Electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid

Controlled formation of cocrystals is an important objective in drug development. Here, cocrystallisation of caffeine and 1-hydroxy-2-naphthoic acid was investigated at the interface between two immiscible electrolyte solutions under chemical polarisation. In this way, selective cocrystallisation wa...

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Main Authors: Kaliszczak, M., Durand, P., Wenger, E., Dossot, M., Jones, Franca, Arrigan, Damien, Herzog, G.
Format: Journal Article
Language:English
Published: ROYAL SOC CHEMISTRY 2022
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/89592
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author Kaliszczak, M.
Durand, P.
Wenger, E.
Dossot, M.
Jones, Franca
Arrigan, Damien
Herzog, G.
author_facet Kaliszczak, M.
Durand, P.
Wenger, E.
Dossot, M.
Jones, Franca
Arrigan, Damien
Herzog, G.
author_sort Kaliszczak, M.
building Curtin Institutional Repository
collection Online Access
description Controlled formation of cocrystals is an important objective in drug development. Here, cocrystallisation of caffeine and 1-hydroxy-2-naphthoic acid was investigated at the interface between two immiscible electrolyte solutions under chemical polarisation. In this way, selective cocrystallisation was achieved, as verified by X-ray diffraction and Raman spectroscopy. Positive interfacial potentials favoured the formation of one polymorphic form of caffeine:1-hydroxy-2-naphthoic acid cocrystal. This approach to electrochemically controlled cocrystallisation opens up new possibilities for drug development.
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institution Curtin University Malaysia
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language English
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publishDate 2022
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spelling curtin-20.500.11937-895922023-01-19T07:26:36Z Electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid Kaliszczak, M. Durand, P. Wenger, E. Dossot, M. Jones, Franca Arrigan, Damien Herzog, G. Science & Technology Physical Sciences Chemistry, Multidisciplinary Crystallography Chemistry PHARMACEUTICAL COCRYSTALS CAFFEINE INTERFACE CRYSTALLIZATION ION Controlled formation of cocrystals is an important objective in drug development. Here, cocrystallisation of caffeine and 1-hydroxy-2-naphthoic acid was investigated at the interface between two immiscible electrolyte solutions under chemical polarisation. In this way, selective cocrystallisation was achieved, as verified by X-ray diffraction and Raman spectroscopy. Positive interfacial potentials favoured the formation of one polymorphic form of caffeine:1-hydroxy-2-naphthoic acid cocrystal. This approach to electrochemically controlled cocrystallisation opens up new possibilities for drug development. 2022 Journal Article http://hdl.handle.net/20.500.11937/89592 10.1039/d1ce01281a English ROYAL SOC CHEMISTRY fulltext
spellingShingle Science & Technology
Physical Sciences
Chemistry, Multidisciplinary
Crystallography
Chemistry
PHARMACEUTICAL COCRYSTALS
CAFFEINE
INTERFACE
CRYSTALLIZATION
ION
Kaliszczak, M.
Durand, P.
Wenger, E.
Dossot, M.
Jones, Franca
Arrigan, Damien
Herzog, G.
Electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid
title Electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid
title_full Electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid
title_fullStr Electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid
title_full_unstemmed Electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid
title_short Electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid
title_sort electrochemically controlled cocrystallisation of caffeine:1-hydroxy-2-naphthoic acid
topic Science & Technology
Physical Sciences
Chemistry, Multidisciplinary
Crystallography
Chemistry
PHARMACEUTICAL COCRYSTALS
CAFFEINE
INTERFACE
CRYSTALLIZATION
ION
url http://hdl.handle.net/20.500.11937/89592