Insights into the wettability alteration of CO2-assisted EOR in carbonate reservoirs

Wettability of oil-brine-carbonate system is an important petro-physical parameter, which governs subsurface multiphase flow and residual oil saturation. CO2-assisted EOR techniques have been identified as cost-effective and environmentally friendly means to unlock remaining hydrocarbon resources fr...

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Main Authors: Chen, Y., Sari, A., Xie, Q., Saeedi, Ali
Format: Journal Article
Published: Elsevier 2019
Online Access:http://hdl.handle.net/20.500.11937/74295
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author Chen, Y.
Sari, A.
Xie, Q.
Saeedi, Ali
author_facet Chen, Y.
Sari, A.
Xie, Q.
Saeedi, Ali
author_sort Chen, Y.
building Curtin Institutional Repository
collection Online Access
description Wettability of oil-brine-carbonate system is an important petro-physical parameter, which governs subsurface multiphase flow and residual oil saturation. CO2-assisted EOR techniques have been identified as cost-effective and environmentally friendly means to unlock remaining hydrocarbon resources from carbonate reservoirs. While wettability alteration appears to be one of the main mechanisms during CO2-assisted EOR implementation, the controlling factor(s) of wettability alteration at molecular level remains unclear. We thus hypothesized that excess of H+ as a result of water uptake of CO2 increases hydrophilicity of oil-brine-carbonate systems. More specifically, the surface charge properties will be alterated to more positive due to the increase of H+ in the brine. To test this hypothesis, we measured oil contact angles on calcite surfaces in the presence of non-carbonated brine, carbonated brine, and acidic brine (pH = 3). We also performed surface complexation modelling to examine how the surface chemistry controls over wettability of oil/brine/carbonate system using PHREEQC. Our contact angle results show that both carbonated brine and acidic brine gave a contact angle of 24° and 22° respectively, while non-carbonated brine gives a contact angle of 73° in 1 mol/L CaCl2 brines. Same trend was also observed in synthesized formation brine, showing that non-carbonated formation brine yielded a contact angle of 69° while both acidic formation brine and carbonated formation brine gave a contact angle of 37°. Experimental results show that both carbonated brine, and acidic brine significantly decreased contact angle compared to non-carbonated brine, suggesting a strong water-wet system. Surface complexation modelling shows that for both carbonated water and acidic water, >CaOH2+ dominates surface charges at calcite surfaces, and –NH+ governs surface charges on oil surfaces. Together, these two processes increase repulsive forces thus hydrophilicity. Our study sheds light on the significant influence of excess H+ due to water uptake of CO2 on oil-brine-carbonate system wettability thus enhancing hydrocarbon recovery in carbonate reservoirs.
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institution Curtin University Malaysia
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spelling curtin-20.500.11937-742952019-05-02T02:20:25Z Insights into the wettability alteration of CO2-assisted EOR in carbonate reservoirs Chen, Y. Sari, A. Xie, Q. Saeedi, Ali Wettability of oil-brine-carbonate system is an important petro-physical parameter, which governs subsurface multiphase flow and residual oil saturation. CO2-assisted EOR techniques have been identified as cost-effective and environmentally friendly means to unlock remaining hydrocarbon resources from carbonate reservoirs. While wettability alteration appears to be one of the main mechanisms during CO2-assisted EOR implementation, the controlling factor(s) of wettability alteration at molecular level remains unclear. We thus hypothesized that excess of H+ as a result of water uptake of CO2 increases hydrophilicity of oil-brine-carbonate systems. More specifically, the surface charge properties will be alterated to more positive due to the increase of H+ in the brine. To test this hypothesis, we measured oil contact angles on calcite surfaces in the presence of non-carbonated brine, carbonated brine, and acidic brine (pH = 3). We also performed surface complexation modelling to examine how the surface chemistry controls over wettability of oil/brine/carbonate system using PHREEQC. Our contact angle results show that both carbonated brine and acidic brine gave a contact angle of 24° and 22° respectively, while non-carbonated brine gives a contact angle of 73° in 1 mol/L CaCl2 brines. Same trend was also observed in synthesized formation brine, showing that non-carbonated formation brine yielded a contact angle of 69° while both acidic formation brine and carbonated formation brine gave a contact angle of 37°. Experimental results show that both carbonated brine, and acidic brine significantly decreased contact angle compared to non-carbonated brine, suggesting a strong water-wet system. Surface complexation modelling shows that for both carbonated water and acidic water, >CaOH2+ dominates surface charges at calcite surfaces, and –NH+ governs surface charges on oil surfaces. Together, these two processes increase repulsive forces thus hydrophilicity. Our study sheds light on the significant influence of excess H+ due to water uptake of CO2 on oil-brine-carbonate system wettability thus enhancing hydrocarbon recovery in carbonate reservoirs. 2019 Journal Article http://hdl.handle.net/20.500.11937/74295 10.1016/j.molliq.2019.01.112 Elsevier restricted
spellingShingle Chen, Y.
Sari, A.
Xie, Q.
Saeedi, Ali
Insights into the wettability alteration of CO2-assisted EOR in carbonate reservoirs
title Insights into the wettability alteration of CO2-assisted EOR in carbonate reservoirs
title_full Insights into the wettability alteration of CO2-assisted EOR in carbonate reservoirs
title_fullStr Insights into the wettability alteration of CO2-assisted EOR in carbonate reservoirs
title_full_unstemmed Insights into the wettability alteration of CO2-assisted EOR in carbonate reservoirs
title_short Insights into the wettability alteration of CO2-assisted EOR in carbonate reservoirs
title_sort insights into the wettability alteration of co2-assisted eor in carbonate reservoirs
url http://hdl.handle.net/20.500.11937/74295