Synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of CdS

© 2018 Elsevier B.V. Nitrogen and sulfur co-doped reduced graphene oxide (NS-rGO) was synthesized using a facile low temperature calcination method, which was then used as support and cocatalyst for the anchor of CdS. The obtained CdS/NS-rGO nanocomposites exhibit ultra-high photocatalytic activity...

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Main Authors: Han, W., Chen, L., Song, W., Wang, Shaobin, Fan, X., Li, Y., Zhang, F., Zhang, G., Peng, W.
Format: Journal Article
Published: Elsevier BV 2018
Online Access:http://hdl.handle.net/20.500.11937/68878
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author Han, W.
Chen, L.
Song, W.
Wang, Shaobin
Fan, X.
Li, Y.
Zhang, F.
Zhang, G.
Peng, W.
author_facet Han, W.
Chen, L.
Song, W.
Wang, Shaobin
Fan, X.
Li, Y.
Zhang, F.
Zhang, G.
Peng, W.
author_sort Han, W.
building Curtin Institutional Repository
collection Online Access
description © 2018 Elsevier B.V. Nitrogen and sulfur co-doped reduced graphene oxide (NS-rGO) was synthesized using a facile low temperature calcination method, which was then used as support and cocatalyst for the anchor of CdS. The obtained CdS/NS-rGO nanocomposites exhibit ultra-high photocatalytic activity for hydrogen evolution and 4-nitrophenol (4-NP) reduction under visible light (? = 420 nm). Their activity could also be adjusted by changing the doping amount of S and N, or by changing the ratios between CdS and NS-rGO. The optimum percentage of NS-rGO is 5 wt%, at which CdS/NS-rGO photocatalyst could achieve the highest H2evolution rate of 1701 µmol h–1g–1. Moreover, the reduction from 4-NP to 4-aminophenol (4-AP) could be completed within only 6 min over this optimized composite. NS-rGO here could provide more active sites as well as tune the band gap structure to increase the photo-activity. The density functional theory (DFT) calculations reveal that NS-rGO has a small Gibbs free energy for H* adsorption (?GH), which could increase the utilization efficency of photo-generated electrons for H2generation. NS-rGO is therefore an idea alternate cocatalyst of noble metals for new photocatalysts development.
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spelling curtin-20.500.11937-688782018-06-29T12:35:26Z Synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of CdS Han, W. Chen, L. Song, W. Wang, Shaobin Fan, X. Li, Y. Zhang, F. Zhang, G. Peng, W. © 2018 Elsevier B.V. Nitrogen and sulfur co-doped reduced graphene oxide (NS-rGO) was synthesized using a facile low temperature calcination method, which was then used as support and cocatalyst for the anchor of CdS. The obtained CdS/NS-rGO nanocomposites exhibit ultra-high photocatalytic activity for hydrogen evolution and 4-nitrophenol (4-NP) reduction under visible light (? = 420 nm). Their activity could also be adjusted by changing the doping amount of S and N, or by changing the ratios between CdS and NS-rGO. The optimum percentage of NS-rGO is 5 wt%, at which CdS/NS-rGO photocatalyst could achieve the highest H2evolution rate of 1701 µmol h–1g–1. Moreover, the reduction from 4-NP to 4-aminophenol (4-AP) could be completed within only 6 min over this optimized composite. NS-rGO here could provide more active sites as well as tune the band gap structure to increase the photo-activity. The density functional theory (DFT) calculations reveal that NS-rGO has a small Gibbs free energy for H* adsorption (?GH), which could increase the utilization efficency of photo-generated electrons for H2generation. NS-rGO is therefore an idea alternate cocatalyst of noble metals for new photocatalysts development. 2018 Journal Article http://hdl.handle.net/20.500.11937/68878 10.1016/j.apcatb.2018.05.021 Elsevier BV restricted
spellingShingle Han, W.
Chen, L.
Song, W.
Wang, Shaobin
Fan, X.
Li, Y.
Zhang, F.
Zhang, G.
Peng, W.
Synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of CdS
title Synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of CdS
title_full Synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of CdS
title_fullStr Synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of CdS
title_full_unstemmed Synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of CdS
title_short Synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of CdS
title_sort synthesis of nitrogen and sulfur co-doped reduced graphene oxide as efficient metal-free cocatalyst for the photo-activity enhancement of cds
url http://hdl.handle.net/20.500.11937/68878