Removal of trace organic chemicals in wastewater effluent by UV/H2O2 and UV/PDS

© 2018 Elsevier Ltd In this study, we comparatively investigated the degradation of 12 trace organic chemicals (TOrCs) during UV/H2O2 and UV/peroxydisulfate (PDS) processes. Second-order rate constants for the reactions of iopromide, phenytoin, caffeine, benzotriazole, and primidone with sulfate rad...

Full description

Bibliographic Details
Main Authors: Nihemaiti, M., Miklos, D., Hübner, U., Linden, K., Drewes, J., Croue, Jean-Philippe
Format: Journal Article
Published: IWA Publishing 2018
Online Access:http://hdl.handle.net/20.500.11937/73251
_version_ 1848762965153546240
author Nihemaiti, M.
Miklos, D.
Hübner, U.
Linden, K.
Drewes, J.
Croue, Jean-Philippe
author_facet Nihemaiti, M.
Miklos, D.
Hübner, U.
Linden, K.
Drewes, J.
Croue, Jean-Philippe
author_sort Nihemaiti, M.
building Curtin Institutional Repository
collection Online Access
description © 2018 Elsevier Ltd In this study, we comparatively investigated the degradation of 12 trace organic chemicals (TOrCs) during UV/H2O2 and UV/peroxydisulfate (PDS) processes. Second-order rate constants for the reactions of iopromide, phenytoin, caffeine, benzotriazole, and primidone with sulfate radical (SO4•-) were determined for the first time. Experiments were conducted in buffered pure water and wastewater effluent with spiked TOrCs. UV/PDS degraded all TOrCs more efficiently than UV/H2O2 in buffered pure water due to the higher yield of SO4•- than that of hydroxyl radical (•OH) at the same initial molar dose of PDS and H2O2, respectively. UV/PDS showed higher selectivity toward TOrCs removal than UV/H2O2 in wastewater effluent. Compounds with electron-rich moieties, such as diclofenac, venlafaxine, and metoprolol, were eliminated faster in UV/PDS whereas UV/H2O2 was more efficient in degrading compounds with lower reactivity to SO4•-. The fluence-based rate constants (kobs-UV/H2O2) of TOrCs in wastewater effluent linearly increased as a function of initial H2O2 dose during UV/H2O2, possibly due to the constant scavenging impact of the wastewater matrix on •OH. However, exponential increase of kobs-UV/PDS with increasing PDS dose was observed for most compounds during UV/PDS, suggesting the decreasing scavenging effect of the water matrix (electron-rich site of effluent organic matter (EfOM)) after initial depletion of SO4•- at low PDS dose. Fulvic and humic-like fluorophores appeared to be more persistent during UV/H2O2 compared to aromatic protein and soluble microbial product-like fluorophores. In contrast, UV/PDS efficiently degraded all identified fluorophores and showed less selectivity toward the fluorescent EfOM components. Removal pattern of TOrCs during pilot-scale UV/PDS was consistent with lab-scale experiments, however, overall removal rates were lower due to the presence of higher concentration of EfOM and nitrite.
first_indexed 2025-11-14T10:55:56Z
format Journal Article
id curtin-20.500.11937-73251
institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T10:55:56Z
publishDate 2018
publisher IWA Publishing
recordtype eprints
repository_type Digital Repository
spelling curtin-20.500.11937-732512023-08-02T06:39:13Z Removal of trace organic chemicals in wastewater effluent by UV/H2O2 and UV/PDS Nihemaiti, M. Miklos, D. Hübner, U. Linden, K. Drewes, J. Croue, Jean-Philippe © 2018 Elsevier Ltd In this study, we comparatively investigated the degradation of 12 trace organic chemicals (TOrCs) during UV/H2O2 and UV/peroxydisulfate (PDS) processes. Second-order rate constants for the reactions of iopromide, phenytoin, caffeine, benzotriazole, and primidone with sulfate radical (SO4•-) were determined for the first time. Experiments were conducted in buffered pure water and wastewater effluent with spiked TOrCs. UV/PDS degraded all TOrCs more efficiently than UV/H2O2 in buffered pure water due to the higher yield of SO4•- than that of hydroxyl radical (•OH) at the same initial molar dose of PDS and H2O2, respectively. UV/PDS showed higher selectivity toward TOrCs removal than UV/H2O2 in wastewater effluent. Compounds with electron-rich moieties, such as diclofenac, venlafaxine, and metoprolol, were eliminated faster in UV/PDS whereas UV/H2O2 was more efficient in degrading compounds with lower reactivity to SO4•-. The fluence-based rate constants (kobs-UV/H2O2) of TOrCs in wastewater effluent linearly increased as a function of initial H2O2 dose during UV/H2O2, possibly due to the constant scavenging impact of the wastewater matrix on •OH. However, exponential increase of kobs-UV/PDS with increasing PDS dose was observed for most compounds during UV/PDS, suggesting the decreasing scavenging effect of the water matrix (electron-rich site of effluent organic matter (EfOM)) after initial depletion of SO4•- at low PDS dose. Fulvic and humic-like fluorophores appeared to be more persistent during UV/H2O2 compared to aromatic protein and soluble microbial product-like fluorophores. In contrast, UV/PDS efficiently degraded all identified fluorophores and showed less selectivity toward the fluorescent EfOM components. Removal pattern of TOrCs during pilot-scale UV/PDS was consistent with lab-scale experiments, however, overall removal rates were lower due to the presence of higher concentration of EfOM and nitrite. 2018 Journal Article http://hdl.handle.net/20.500.11937/73251 10.1016/j.watres.2018.08.052 IWA Publishing restricted
spellingShingle Nihemaiti, M.
Miklos, D.
Hübner, U.
Linden, K.
Drewes, J.
Croue, Jean-Philippe
Removal of trace organic chemicals in wastewater effluent by UV/H2O2 and UV/PDS
title Removal of trace organic chemicals in wastewater effluent by UV/H2O2 and UV/PDS
title_full Removal of trace organic chemicals in wastewater effluent by UV/H2O2 and UV/PDS
title_fullStr Removal of trace organic chemicals in wastewater effluent by UV/H2O2 and UV/PDS
title_full_unstemmed Removal of trace organic chemicals in wastewater effluent by UV/H2O2 and UV/PDS
title_short Removal of trace organic chemicals in wastewater effluent by UV/H2O2 and UV/PDS
title_sort removal of trace organic chemicals in wastewater effluent by uv/h2o2 and uv/pds
url http://hdl.handle.net/20.500.11937/73251