Molecular Dynamics in Ag2B12H12 Studied by Nuclear Magnetic Resonance

We present a molecular dynamics study of the low-temperature polymorph of silver closo-borate α-Ag2B12H12, which is a promising ionic conductor. By means of 1H and 11B nuclear magnetic resonance spectroscopy, we identified two dynamic processes in the system that involve the movements of B12H122- ca...

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Main Authors: Gradisěk, A., Jørgensen, M., Paskevicius, Mark, Hansen, B.R.S., Jensen, T.R.
Format: Journal Article
Language:English
Published: AMER CHEMICAL SOC 2021
Subjects:
Online Access:http://purl.org/au-research/grants/arc/FT160100303
http://hdl.handle.net/20.500.11937/90584
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author Gradisěk, A.
Jørgensen, M.
Paskevicius, Mark
Hansen, B.R.S.
Jensen, T.R.
author_facet Gradisěk, A.
Jørgensen, M.
Paskevicius, Mark
Hansen, B.R.S.
Jensen, T.R.
author_sort Gradisěk, A.
building Curtin Institutional Repository
collection Online Access
description We present a molecular dynamics study of the low-temperature polymorph of silver closo-borate α-Ag2B12H12, which is a promising ionic conductor. By means of 1H and 11B nuclear magnetic resonance spectroscopy, we identified two dynamic processes in the system that involve the movements of B12H122- cages: fast rotations with an activation energy of 308 meV and tumbling of the cages at lower temperatures with an activation energy of 67 meV. Fast rotations are known to facilitate the diffusion of Ag+ ions (the activation energy of 482 meV for ion jumps was determined from solid-state ionic conductivity measurements) while the tumbling motions are likely made possible by either impurities or local disorder, allowing for easier reorientations of the boron cages.
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spelling curtin-20.500.11937-905842023-03-24T05:14:45Z Molecular Dynamics in Ag2B12H12 Studied by Nuclear Magnetic Resonance Gradisěk, A. Jørgensen, M. Paskevicius, Mark Hansen, B.R.S. Jensen, T.R. Science & Technology Physical Sciences Technology Chemistry, Physical Nanoscience & Nanotechnology Materials Science, Multidisciplinary Chemistry Science & Technology - Other Topics Materials Science SODIUM SUPERIONIC CONDUCTION REORIENTATIONAL DYNAMICS ANION REORIENTATIONS IONIC-CONDUCTIVITY SOLID ELECTROLYTES LITHIUM SALTS NA MOTION We present a molecular dynamics study of the low-temperature polymorph of silver closo-borate α-Ag2B12H12, which is a promising ionic conductor. By means of 1H and 11B nuclear magnetic resonance spectroscopy, we identified two dynamic processes in the system that involve the movements of B12H122- cages: fast rotations with an activation energy of 308 meV and tumbling of the cages at lower temperatures with an activation energy of 67 meV. Fast rotations are known to facilitate the diffusion of Ag+ ions (the activation energy of 482 meV for ion jumps was determined from solid-state ionic conductivity measurements) while the tumbling motions are likely made possible by either impurities or local disorder, allowing for easier reorientations of the boron cages. 2021 Journal Article http://hdl.handle.net/20.500.11937/90584 10.1021/acs.jpcc.1c00528 English http://purl.org/au-research/grants/arc/FT160100303 http://creativecommons.org/licenses/by/4.0/ AMER CHEMICAL SOC fulltext
spellingShingle Science & Technology
Physical Sciences
Technology
Chemistry, Physical
Nanoscience & Nanotechnology
Materials Science, Multidisciplinary
Chemistry
Science & Technology - Other Topics
Materials Science
SODIUM SUPERIONIC CONDUCTION
REORIENTATIONAL DYNAMICS
ANION REORIENTATIONS
IONIC-CONDUCTIVITY
SOLID ELECTROLYTES
LITHIUM
SALTS
NA
MOTION
Gradisěk, A.
Jørgensen, M.
Paskevicius, Mark
Hansen, B.R.S.
Jensen, T.R.
Molecular Dynamics in Ag2B12H12 Studied by Nuclear Magnetic Resonance
title Molecular Dynamics in Ag2B12H12 Studied by Nuclear Magnetic Resonance
title_full Molecular Dynamics in Ag2B12H12 Studied by Nuclear Magnetic Resonance
title_fullStr Molecular Dynamics in Ag2B12H12 Studied by Nuclear Magnetic Resonance
title_full_unstemmed Molecular Dynamics in Ag2B12H12 Studied by Nuclear Magnetic Resonance
title_short Molecular Dynamics in Ag2B12H12 Studied by Nuclear Magnetic Resonance
title_sort molecular dynamics in ag2b12h12 studied by nuclear magnetic resonance
topic Science & Technology
Physical Sciences
Technology
Chemistry, Physical
Nanoscience & Nanotechnology
Materials Science, Multidisciplinary
Chemistry
Science & Technology - Other Topics
Materials Science
SODIUM SUPERIONIC CONDUCTION
REORIENTATIONAL DYNAMICS
ANION REORIENTATIONS
IONIC-CONDUCTIVITY
SOLID ELECTROLYTES
LITHIUM
SALTS
NA
MOTION
url http://purl.org/au-research/grants/arc/FT160100303
http://hdl.handle.net/20.500.11937/90584