A Universal Strategy to Design Superior Water-Splitting Electrocatalysts Based on Fast In Situ Reconstruction of Amorphous Nanofilm Precursors

© 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim The development of efficient bifunctional electrodes with extraordinary mass activity and robust stability is an eternal yet challenging goal for the water-splitting process. Surface reconstruction during electrocatalysis can form fresh-composi...

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Main Authors: Chen, G., Hu, Z., Zhu, Y., Gu, B., Zhong, Y., Lin, H., Chen, C., Zhou, W., Shao, Zongping
Format: Journal Article
Published: Wiley - V C H Verlag GmbH & Co. KGaA 2018
Online Access:http://hdl.handle.net/20.500.11937/71649
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author Chen, G.
Hu, Z.
Zhu, Y.
Gu, B.
Zhong, Y.
Lin, H.
Chen, C.
Zhou, W.
Shao, Zongping
author_facet Chen, G.
Hu, Z.
Zhu, Y.
Gu, B.
Zhong, Y.
Lin, H.
Chen, C.
Zhou, W.
Shao, Zongping
author_sort Chen, G.
building Curtin Institutional Repository
collection Online Access
description © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim The development of efficient bifunctional electrodes with extraordinary mass activity and robust stability is an eternal yet challenging goal for the water-splitting process. Surface reconstruction during electrocatalysis can form fresh-composition electrocatalysts with unusual amorphous phases in situ, which are more active but difficult to prepare by conventional methods. Here, a facile strategy based on fast reconstruction of amorphous nanofilm precursors is proposed for exploring precious-metal-free catalysts with good electronic conductivity, ultrahigh activity, and robust stability. As a proof of concept, an amorphous SrCo0.85Fe0.1P0.05O3-d (SCFP) nanofilm precursor with weak chemical bonds deposited onto a conductive nickel foam (NF) substrate (SCFP-NF) is synthesized by utilizing a high-energy argon plasma to break the strong chemical bonds in a crystalline SCFP target. The quickly reconstructed SCFP-NF bifunctional catalysts show ultrahigh mass activity of up to 1000 mA mg-1 at an overpotential of 550 mV and extremely long operational stability of up to 650 h at 10 mA cm-2, significantly overperforming state-of-the-art precious-metal catalysts. Such a strategy is further demonstrated to be a universal method, which can be applied to accelerate the reconstruction of other material systems to obtain various efficient electrocatalysts.
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publisher Wiley - V C H Verlag GmbH & Co. KGaA
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spelling curtin-20.500.11937-716492018-12-13T09:32:28Z A Universal Strategy to Design Superior Water-Splitting Electrocatalysts Based on Fast In Situ Reconstruction of Amorphous Nanofilm Precursors Chen, G. Hu, Z. Zhu, Y. Gu, B. Zhong, Y. Lin, H. Chen, C. Zhou, W. Shao, Zongping © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim The development of efficient bifunctional electrodes with extraordinary mass activity and robust stability is an eternal yet challenging goal for the water-splitting process. Surface reconstruction during electrocatalysis can form fresh-composition electrocatalysts with unusual amorphous phases in situ, which are more active but difficult to prepare by conventional methods. Here, a facile strategy based on fast reconstruction of amorphous nanofilm precursors is proposed for exploring precious-metal-free catalysts with good electronic conductivity, ultrahigh activity, and robust stability. As a proof of concept, an amorphous SrCo0.85Fe0.1P0.05O3-d (SCFP) nanofilm precursor with weak chemical bonds deposited onto a conductive nickel foam (NF) substrate (SCFP-NF) is synthesized by utilizing a high-energy argon plasma to break the strong chemical bonds in a crystalline SCFP target. The quickly reconstructed SCFP-NF bifunctional catalysts show ultrahigh mass activity of up to 1000 mA mg-1 at an overpotential of 550 mV and extremely long operational stability of up to 650 h at 10 mA cm-2, significantly overperforming state-of-the-art precious-metal catalysts. Such a strategy is further demonstrated to be a universal method, which can be applied to accelerate the reconstruction of other material systems to obtain various efficient electrocatalysts. 2018 Journal Article http://hdl.handle.net/20.500.11937/71649 10.1002/adma.201804333 Wiley - V C H Verlag GmbH & Co. KGaA restricted
spellingShingle Chen, G.
Hu, Z.
Zhu, Y.
Gu, B.
Zhong, Y.
Lin, H.
Chen, C.
Zhou, W.
Shao, Zongping
A Universal Strategy to Design Superior Water-Splitting Electrocatalysts Based on Fast In Situ Reconstruction of Amorphous Nanofilm Precursors
title A Universal Strategy to Design Superior Water-Splitting Electrocatalysts Based on Fast In Situ Reconstruction of Amorphous Nanofilm Precursors
title_full A Universal Strategy to Design Superior Water-Splitting Electrocatalysts Based on Fast In Situ Reconstruction of Amorphous Nanofilm Precursors
title_fullStr A Universal Strategy to Design Superior Water-Splitting Electrocatalysts Based on Fast In Situ Reconstruction of Amorphous Nanofilm Precursors
title_full_unstemmed A Universal Strategy to Design Superior Water-Splitting Electrocatalysts Based on Fast In Situ Reconstruction of Amorphous Nanofilm Precursors
title_short A Universal Strategy to Design Superior Water-Splitting Electrocatalysts Based on Fast In Situ Reconstruction of Amorphous Nanofilm Precursors
title_sort universal strategy to design superior water-splitting electrocatalysts based on fast in situ reconstruction of amorphous nanofilm precursors
url http://hdl.handle.net/20.500.11937/71649