure and homogenization cycles had significant effects on the CNF
yield, crystallinity, and diameter, whereas the interaction between the pressure and homogenization
cycles had a significant effect on the CNF crystallinity. The optimized experimental conditions for the
HPH process were a homogenization pressure of 56 MPa, 44 P homogenization cycles, and a 0.1 wt% fiber
suspension concentration. Under these conditions,the isolated kenaf bast CNF yield was 89.9% with 56.5%
CNF crystallinity and a CNF diameter of 8 nm |
| first_indexed | 2025-11-14T16:05:36Z |
| format | Article |
| id | iium-43424 |
| institution | International Islamic University Malaysia |
| institution_category | Local University |
| language | English English |
| last_indexed | 2025-11-14T16:05:36Z |
| publishDate | 2015 |
| publisher | Elsevier |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | iium-434242017-11-03T04:33:45Z http://irep.iium.edu.my/43424/ Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology Davoudpour, Yalda Hossain (Md.), Sohrab Abdul Khalil, H.P.S. Mohamad Haafiz, M.K. Mohd Ishak, Z.A. Hassan, Azman Sarker, Md. Zaidul Islam Q Science (General) T Technology (General) Response surface methodology (RSM) was used to determine the effects of high pressure homogenization (HPH) parameters (pressure and number of cycles) on the isolated yield, crystallinity, and diameter of kenaf bast cellulose nanofibers (CNF). Central composite design of experiments was utilized to determine the optimal pressure and number of cycles of HPS for the highest CNF yield, crystallinity, and lowest CNF diameter. The linear terms for the pressure and homogenization cycles had significant effects on the CNF yield, crystallinity, and diameter, whereas the interaction between the pressure and homogenization cycles had a significant effect on the CNF crystallinity. The optimized experimental conditions for the HPH process were a homogenization pressure of 56 MPa, 44 P homogenization cycles, and a 0.1 wt% fiber suspension concentration. Under these conditions,the isolated kenaf bast CNF yield was 89.9% with 56.5% CNF crystallinity and a CNF diameter of 8 nm Elsevier 2015 Article PeerReviewed application/pdf en http://irep.iium.edu.my/43424/1/industrial_crops.pdf application/pdf en http://irep.iium.edu.my/43424/4/43424_Optimization%20of%20high%20pressure%20homogenization%20parameters.pdf Davoudpour, Yalda and Hossain (Md.), Sohrab and Abdul Khalil, H.P.S. and Mohamad Haafiz, M.K. and Mohd Ishak, Z.A. and Hassan, Azman and Sarker, Md. Zaidul Islam (2015) Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology. Industrial Crops and Products, 74. pp. 381-387. ISSN 0926-6690 http://dx.doi.org/10.1016/j.indcrop.2015.05.029 |
| spellingShingle | Q Science (General) T Technology (General) Davoudpour, Yalda Hossain (Md.), Sohrab Abdul Khalil, H.P.S. Mohamad Haafiz, M.K. Mohd Ishak, Z.A. Hassan, Azman Sarker, Md. Zaidul Islam Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology |
| title | Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology |
| title_full | Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology |
| title_fullStr | Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology |
| title_full_unstemmed | Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology |
| title_short | Optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology |
| title_sort | optimization of high pressure homogenization parameters for the isolation of cellulosic nanofibers using response surface methodology |
| topic | Q Science (General) T Technology (General) |
| url | http://irep.iium.edu.my/43424/ http://irep.iium.edu.my/43424/ http://irep.iium.edu.my/43424/1/industrial_crops.pdf http://irep.iium.edu.my/43424/4/43424_Optimization%20of%20high%20pressure%20homogenization%20parameters.pdf |