Macroscopic electrostatic effects in ATR-FTIR spectra of modern and archeological bones

© 2018 Walter de Gruyter GmbH, Berlin/Boston 2018. Bones mostly consist of composite materials based on almost equivalent volume fractions of mineral (apatite) and organic (collagen) components. Accordingly, their infrared spectroscopic properties should reflect this composite nature. In this letter...

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Main Authors: Aufort, Julie, Lebon, M., Gallet, X., Ségalen, L., Gervais, C., Brouder, C., Balan, E.
Format: Journal Article
Language:English
Published: MINERALOGICAL SOC AMER 2018
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/76339
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author Aufort, Julie
Lebon, M.
Gallet, X.
Ségalen, L.
Gervais, C.
Brouder, C.
Balan, E.
author_facet Aufort, Julie
Lebon, M.
Gallet, X.
Ségalen, L.
Gervais, C.
Brouder, C.
Balan, E.
author_sort Aufort, Julie
building Curtin Institutional Repository
collection Online Access
description © 2018 Walter de Gruyter GmbH, Berlin/Boston 2018. Bones mostly consist of composite materials based on almost equivalent volume fractions of mineral (apatite) and organic (collagen) components. Accordingly, their infrared spectroscopic properties should reflect this composite nature. In this letter, we show by theory and experiment that the variability of the strong phosphate bands in the ATR-FTIR spectra of a series of modern and archeological bone samples can be related to electrostatic interactions affecting apatite particles and depending on the bone collagen content. Key parameters controlling the shape of these bands are the mineral volume fraction and the dielectric constant of the embedding matrix. The magnitude of these effects is larger than the one related to microscopic changes of the apatite structure. Consequently, the interplay of microscopic and macroscopic parameters should be considered when using FTIR spectroscopy to monitor the preservation state of bioapatite during diagenetic and fossilization processes, especially during the degradation of the organic fraction of bone.
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spelling curtin-20.500.11937-763392019-09-25T07:34:22Z Macroscopic electrostatic effects in ATR-FTIR spectra of modern and archeological bones Aufort, Julie Lebon, M. Gallet, X. Ségalen, L. Gervais, C. Brouder, C. Balan, E. Science & Technology Physical Sciences Geochemistry & Geophysics Mineralogy ATR-FTIR spectroscopy bone fossilization electrostatic properties Biomaterials-Mineralogy Meets Medicine INFRARED-SPECTROSCOPY DIAGENESIS BIOMINERALS CRYSTALS APATITE ENAMEL © 2018 Walter de Gruyter GmbH, Berlin/Boston 2018. Bones mostly consist of composite materials based on almost equivalent volume fractions of mineral (apatite) and organic (collagen) components. Accordingly, their infrared spectroscopic properties should reflect this composite nature. In this letter, we show by theory and experiment that the variability of the strong phosphate bands in the ATR-FTIR spectra of a series of modern and archeological bone samples can be related to electrostatic interactions affecting apatite particles and depending on the bone collagen content. Key parameters controlling the shape of these bands are the mineral volume fraction and the dielectric constant of the embedding matrix. The magnitude of these effects is larger than the one related to microscopic changes of the apatite structure. Consequently, the interplay of microscopic and macroscopic parameters should be considered when using FTIR spectroscopy to monitor the preservation state of bioapatite during diagenetic and fossilization processes, especially during the degradation of the organic fraction of bone. 2018 Journal Article http://hdl.handle.net/20.500.11937/76339 10.2138/am-2018-6320CCBYNCND English https://creativecommons.org/licenses/by-nc-nd/3.0/ MINERALOGICAL SOC AMER fulltext
spellingShingle Science & Technology
Physical Sciences
Geochemistry & Geophysics
Mineralogy
ATR-FTIR spectroscopy
bone
fossilization
electrostatic properties
Biomaterials-Mineralogy Meets Medicine
INFRARED-SPECTROSCOPY
DIAGENESIS
BIOMINERALS
CRYSTALS
APATITE
ENAMEL
Aufort, Julie
Lebon, M.
Gallet, X.
Ségalen, L.
Gervais, C.
Brouder, C.
Balan, E.
Macroscopic electrostatic effects in ATR-FTIR spectra of modern and archeological bones
title Macroscopic electrostatic effects in ATR-FTIR spectra of modern and archeological bones
title_full Macroscopic electrostatic effects in ATR-FTIR spectra of modern and archeological bones
title_fullStr Macroscopic electrostatic effects in ATR-FTIR spectra of modern and archeological bones
title_full_unstemmed Macroscopic electrostatic effects in ATR-FTIR spectra of modern and archeological bones
title_short Macroscopic electrostatic effects in ATR-FTIR spectra of modern and archeological bones
title_sort macroscopic electrostatic effects in atr-ftir spectra of modern and archeological bones
topic Science & Technology
Physical Sciences
Geochemistry & Geophysics
Mineralogy
ATR-FTIR spectroscopy
bone
fossilization
electrostatic properties
Biomaterials-Mineralogy Meets Medicine
INFRARED-SPECTROSCOPY
DIAGENESIS
BIOMINERALS
CRYSTALS
APATITE
ENAMEL
url http://hdl.handle.net/20.500.11937/76339