The corona of a surface bubble promotes electrochemical reactions

The evolution of gaseous products is a feature common to several electrochemical processes, often resulting in bubbles adhering to the electrode’s surface. Adherent bubbles reduce the electrode active area, and are therefore generally treated as electrochemically inert entities. Here, we show that t...

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Main Authors: Vogel, Yan, Evans, Cameron, Belotti, Mattia, Xu, L., Russell, I.C., Yu, L.J., Fung, A.K.K., Hill, N.S., Darwish, Nadim, Gonçales, V.R., Coote, M.L., Swaminathan Iyer, K., Ciampi, Simone
Format: Journal Article
Language:English
Published: NATURE RESEARCH 2020
Subjects:
Online Access:http://purl.org/au-research/grants/arc/DP190100735
http://hdl.handle.net/20.500.11937/90474
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author Vogel, Yan
Evans, Cameron
Belotti, Mattia
Xu, L.
Russell, I.C.
Yu, L.J.
Fung, A.K.K.
Hill, N.S.
Darwish, Nadim
Gonçales, V.R.
Coote, M.L.
Swaminathan Iyer, K.
Ciampi, Simone
author_facet Vogel, Yan
Evans, Cameron
Belotti, Mattia
Xu, L.
Russell, I.C.
Yu, L.J.
Fung, A.K.K.
Hill, N.S.
Darwish, Nadim
Gonçales, V.R.
Coote, M.L.
Swaminathan Iyer, K.
Ciampi, Simone
author_sort Vogel, Yan
building Curtin Institutional Repository
collection Online Access
description The evolution of gaseous products is a feature common to several electrochemical processes, often resulting in bubbles adhering to the electrode’s surface. Adherent bubbles reduce the electrode active area, and are therefore generally treated as electrochemically inert entities. Here, we show that this general assumption does not hold for gas bubbles masking anodes operating in water. By means of imaging electrochemiluminescent systems, and by studying the anisotropy of polymer growth around bubbles, we demonstrate that gas cavities adhering to an electrode surface initiate the oxidation of water-soluble species more effectively than electrode areas free of bubbles. The corona of a bubble accumulates hydroxide anions, unbalanced by cations, a phenomenon which causes the oxidation of hydroxide ions to hydroxyl radicals to occur at potentials at least 0.7 V below redox tabled values. The downhill shift of the hydroxide oxidation at the corona of the bubble is likely to be a general mechanism involved in the initiation of heterogeneous electrochemical reactions in water, and could be harnessed in chemical synthesis.
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spelling curtin-20.500.11937-904742023-03-16T06:20:13Z The corona of a surface bubble promotes electrochemical reactions Vogel, Yan Evans, Cameron Belotti, Mattia Xu, L. Russell, I.C. Yu, L.J. Fung, A.K.K. Hill, N.S. Darwish, Nadim Gonçales, V.R. Coote, M.L. Swaminathan Iyer, K. Ciampi, Simone Science & Technology Multidisciplinary Sciences Science & Technology - Other Topics BASIS-SETS HYDROGEN CHEMILUMINESCENCE ENERGY ELECTROLYSIS INTERFACE EVOLUTION LUMINOL MODEL The evolution of gaseous products is a feature common to several electrochemical processes, often resulting in bubbles adhering to the electrode’s surface. Adherent bubbles reduce the electrode active area, and are therefore generally treated as electrochemically inert entities. Here, we show that this general assumption does not hold for gas bubbles masking anodes operating in water. By means of imaging electrochemiluminescent systems, and by studying the anisotropy of polymer growth around bubbles, we demonstrate that gas cavities adhering to an electrode surface initiate the oxidation of water-soluble species more effectively than electrode areas free of bubbles. The corona of a bubble accumulates hydroxide anions, unbalanced by cations, a phenomenon which causes the oxidation of hydroxide ions to hydroxyl radicals to occur at potentials at least 0.7 V below redox tabled values. The downhill shift of the hydroxide oxidation at the corona of the bubble is likely to be a general mechanism involved in the initiation of heterogeneous electrochemical reactions in water, and could be harnessed in chemical synthesis. 2020 Journal Article http://hdl.handle.net/20.500.11937/90474 10.1038/s41467-020-20186-0 English http://purl.org/au-research/grants/arc/DP190100735 http://purl.org/au-research/grants/arc/FT190100148 http://creativecommons.org/licenses/by/4.0/ NATURE RESEARCH fulltext
spellingShingle Science & Technology
Multidisciplinary Sciences
Science & Technology - Other Topics
BASIS-SETS
HYDROGEN
CHEMILUMINESCENCE
ENERGY
ELECTROLYSIS
INTERFACE
EVOLUTION
LUMINOL
MODEL
Vogel, Yan
Evans, Cameron
Belotti, Mattia
Xu, L.
Russell, I.C.
Yu, L.J.
Fung, A.K.K.
Hill, N.S.
Darwish, Nadim
Gonçales, V.R.
Coote, M.L.
Swaminathan Iyer, K.
Ciampi, Simone
The corona of a surface bubble promotes electrochemical reactions
title The corona of a surface bubble promotes electrochemical reactions
title_full The corona of a surface bubble promotes electrochemical reactions
title_fullStr The corona of a surface bubble promotes electrochemical reactions
title_full_unstemmed The corona of a surface bubble promotes electrochemical reactions
title_short The corona of a surface bubble promotes electrochemical reactions
title_sort corona of a surface bubble promotes electrochemical reactions
topic Science & Technology
Multidisciplinary Sciences
Science & Technology - Other Topics
BASIS-SETS
HYDROGEN
CHEMILUMINESCENCE
ENERGY
ELECTROLYSIS
INTERFACE
EVOLUTION
LUMINOL
MODEL
url http://purl.org/au-research/grants/arc/DP190100735
http://purl.org/au-research/grants/arc/DP190100735
http://hdl.handle.net/20.500.11937/90474