Activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of CO2, CH4 and N2

Activated carbon monoliths with hierarchical pore structures were prepared from petroleum tar pitch and powdered coal in a low pressure foaming process with potassium hydroxide activation. The effects of coal to tar pitch ratio and of the amount of potassium hydroxide on the stability of tar pitch d...

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Main Authors: Arami-Niya, Arash, Rufford, T.E., Zhu, Z.
Format: Journal Article
Language:English
Published: PERGAMON-ELSEVIER SCIENCE LTD 2016
Subjects:
Online Access:http://purl.org/au-research/grants/arc/DE140100569
http://hdl.handle.net/20.500.11937/78461
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author Arami-Niya, Arash
Rufford, T.E.
Zhu, Z.
author_facet Arami-Niya, Arash
Rufford, T.E.
Zhu, Z.
author_sort Arami-Niya, Arash
building Curtin Institutional Repository
collection Online Access
description Activated carbon monoliths with hierarchical pore structures were prepared from petroleum tar pitch and powdered coal in a low pressure foaming process with potassium hydroxide activation. The effects of coal to tar pitch ratio and of the amount of potassium hydroxide on the stability of tar pitch during the foaming process, the product's density and the micropore structure were studied. The carbon monolith prepared with adding 50%wt coal to pitch retained the shape of the cylindrical foam mould. This carbon monolith featured an open-cell structure with cell widths of around 2 μm and a well-developed microporosity that presented a BET specific surface area of 1044 m2 g-1. The apparent density of this structure was 0.42 g cm-3. The adsorption capacity of the carbon monolith for CO2, N2 and CH4 were evaluated by the volumetric sorption method at pressures up to 130 kPa and by a gravimetric sorption method for pressures up to 4500 kPa. At 298 K and pressures close to 3500 kPa the adsorption capacities of the carbon monolith prepared with 50%wt coal to pitch were 7.398 mol kg-1 CO2, 5.049 mol kg-1 CH4 and 3.516 mol kg-1 N2. The sorption results suggest these activated carbon monoliths have potential as monolithic adsorbents for gas separation or storage applications.
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spelling curtin-20.500.11937-784612021-02-16T03:55:56Z Activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of CO2, CH4 and N2 Arami-Niya, Arash Rufford, T.E. Zhu, Z. Science & Technology Physical Sciences Technology Chemistry, Physical Materials Science, Multidisciplinary Chemistry Materials Science FOAM CATALYST SUPPORTS METHANE GAS EQUILIBRIA NITROGEN MIXTURES KINETICS Activated carbon monoliths with hierarchical pore structures were prepared from petroleum tar pitch and powdered coal in a low pressure foaming process with potassium hydroxide activation. The effects of coal to tar pitch ratio and of the amount of potassium hydroxide on the stability of tar pitch during the foaming process, the product's density and the micropore structure were studied. The carbon monolith prepared with adding 50%wt coal to pitch retained the shape of the cylindrical foam mould. This carbon monolith featured an open-cell structure with cell widths of around 2 μm and a well-developed microporosity that presented a BET specific surface area of 1044 m2 g-1. The apparent density of this structure was 0.42 g cm-3. The adsorption capacity of the carbon monolith for CO2, N2 and CH4 were evaluated by the volumetric sorption method at pressures up to 130 kPa and by a gravimetric sorption method for pressures up to 4500 kPa. At 298 K and pressures close to 3500 kPa the adsorption capacities of the carbon monolith prepared with 50%wt coal to pitch were 7.398 mol kg-1 CO2, 5.049 mol kg-1 CH4 and 3.516 mol kg-1 N2. The sorption results suggest these activated carbon monoliths have potential as monolithic adsorbents for gas separation or storage applications. 2016 Journal Article http://hdl.handle.net/20.500.11937/78461 10.1016/j.carbon.2016.02.098 English http://purl.org/au-research/grants/arc/DE140100569 http://purl.org/au-research/grants/arc/FT120100720 PERGAMON-ELSEVIER SCIENCE LTD fulltext
spellingShingle Science & Technology
Physical Sciences
Technology
Chemistry, Physical
Materials Science, Multidisciplinary
Chemistry
Materials Science
FOAM CATALYST SUPPORTS
METHANE
GAS
EQUILIBRIA
NITROGEN
MIXTURES
KINETICS
Arami-Niya, Arash
Rufford, T.E.
Zhu, Z.
Activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of CO2, CH4 and N2
title Activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of CO2, CH4 and N2
title_full Activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of CO2, CH4 and N2
title_fullStr Activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of CO2, CH4 and N2
title_full_unstemmed Activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of CO2, CH4 and N2
title_short Activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of CO2, CH4 and N2
title_sort activated carbon monoliths with hierarchical pore structure from tar pitch and coal powder for the adsorption of co2, ch4 and n2
topic Science & Technology
Physical Sciences
Technology
Chemistry, Physical
Materials Science, Multidisciplinary
Chemistry
Materials Science
FOAM CATALYST SUPPORTS
METHANE
GAS
EQUILIBRIA
NITROGEN
MIXTURES
KINETICS
url http://purl.org/au-research/grants/arc/DE140100569
http://purl.org/au-research/grants/arc/DE140100569
http://hdl.handle.net/20.500.11937/78461