Volatile-char interactions: Roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity

© 2018 The Combustion Institute. This study reports the roles of volatiles with distinctly-different chemistry in determining char reactivity and char structure during in situ volatile-char interactions under non-catalytic conditions. Volatiles were generated in situ from polyethylene (PE), double-a...

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Main Authors: Chen, X., Wu, Hongwei
Format: Journal Article
Published: Combustion Institute 2018
Online Access:http://hdl.handle.net/20.500.11937/68665
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author Chen, X.
Wu, Hongwei
author_facet Chen, X.
Wu, Hongwei
author_sort Chen, X.
building Curtin Institutional Repository
collection Online Access
description © 2018 The Combustion Institute. This study reports the roles of volatiles with distinctly-different chemistry in determining char reactivity and char structure during in situ volatile-char interactions under non-catalytic conditions. Volatiles were generated in situ from polyethylene (PE), double-acid washed biosolid (DAWB), polyethylene glycol (PEG) or cellulose and interacted with char prepared from DAWB that is free of catalytically-active inorganic species in a two-stage reactor at 1000 °C. The experimental results show that both H- and O-containing reactive species play different roles during in situ volatile-char interactions. It has been found that char reactivity decreases substantially after in situ volatile-char interactions. Results from Raman analysis of the char after in situ interactions with the PE volatiles show H-containing reactive species substantially enhance the condensation of the aromatic ring systems within the char, thus slightly decreasing the H content in char and also making char carbon structure considerably less reactive. It has also been found that the reactivity of char after in situ volatile-char interactions increases with increasing O/H molar ratio of volatiles. The results indicate that O-containing reactive species in volatiles can react with char to form C. O complex oxides that mitigate the carbon structure from condensing into large aromatic ring systems, thus increasing O and H contents in char and enhancing char reactivity.
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spelling curtin-20.500.11937-686652018-06-29T12:35:14Z Volatile-char interactions: Roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity Chen, X. Wu, Hongwei © 2018 The Combustion Institute. This study reports the roles of volatiles with distinctly-different chemistry in determining char reactivity and char structure during in situ volatile-char interactions under non-catalytic conditions. Volatiles were generated in situ from polyethylene (PE), double-acid washed biosolid (DAWB), polyethylene glycol (PEG) or cellulose and interacted with char prepared from DAWB that is free of catalytically-active inorganic species in a two-stage reactor at 1000 °C. The experimental results show that both H- and O-containing reactive species play different roles during in situ volatile-char interactions. It has been found that char reactivity decreases substantially after in situ volatile-char interactions. Results from Raman analysis of the char after in situ interactions with the PE volatiles show H-containing reactive species substantially enhance the condensation of the aromatic ring systems within the char, thus slightly decreasing the H content in char and also making char carbon structure considerably less reactive. It has also been found that the reactivity of char after in situ volatile-char interactions increases with increasing O/H molar ratio of volatiles. The results indicate that O-containing reactive species in volatiles can react with char to form C. O complex oxides that mitigate the carbon structure from condensing into large aromatic ring systems, thus increasing O and H contents in char and enhancing char reactivity. 2018 Journal Article http://hdl.handle.net/20.500.11937/68665 10.1016/j.proci.2018.05.019 Combustion Institute restricted
spellingShingle Chen, X.
Wu, Hongwei
Volatile-char interactions: Roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity
title Volatile-char interactions: Roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity
title_full Volatile-char interactions: Roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity
title_fullStr Volatile-char interactions: Roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity
title_full_unstemmed Volatile-char interactions: Roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity
title_short Volatile-char interactions: Roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity
title_sort volatile-char interactions: roles of in situ volatiles with distinctly-different chemistry in determining char structure and reactivity
url http://hdl.handle.net/20.500.11937/68665