Core-Shell Structured PtRuCo x Nanoparticles on Carbon Nanotubes as Highly Active and Durable Electrocatalysts for Direct Methanol Fuel Cells

Ternary alloy PtRuCox nanoparticles (NPs) with Co-rich core and PtRu skinned shell on carbon nanotubes (CNTs) have been successfully synthesized as electrocatalysts for methanol oxidation reaction (MOR) of direct methanol fuel cells (DMFCs) via a successive dealloying and annealing treatment of PtRu...

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Main Authors: Cheng, Yi, Shen, P., Saunders, M., Jiang, San Ping
Format: Journal Article
Published: Elsevier Ltd 2015
Online Access:http://purl.org/au-research/grants/arc/DP150102044
http://hdl.handle.net/20.500.11937/7316
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author Cheng, Yi
Shen, P.
Saunders, M.
Jiang, San Ping
author_facet Cheng, Yi
Shen, P.
Saunders, M.
Jiang, San Ping
author_sort Cheng, Yi
building Curtin Institutional Repository
collection Online Access
description Ternary alloy PtRuCox nanoparticles (NPs) with Co-rich core and PtRu skinned shell on carbon nanotubes (CNTs) have been successfully synthesized as electrocatalysts for methanol oxidation reaction (MOR) of direct methanol fuel cells (DMFCs) via a successive dealloying and annealing treatment of PtRuCo alloy particles. The best results were obtained on dealloyed PtRuCox NPs annealed at 450 °C in argon with x = 0.48, characterizing by a ~1 nm thick Co-free PtRu shell. The core–shell structured PtRuCox catalysts exhibit a high activity for MOR, 400 A g−1pt measured at 0.40 V (vs Ag/AgCl), almost 4 times higher than 104 A g−1Pt for the reaction on the PtRuCo alloy before deallaying and annealing treatment. The core–shell structured PtRuCox NPs also show excellent structural stability; maintaining 74% of the activity after 1000 cycle between −0.2 to 1.0 V (vs. Ag/AgCl), significantly higher than 49% for PtRuCo and 25% for the conventional PtRu/C catalysts. The results demonstrate that the successive dealloying and annealing treatment is very effective to synthesize core–shell structured PtRuCox ternary alloy electrocatalysts with high activity and durability for DMFCs.
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spelling curtin-20.500.11937-73162022-10-12T07:13:34Z Core-Shell Structured PtRuCo x Nanoparticles on Carbon Nanotubes as Highly Active and Durable Electrocatalysts for Direct Methanol Fuel Cells Cheng, Yi Shen, P. Saunders, M. Jiang, San Ping Ternary alloy PtRuCox nanoparticles (NPs) with Co-rich core and PtRu skinned shell on carbon nanotubes (CNTs) have been successfully synthesized as electrocatalysts for methanol oxidation reaction (MOR) of direct methanol fuel cells (DMFCs) via a successive dealloying and annealing treatment of PtRuCo alloy particles. The best results were obtained on dealloyed PtRuCox NPs annealed at 450 °C in argon with x = 0.48, characterizing by a ~1 nm thick Co-free PtRu shell. The core–shell structured PtRuCox catalysts exhibit a high activity for MOR, 400 A g−1pt measured at 0.40 V (vs Ag/AgCl), almost 4 times higher than 104 A g−1Pt for the reaction on the PtRuCo alloy before deallaying and annealing treatment. The core–shell structured PtRuCox NPs also show excellent structural stability; maintaining 74% of the activity after 1000 cycle between −0.2 to 1.0 V (vs. Ag/AgCl), significantly higher than 49% for PtRuCo and 25% for the conventional PtRu/C catalysts. The results demonstrate that the successive dealloying and annealing treatment is very effective to synthesize core–shell structured PtRuCox ternary alloy electrocatalysts with high activity and durability for DMFCs. 2015 Journal Article http://hdl.handle.net/20.500.11937/7316 10.1016/j.electacta.2015.01.137 http://purl.org/au-research/grants/arc/DP150102044 Elsevier Ltd restricted
spellingShingle Cheng, Yi
Shen, P.
Saunders, M.
Jiang, San Ping
Core-Shell Structured PtRuCo x Nanoparticles on Carbon Nanotubes as Highly Active and Durable Electrocatalysts for Direct Methanol Fuel Cells
title Core-Shell Structured PtRuCo x Nanoparticles on Carbon Nanotubes as Highly Active and Durable Electrocatalysts for Direct Methanol Fuel Cells
title_full Core-Shell Structured PtRuCo x Nanoparticles on Carbon Nanotubes as Highly Active and Durable Electrocatalysts for Direct Methanol Fuel Cells
title_fullStr Core-Shell Structured PtRuCo x Nanoparticles on Carbon Nanotubes as Highly Active and Durable Electrocatalysts for Direct Methanol Fuel Cells
title_full_unstemmed Core-Shell Structured PtRuCo x Nanoparticles on Carbon Nanotubes as Highly Active and Durable Electrocatalysts for Direct Methanol Fuel Cells
title_short Core-Shell Structured PtRuCo x Nanoparticles on Carbon Nanotubes as Highly Active and Durable Electrocatalysts for Direct Methanol Fuel Cells
title_sort core-shell structured ptruco x nanoparticles on carbon nanotubes as highly active and durable electrocatalysts for direct methanol fuel cells
url http://purl.org/au-research/grants/arc/DP150102044
http://hdl.handle.net/20.500.11937/7316