Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith

Response surface methodology (RSM) was applied to optimize the variables affecting the Supercritical carbon dioxide (SC–CO2) extraction of non-polar compounds from Zingiber zerumbet using the Box-Behnken design (BBD). Dependent variables were the percentage of the chemical components in the ginger...

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Main Authors: Nik Ab Rahman, Nik Norulaini, Omar, Anuar, A. K. M., Omar, F. M. Alkarkhi, Abbas, Setianto, Wahyu, Mohd Omar, Fatehah, Ferdosh, Sahena, Sarker, Md. Zaidul Islam
Format: Article
Language:English
Published: Elsevier Inc. 2009
Subjects:
Online Access:http://irep.iium.edu.my/24846/
http://irep.iium.edu.my/24846/1/Food_Chem_Zinger.pdf
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author Nik Ab Rahman, Nik Norulaini
Omar, Anuar
A. K. M., Omar
F. M. Alkarkhi, Abbas
Setianto, Wahyu
Mohd Omar, Fatehah
Ferdosh, Sahena
Sarker, Md. Zaidul Islam
author_facet Nik Ab Rahman, Nik Norulaini
Omar, Anuar
A. K. M., Omar
F. M. Alkarkhi, Abbas
Setianto, Wahyu
Mohd Omar, Fatehah
Ferdosh, Sahena
Sarker, Md. Zaidul Islam
author_sort Nik Ab Rahman, Nik Norulaini
building IIUM Repository
collection Online Access
description Response surface methodology (RSM) was applied to optimize the variables affecting the Supercritical carbon dioxide (SC–CO2) extraction of non-polar compounds from Zingiber zerumbet using the Box-Behnken design (BBD). Dependent variables were the percentage of the chemical components in the ginger vis a vis a-caryophyllene (y1), camphene (y2), and zerumbone (2,6,10-cycloundecatrien-1-one, 2,6,9,9-tetramethyl-) (y3). Pressure was the most significant parameter affecting the amount of each compound extracted. When temperature was kept constant and pressure was increased, all of the dependent variables increased concomitantly. Since pressure and temperature are two of the major influential factors in the extraction using SC–CO2, any combination of these two parameters could be selected to ascertain the optimum combination for a particular compound in the extract. Extraction at 30 �C and 55 MPa with total amount of 30 g of CO2 used was found to maximize all the responses.
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spelling iium-248462015-12-31T04:00:51Z http://irep.iium.edu.my/24846/ Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith Nik Ab Rahman, Nik Norulaini Omar, Anuar A. K. M., Omar F. M. Alkarkhi, Abbas Setianto, Wahyu Mohd Omar, Fatehah Ferdosh, Sahena Sarker, Md. Zaidul Islam QD Chemistry Response surface methodology (RSM) was applied to optimize the variables affecting the Supercritical carbon dioxide (SC–CO2) extraction of non-polar compounds from Zingiber zerumbet using the Box-Behnken design (BBD). Dependent variables were the percentage of the chemical components in the ginger vis a vis a-caryophyllene (y1), camphene (y2), and zerumbone (2,6,10-cycloundecatrien-1-one, 2,6,9,9-tetramethyl-) (y3). Pressure was the most significant parameter affecting the amount of each compound extracted. When temperature was kept constant and pressure was increased, all of the dependent variables increased concomitantly. Since pressure and temperature are two of the major influential factors in the extraction using SC–CO2, any combination of these two parameters could be selected to ascertain the optimum combination for a particular compound in the extract. Extraction at 30 �C and 55 MPa with total amount of 30 g of CO2 used was found to maximize all the responses. Elsevier Inc. 2009 Article PeerReviewed application/pdf en http://irep.iium.edu.my/24846/1/Food_Chem_Zinger.pdf Nik Ab Rahman, Nik Norulaini and Omar, Anuar and A. K. M., Omar and F. M. Alkarkhi, Abbas and Setianto, Wahyu and Mohd Omar, Fatehah and Ferdosh, Sahena and Sarker, Md. Zaidul Islam (2009) Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith. Food Chemistry, 114 (2). pp. 702-705. ISSN 03088146 http://dx.doi.org/10.1016/j.foodchem.2008.09.075 doi:10.1016/j.foodchem.2008.09.075
spellingShingle QD Chemistry
Nik Ab Rahman, Nik Norulaini
Omar, Anuar
A. K. M., Omar
F. M. Alkarkhi, Abbas
Setianto, Wahyu
Mohd Omar, Fatehah
Ferdosh, Sahena
Sarker, Md. Zaidul Islam
Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith
title Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith
title_full Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith
title_fullStr Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith
title_full_unstemmed Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith
title_short Optimization of SC–CO2 extraction of zerumbone from Zingiber zerumbet (L) Smith
title_sort optimization of sc–co2 extraction of zerumbone from zingiber zerumbet (l) smith
topic QD Chemistry
url http://irep.iium.edu.my/24846/
http://irep.iium.edu.my/24846/
http://irep.iium.edu.my/24846/
http://irep.iium.edu.my/24846/1/Food_Chem_Zinger.pdf