Improved efficiency of tocotrienol extraction from fresh and processed latex

Vitamin E, mainly in the form of tocotrienols, was extracted from Hevea brasiliensis latex with organic solvents. The content of tocotrienols and a small amount of tocopherols recovered from the latex was determined using high performance liquid chromatoghraphy (HPLC). Gas chromatoghraphy-mass spect...

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Main Authors: Sajari, Roslinda, Abd Razak, Nurul Hainiza, Yusof, Faridah, Mad Arif, Siti Arija, Perkins, M., Yeang, H. Y.
Format: Article
Language:English
English
Published: Malaysian Rubber Board, Malaysia 2014
Subjects:
Online Access:http://irep.iium.edu.my/41568/
http://irep.iium.edu.my/41568/1/P_57.pdf
http://irep.iium.edu.my/41568/3/41568_Improved%20efficiency%20of%20tocotrienol.SCOPUSpdf.pdf
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author Sajari, Roslinda
Abd Razak, Nurul Hainiza
Yusof, Faridah
Mad Arif, Siti Arija
Perkins, M.
Yeang, H. Y.
author_facet Sajari, Roslinda
Abd Razak, Nurul Hainiza
Yusof, Faridah
Mad Arif, Siti Arija
Perkins, M.
Yeang, H. Y.
author_sort Sajari, Roslinda
building IIUM Repository
collection Online Access
description Vitamin E, mainly in the form of tocotrienols, was extracted from Hevea brasiliensis latex with organic solvents. The content of tocotrienols and a small amount of tocopherols recovered from the latex was determined using high performance liquid chromatoghraphy (HPLC). Gas chromatoghraphy-mass spectrometry (GC-MS) confirmed the identities of the tocotrienols and tocopherols forms that were present. Gamma-tocotrienol was the most abundant form of vitamin E in Hevea latex. The yield of tocotrienols (339 ug/g of latex) was significantly increased by the use of the detergant Triton X-100 in the extraction procedure. This method improves the extraction efficiency by 83%. Through drying of the organic fraction using anhydrous magnesium sulphate following phase separation was also advantageous in the extraction procedure. On the other hand, the presence of ammonia in latex suspension reduced extraction efficiency. Vitamin E was also found in the waste serum generated from the processing of deproteinised natural rubber (DPNR). Although the yield vitamin from this source was relatively low, there is a potential to modify the processing procedure another value added end product i.e. latex vitamin E in addition to DPNR.
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publishDate 2014
publisher Malaysian Rubber Board, Malaysia
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spelling iium-415682017-09-19T01:24:05Z http://irep.iium.edu.my/41568/ Improved efficiency of tocotrienol extraction from fresh and processed latex Sajari, Roslinda Abd Razak, Nurul Hainiza Yusof, Faridah Mad Arif, Siti Arija Perkins, M. Yeang, H. Y. Q Science (General) Vitamin E, mainly in the form of tocotrienols, was extracted from Hevea brasiliensis latex with organic solvents. The content of tocotrienols and a small amount of tocopherols recovered from the latex was determined using high performance liquid chromatoghraphy (HPLC). Gas chromatoghraphy-mass spectrometry (GC-MS) confirmed the identities of the tocotrienols and tocopherols forms that were present. Gamma-tocotrienol was the most abundant form of vitamin E in Hevea latex. The yield of tocotrienols (339 ug/g of latex) was significantly increased by the use of the detergant Triton X-100 in the extraction procedure. This method improves the extraction efficiency by 83%. Through drying of the organic fraction using anhydrous magnesium sulphate following phase separation was also advantageous in the extraction procedure. On the other hand, the presence of ammonia in latex suspension reduced extraction efficiency. Vitamin E was also found in the waste serum generated from the processing of deproteinised natural rubber (DPNR). Although the yield vitamin from this source was relatively low, there is a potential to modify the processing procedure another value added end product i.e. latex vitamin E in addition to DPNR. Malaysian Rubber Board, Malaysia 2014 Article PeerReviewed application/pdf en http://irep.iium.edu.my/41568/1/P_57.pdf application/pdf en http://irep.iium.edu.my/41568/3/41568_Improved%20efficiency%20of%20tocotrienol.SCOPUSpdf.pdf Sajari, Roslinda and Abd Razak, Nurul Hainiza and Yusof, Faridah and Mad Arif, Siti Arija and Perkins, M. and Yeang, H. Y. (2014) Improved efficiency of tocotrienol extraction from fresh and processed latex. Journal of Rubber Research, 17 (4). pp. 245-260. ISSN 1511-1768 http://www.kppk.gov.my/
spellingShingle Q Science (General)
Sajari, Roslinda
Abd Razak, Nurul Hainiza
Yusof, Faridah
Mad Arif, Siti Arija
Perkins, M.
Yeang, H. Y.
Improved efficiency of tocotrienol extraction from fresh and processed latex
title Improved efficiency of tocotrienol extraction from fresh and processed latex
title_full Improved efficiency of tocotrienol extraction from fresh and processed latex
title_fullStr Improved efficiency of tocotrienol extraction from fresh and processed latex
title_full_unstemmed Improved efficiency of tocotrienol extraction from fresh and processed latex
title_short Improved efficiency of tocotrienol extraction from fresh and processed latex
title_sort improved efficiency of tocotrienol extraction from fresh and processed latex
topic Q Science (General)
url http://irep.iium.edu.my/41568/
http://irep.iium.edu.my/41568/
http://irep.iium.edu.my/41568/1/P_57.pdf
http://irep.iium.edu.my/41568/3/41568_Improved%20efficiency%20of%20tocotrienol.SCOPUSpdf.pdf