Sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification

© 2015 Elsevier B.V. Abstract First, styrene was grafted onto the surface of halloysite nanotubes (HNTs) via distillation-precipitation polymerization and the above modified HNTs were sulfonated by concentrated sulfuric acid to prepare highly crosslinked HNTs-SO<inf>3</inf&g...

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Main Authors: Wang, Y., Zhu, J., Dong, G., Zhang, Y., Guo, N., Liu, Jian
Format: Journal Article
Published: Pergamon Press 2015
Online Access:http://hdl.handle.net/20.500.11937/72896
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author Wang, Y.
Zhu, J.
Dong, G.
Zhang, Y.
Guo, N.
Liu, Jian
author_facet Wang, Y.
Zhu, J.
Dong, G.
Zhang, Y.
Guo, N.
Liu, Jian
author_sort Wang, Y.
building Curtin Institutional Repository
collection Online Access
description © 2015 Elsevier B.V. Abstract First, styrene was grafted onto the surface of halloysite nanotubes (HNTs) via distillation-precipitation polymerization and the above modified HNTs were sulfonated by concentrated sulfuric acid to prepare highly crosslinked HNTs-SO<inf>3</inf>H. Then, HNTs-SO<inf>3</inf>H was used as a novel inorganic filler to fabricate polyethersulfone (PES) nanofiltration hybrid membrane via classical phase inversion method. The morphology and separation performance of the above membranes were characterized by scan electron microscope (SEM), transmission electron microscope (TEM), water contact angle and mechanical measurement. The results revealed that water flux of the hybrid membranes was improved greatly after adding HNTs-SO<inf>3</inf>H. Especially, the hybrid membranes showed higher rejections for Reactive Black 5 (above 90%) and Reactive Red 49 (80-90%). Meanwhile, the rejection for salts declined to under 10% and the order for different salt solutions was Na<inf>2</inf>SO<inf>4</inf> > MgSO<inf>4</inf> > MgCl<inf>2</inf> > NaCl, indicating the characteristics of negatively charged nanofiltration membranes.
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institution Curtin University Malaysia
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publishDate 2015
publisher Pergamon Press
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spelling curtin-20.500.11937-728962018-12-14T01:02:56Z Sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification Wang, Y. Zhu, J. Dong, G. Zhang, Y. Guo, N. Liu, Jian © 2015 Elsevier B.V. Abstract First, styrene was grafted onto the surface of halloysite nanotubes (HNTs) via distillation-precipitation polymerization and the above modified HNTs were sulfonated by concentrated sulfuric acid to prepare highly crosslinked HNTs-SO<inf>3</inf>H. Then, HNTs-SO<inf>3</inf>H was used as a novel inorganic filler to fabricate polyethersulfone (PES) nanofiltration hybrid membrane via classical phase inversion method. The morphology and separation performance of the above membranes were characterized by scan electron microscope (SEM), transmission electron microscope (TEM), water contact angle and mechanical measurement. The results revealed that water flux of the hybrid membranes was improved greatly after adding HNTs-SO<inf>3</inf>H. Especially, the hybrid membranes showed higher rejections for Reactive Black 5 (above 90%) and Reactive Red 49 (80-90%). Meanwhile, the rejection for salts declined to under 10% and the order for different salt solutions was Na<inf>2</inf>SO<inf>4</inf> > MgSO<inf>4</inf> > MgCl<inf>2</inf> > NaCl, indicating the characteristics of negatively charged nanofiltration membranes. 2015 Journal Article http://hdl.handle.net/20.500.11937/72896 10.1016/j.seppur.2015.07.005 Pergamon Press restricted
spellingShingle Wang, Y.
Zhu, J.
Dong, G.
Zhang, Y.
Guo, N.
Liu, Jian
Sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification
title Sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification
title_full Sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification
title_fullStr Sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification
title_full_unstemmed Sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification
title_short Sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification
title_sort sulfonated halloysite nanotubes/polyethersulfone nanocomposite membrane for efficient dye purification
url http://hdl.handle.net/20.500.11937/72896