Photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand

© 2019 The Royal Society of Chemistry. A conjugated β-triketone, tris(2-naphthoyl)methane (tnmH), has been synthesized and successfully utilized as an antenna moiety for sensitization of the trivalent lanthanoids Eu 3+ , Sm 3+ , Yb 3+ and Nd 3+ , in an isomorphous series of mononuclear complexes fo...

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Main Authors: Abad Galán, L., Wada, S., Cameron, L., Sobolev, A., Hasegawa, Y., Zysman-Colman, E., Ogden, Mark, Massi, Massimiliano
Format: Journal Article
Language:English
Published: ROYAL SOC CHEMISTRY 2019
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/75548
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author Abad Galán, L.
Wada, S.
Cameron, L.
Sobolev, A.
Hasegawa, Y.
Zysman-Colman, E.
Ogden, Mark
Massi, Massimiliano
author_facet Abad Galán, L.
Wada, S.
Cameron, L.
Sobolev, A.
Hasegawa, Y.
Zysman-Colman, E.
Ogden, Mark
Massi, Massimiliano
author_sort Abad Galán, L.
building Curtin Institutional Repository
collection Online Access
description © 2019 The Royal Society of Chemistry. A conjugated β-triketone, tris(2-naphthoyl)methane (tnmH), has been synthesized and successfully utilized as an antenna moiety for sensitization of the trivalent lanthanoids Eu 3+ , Sm 3+ , Yb 3+ and Nd 3+ , in an isomorphous series of mononuclear complexes formulated as [Ln(tnm) 3 (DMSO) 2 ] (Ln 3+ = Nd 3+ , Sm 3+ , Eu 3+ , Gd 3+ and Yb 3+ ). The photophysical properties of the materials were characterized as comprehensively as possible, with overall quantum yields, intrinsic quantum yields based on calculated radiative decays, and sensitization efficiencies reported. This investigation improves understanding of the sensitization processes occurring in the near-infrared (NIR) region, where quantitative data are currently scarce. In fact, the [Yb(tnm) 3 (DMSO) 2 ] and its deuterated analogue, [Yb(tnm) 3 (d 6 -DMSO) 2 ], present high values of overall quantum yield of 4% and 6%, respectively, which makes them useful and readily accessible references for future investigation of NIR-emitting systems.
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spelling curtin-20.500.11937-755482020-02-24T07:37:34Z Photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand Abad Galán, L. Wada, S. Cameron, L. Sobolev, A. Hasegawa, Y. Zysman-Colman, E. Ogden, Mark Massi, Massimiliano Science & Technology Physical Sciences Chemistry, Inorganic & Nuclear Chemistry BETA-DIKETONATE COMPLEXES RADIATIVE LIFETIME NIR-LUMINESCENCE EMISSION EXCITATION ENERGY ND FLUORINATION NEODYMIUM LN © 2019 The Royal Society of Chemistry. A conjugated β-triketone, tris(2-naphthoyl)methane (tnmH), has been synthesized and successfully utilized as an antenna moiety for sensitization of the trivalent lanthanoids Eu 3+ , Sm 3+ , Yb 3+ and Nd 3+ , in an isomorphous series of mononuclear complexes formulated as [Ln(tnm) 3 (DMSO) 2 ] (Ln 3+ = Nd 3+ , Sm 3+ , Eu 3+ , Gd 3+ and Yb 3+ ). The photophysical properties of the materials were characterized as comprehensively as possible, with overall quantum yields, intrinsic quantum yields based on calculated radiative decays, and sensitization efficiencies reported. This investigation improves understanding of the sensitization processes occurring in the near-infrared (NIR) region, where quantitative data are currently scarce. In fact, the [Yb(tnm) 3 (DMSO) 2 ] and its deuterated analogue, [Yb(tnm) 3 (d 6 -DMSO) 2 ], present high values of overall quantum yield of 4% and 6%, respectively, which makes them useful and readily accessible references for future investigation of NIR-emitting systems. 2019 Journal Article http://hdl.handle.net/20.500.11937/75548 10.1039/c8dt04749a English ROYAL SOC CHEMISTRY fulltext
spellingShingle Science & Technology
Physical Sciences
Chemistry, Inorganic & Nuclear
Chemistry
BETA-DIKETONATE COMPLEXES
RADIATIVE LIFETIME
NIR-LUMINESCENCE
EMISSION
EXCITATION
ENERGY
ND
FLUORINATION
NEODYMIUM
LN
Abad Galán, L.
Wada, S.
Cameron, L.
Sobolev, A.
Hasegawa, Y.
Zysman-Colman, E.
Ogden, Mark
Massi, Massimiliano
Photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand
title Photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand
title_full Photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand
title_fullStr Photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand
title_full_unstemmed Photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand
title_short Photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand
title_sort photophysical investigation of near infrared emitting lanthanoid complexes incorporating tris(2-naphthoyl)methane as a new antenna ligand
topic Science & Technology
Physical Sciences
Chemistry, Inorganic & Nuclear
Chemistry
BETA-DIKETONATE COMPLEXES
RADIATIVE LIFETIME
NIR-LUMINESCENCE
EMISSION
EXCITATION
ENERGY
ND
FLUORINATION
NEODYMIUM
LN
url http://hdl.handle.net/20.500.11937/75548