SEM study of debonding /pull-out features & FTIR analysis of bonding in fly ash- epoxy particulate composites

This research utilises as received coal power fly ash (FA) as a value-added component added to epoxy resin for making a superior matrix for fibre reinforced composites in load-bearing applications. The epoxy resin used in this project was DGEBA cured by cycloaliphatic polyamine at 120 Co for 2 hou...

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Main Authors: Ibraheem1, Shahad, Standard, Owen, Pramod, Koshy, Devasahayam, Sheila, Bandyopadhyay, Sri
Format: Journal Article
Language:English
Published: 2016
Online Access:https://www.erpublications.com/our-journals-dtl-pdf.php?pid=1&id=166&start=20&pagesize=10
http://hdl.handle.net/20.500.11937/92709
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author Ibraheem1, Shahad
Standard, Owen
Pramod, Koshy
Devasahayam, Sheila
Bandyopadhyay, Sri
author_facet Ibraheem1, Shahad
Standard, Owen
Pramod, Koshy
Devasahayam, Sheila
Bandyopadhyay, Sri
author_sort Ibraheem1, Shahad
building Curtin Institutional Repository
collection Online Access
description This research utilises as received coal power fly ash (FA) as a value-added component added to epoxy resin for making a superior matrix for fibre reinforced composites in load-bearing applications. The epoxy resin used in this project was DGEBA cured by cycloaliphatic polyamine at 120 Co for 2 hours. A fly ash with particle size ranging between 2 – 20 micron was added to the epoxy in 0, 10, 20, 30, 40 & 50 wt% proportions. Scanning Electron Microscopy (SEM) of tensile fracture surfaces of the composites using ASTM D638 tensile samples provide significant evidence of Fly Ash debonding and pull-out from the epoxy matrix indicating good mechanical bonding between FA and epoxy matrix. Fourier transform infrared spectroscopy (FTIR) of pure epoxy, pure fly ash and selective composites (20 and40 wt % FA-epoxy composites) shows distinct evidence of fly ash functional groups’ interaction with the epoxy matrix. Some selected SIMS (secondary ion mass spectrometry) results are presented for the 20wt % fly ash /epoxy composites.
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institution Curtin University Malaysia
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language English
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publishDate 2016
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spelling curtin-20.500.11937-927092023-07-24T04:09:17Z SEM study of debonding /pull-out features & FTIR analysis of bonding in fly ash- epoxy particulate composites Ibraheem1, Shahad Standard, Owen Pramod, Koshy Devasahayam, Sheila Bandyopadhyay, Sri This research utilises as received coal power fly ash (FA) as a value-added component added to epoxy resin for making a superior matrix for fibre reinforced composites in load-bearing applications. The epoxy resin used in this project was DGEBA cured by cycloaliphatic polyamine at 120 Co for 2 hours. A fly ash with particle size ranging between 2 – 20 micron was added to the epoxy in 0, 10, 20, 30, 40 & 50 wt% proportions. Scanning Electron Microscopy (SEM) of tensile fracture surfaces of the composites using ASTM D638 tensile samples provide significant evidence of Fly Ash debonding and pull-out from the epoxy matrix indicating good mechanical bonding between FA and epoxy matrix. Fourier transform infrared spectroscopy (FTIR) of pure epoxy, pure fly ash and selective composites (20 and40 wt % FA-epoxy composites) shows distinct evidence of fly ash functional groups’ interaction with the epoxy matrix. Some selected SIMS (secondary ion mass spectrometry) results are presented for the 20wt % fly ash /epoxy composites. 2016 Journal Article http://hdl.handle.net/20.500.11937/92709 English https://www.erpublications.com/our-journals-dtl-pdf.php?pid=1&id=166&start=20&pagesize=10 http://creativecommons.org/licenses/by/4.0/ fulltext
spellingShingle Ibraheem1, Shahad
Standard, Owen
Pramod, Koshy
Devasahayam, Sheila
Bandyopadhyay, Sri
SEM study of debonding /pull-out features & FTIR analysis of bonding in fly ash- epoxy particulate composites
title SEM study of debonding /pull-out features & FTIR analysis of bonding in fly ash- epoxy particulate composites
title_full SEM study of debonding /pull-out features & FTIR analysis of bonding in fly ash- epoxy particulate composites
title_fullStr SEM study of debonding /pull-out features & FTIR analysis of bonding in fly ash- epoxy particulate composites
title_full_unstemmed SEM study of debonding /pull-out features & FTIR analysis of bonding in fly ash- epoxy particulate composites
title_short SEM study of debonding /pull-out features & FTIR analysis of bonding in fly ash- epoxy particulate composites
title_sort sem study of debonding /pull-out features & ftir analysis of bonding in fly ash- epoxy particulate composites
url https://www.erpublications.com/our-journals-dtl-pdf.php?pid=1&id=166&start=20&pagesize=10
http://hdl.handle.net/20.500.11937/92709