Manganese doping on biphasic calcium phosphate ceramics for machanical improvement

SUMMARY Manganese doped biphasic calcium phosphate powders have been synthesized via sol-gel method. The powders are of nanosize and high crystallinity. Dense pure BCP and Mn-doped BCP ceramics were fabricated via uniaxial pressing using the sol-gel derived powders. The compacted discs were si...

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Main Author: Sopyan, Iis
Format: Article
Language:English
Published: Malaysian Medical Associations 2010
Subjects:
Online Access:http://irep.iium.edu.my/20023/
http://irep.iium.edu.my/20023/1/Mangenese_doping_on_biphasic_calsium.pdf
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author Sopyan, Iis
author_facet Sopyan, Iis
author_sort Sopyan, Iis
building IIUM Repository
collection Online Access
description SUMMARY Manganese doped biphasic calcium phosphate powders have been synthesized via sol-gel method. The powders are of nanosize and high crystallinity. Dense pure BCP and Mn-doped BCP ceramics were fabricated via uniaxial pressing using the sol-gel derived powders. The compacted discs were sintered in air atmosphere with temperatures ranging from 1000 ºC to 1400 ºC. The presence of manganese improves the densification in the BCP mixture as the relative density increased with Mn doping and also sintering temperature. Considerable grain growth has been observed at 1300 ºC for Mn-doped BCP samples compared to the pure BCP. Furthermore, 15 mol% Mn showed the maximum hardness value of 6.66 GPa at 1400 ºC compared to pure BCP of only 2.89 GPa. Similarly, the Mn-doped BCP has superior fracture toughness where it attained maximum values of 1.05 MPam1/2 at 1400 ºC compared to 0.72 MPam1/2 at 1300 ºC of pure BCP.
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spelling iium-200232012-02-18T08:35:47Z http://irep.iium.edu.my/20023/ Manganese doping on biphasic calcium phosphate ceramics for machanical improvement Sopyan, Iis TJ Mechanical engineering and machinery SUMMARY Manganese doped biphasic calcium phosphate powders have been synthesized via sol-gel method. The powders are of nanosize and high crystallinity. Dense pure BCP and Mn-doped BCP ceramics were fabricated via uniaxial pressing using the sol-gel derived powders. The compacted discs were sintered in air atmosphere with temperatures ranging from 1000 ºC to 1400 ºC. The presence of manganese improves the densification in the BCP mixture as the relative density increased with Mn doping and also sintering temperature. Considerable grain growth has been observed at 1300 ºC for Mn-doped BCP samples compared to the pure BCP. Furthermore, 15 mol% Mn showed the maximum hardness value of 6.66 GPa at 1400 ºC compared to pure BCP of only 2.89 GPa. Similarly, the Mn-doped BCP has superior fracture toughness where it attained maximum values of 1.05 MPam1/2 at 1400 ºC compared to 0.72 MPam1/2 at 1300 ºC of pure BCP. Malaysian Medical Associations 2010-10 Article PeerReviewed application/pdf en http://irep.iium.edu.my/20023/1/Mangenese_doping_on_biphasic_calsium.pdf Sopyan, Iis (2010) Manganese doping on biphasic calcium phosphate ceramics for machanical improvement. Medical Journal of Malaysia, 65. pp. 14-16. ISSN 0300-5283 http://www.e-mjm.org/2010/Sup_tissue_engineering_part1.pdf#nameddest=te9
spellingShingle TJ Mechanical engineering and machinery
Sopyan, Iis
Manganese doping on biphasic calcium phosphate ceramics for machanical improvement
title Manganese doping on biphasic calcium phosphate ceramics for machanical improvement
title_full Manganese doping on biphasic calcium phosphate ceramics for machanical improvement
title_fullStr Manganese doping on biphasic calcium phosphate ceramics for machanical improvement
title_full_unstemmed Manganese doping on biphasic calcium phosphate ceramics for machanical improvement
title_short Manganese doping on biphasic calcium phosphate ceramics for machanical improvement
title_sort manganese doping on biphasic calcium phosphate ceramics for machanical improvement
topic TJ Mechanical engineering and machinery
url http://irep.iium.edu.my/20023/
http://irep.iium.edu.my/20023/
http://irep.iium.edu.my/20023/1/Mangenese_doping_on_biphasic_calsium.pdf