Synthesis of SiO2 nanostructures using sol-gel method

Sol-gel method is the simplest method and has the ability to control the particle size and morphology through systematic monitoring of reaction parameters. The objective of this research is to synthesize silica nanostructures by sol-gel method and to characterize the synthesized silica nanostructu...

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Main Authors: Hassan, Noor Azlina, J.N., Hasnidawani, Hassan, Norita, Surip,, Siti Norasmah
Format: Proceeding Paper
Language:English
English
Published: Polish Academy Of Sciences Institute Of Physics 2016
Subjects:
Online Access:http://irep.iium.edu.my/38498/
http://irep.iium.edu.my/38498/2/38498-Synthesis%20of%20SiO2%20Nanostructures%20Using%20Sol-Gel%20Method_SCOPUS.pdf
http://irep.iium.edu.my/38498/4/38498-new.pdf
_version_ 1848781619748405248
author Hassan, Noor Azlina
J.N., Hasnidawani
Hassan, Norita
Surip,, Siti Norasmah
author_facet Hassan, Noor Azlina
J.N., Hasnidawani
Hassan, Norita
Surip,, Siti Norasmah
author_sort Hassan, Noor Azlina
building IIUM Repository
collection Online Access
description Sol-gel method is the simplest method and has the ability to control the particle size and morphology through systematic monitoring of reaction parameters. The objective of this research is to synthesize silica nanostructures by sol-gel method and to characterize the synthesized silica nanostructures. Silica nanoparticles were synthesized via the sol-gel method using Tetraethyl orthosilicate as a precursor. The acetic acid and distilled water were used as the catalyst and the hydrolyzing agent. Varied parameters of the study were the aging time in the range of 2 to 6 h and the calcination temperature in the range of 600–700 ◦C. The obtained silica nanopowder was characterized using FESEM, and Nano-Particle Size Analyzer. The results show that the silica nanospheres were successfully synthesized by using sol-gel method with the optimum parameters of 700 ◦C of calcination temperature and 2 h of aging time. The average size of silica nanoparticles was in the range of 79.68 nm to 87.35 nm.
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format Proceeding Paper
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institution International Islamic University Malaysia
institution_category Local University
language English
English
last_indexed 2025-11-14T15:52:27Z
publishDate 2016
publisher Polish Academy Of Sciences Institute Of Physics
recordtype eprints
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spelling iium-384982018-02-25T09:21:20Z http://irep.iium.edu.my/38498/ Synthesis of SiO2 nanostructures using sol-gel method Hassan, Noor Azlina J.N., Hasnidawani Hassan, Norita Surip,, Siti Norasmah T Technology (General) Sol-gel method is the simplest method and has the ability to control the particle size and morphology through systematic monitoring of reaction parameters. The objective of this research is to synthesize silica nanostructures by sol-gel method and to characterize the synthesized silica nanostructures. Silica nanoparticles were synthesized via the sol-gel method using Tetraethyl orthosilicate as a precursor. The acetic acid and distilled water were used as the catalyst and the hydrolyzing agent. Varied parameters of the study were the aging time in the range of 2 to 6 h and the calcination temperature in the range of 600–700 ◦C. The obtained silica nanopowder was characterized using FESEM, and Nano-Particle Size Analyzer. The results show that the silica nanospheres were successfully synthesized by using sol-gel method with the optimum parameters of 700 ◦C of calcination temperature and 2 h of aging time. The average size of silica nanoparticles was in the range of 79.68 nm to 87.35 nm. Polish Academy Of Sciences Institute Of Physics 2016-04 Proceeding Paper PeerReviewed application/pdf en http://irep.iium.edu.my/38498/2/38498-Synthesis%20of%20SiO2%20Nanostructures%20Using%20Sol-Gel%20Method_SCOPUS.pdf application/pdf en http://irep.iium.edu.my/38498/4/38498-new.pdf Hassan, Noor Azlina and J.N., Hasnidawani and Hassan, Norita and Surip,, Siti Norasmah (2016) Synthesis of SiO2 nanostructures using sol-gel method. In: 5th International Advances in Applied Physics and Materials Science Congress & Exhibition (APMAS 2015), 16th-19th April 2015, Lykia, Oludeniz, Turkey. http://przyrbwn.icm.edu.pl/APP/PDF/129/a129z4p111.pdf 10.12693/APhysPolA.129.842
spellingShingle T Technology (General)
Hassan, Noor Azlina
J.N., Hasnidawani
Hassan, Norita
Surip,, Siti Norasmah
Synthesis of SiO2 nanostructures using sol-gel method
title Synthesis of SiO2 nanostructures using sol-gel method
title_full Synthesis of SiO2 nanostructures using sol-gel method
title_fullStr Synthesis of SiO2 nanostructures using sol-gel method
title_full_unstemmed Synthesis of SiO2 nanostructures using sol-gel method
title_short Synthesis of SiO2 nanostructures using sol-gel method
title_sort synthesis of sio2 nanostructures using sol-gel method
topic T Technology (General)
url http://irep.iium.edu.my/38498/
http://irep.iium.edu.my/38498/
http://irep.iium.edu.my/38498/
http://irep.iium.edu.my/38498/2/38498-Synthesis%20of%20SiO2%20Nanostructures%20Using%20Sol-Gel%20Method_SCOPUS.pdf
http://irep.iium.edu.my/38498/4/38498-new.pdf