The electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the VO2+/VO2+ redox couple

Carbon nanotubes (CNTs) have been applied as catalysts in the VO 2 + /VO 2+ redox, whereas the mechanism of CNTs for the redox reaction is still unclear. In this work, the mechanism of the VO 2 + /VO 2+ redox is investigated by comparing the electrocatalytic performance of CNTs with different distri...

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Main Authors: Lv, Z., Zhang, J., Lv, Y., Cheng, Y., Jiang, San Ping, Xiang, Y., Lu, S.
Format: Journal Article
Published: R S C Publications 2018
Online Access:http://hdl.handle.net/20.500.11937/67658
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author Lv, Z.
Zhang, J.
Lv, Y.
Cheng, Y.
Jiang, San Ping
Xiang, Y.
Lu, S.
author_facet Lv, Z.
Zhang, J.
Lv, Y.
Cheng, Y.
Jiang, San Ping
Xiang, Y.
Lu, S.
author_sort Lv, Z.
building Curtin Institutional Repository
collection Online Access
description Carbon nanotubes (CNTs) have been applied as catalysts in the VO 2 + /VO 2+ redox, whereas the mechanism of CNTs for the redox reaction is still unclear. In this work, the mechanism of the VO 2 + /VO 2+ redox is investigated by comparing the electrocatalytic performance of CNTs with different distributions. For different CNTs, the peak current density of the VO 2 + /VO 2+ redox increases with increasing content of oxygen-functional groups on the surface of CNTs, especially the carboxyl group which is proved as active sites for the redox reaction. Moreover, the reversibility of the VO 2 + /VO 2+ redox decreases with increasing defects of CNTs, as the defects affect the charge transfer of the catalytic reaction. Nevertheless, when a multi-walled CNT sample is oxidized to achieve a high content of oxygen functional groups and defects, the peak current density of the redox reaction increases from 38.5 mA mg -1 to 45.4 mA mg -1 whilst the peak potential separation (ΔE p ) also increases from 0.176 V to 0.209 V. Overall, a balance between the oxygen functional groups and the defects of CNTs affects the peak current and the reversibility for the VO 2 + /VO 2+ redox.
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spelling curtin-20.500.11937-676582018-09-26T06:09:14Z The electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the VO2+/VO2+ redox couple Lv, Z. Zhang, J. Lv, Y. Cheng, Y. Jiang, San Ping Xiang, Y. Lu, S. Carbon nanotubes (CNTs) have been applied as catalysts in the VO 2 + /VO 2+ redox, whereas the mechanism of CNTs for the redox reaction is still unclear. In this work, the mechanism of the VO 2 + /VO 2+ redox is investigated by comparing the electrocatalytic performance of CNTs with different distributions. For different CNTs, the peak current density of the VO 2 + /VO 2+ redox increases with increasing content of oxygen-functional groups on the surface of CNTs, especially the carboxyl group which is proved as active sites for the redox reaction. Moreover, the reversibility of the VO 2 + /VO 2+ redox decreases with increasing defects of CNTs, as the defects affect the charge transfer of the catalytic reaction. Nevertheless, when a multi-walled CNT sample is oxidized to achieve a high content of oxygen functional groups and defects, the peak current density of the redox reaction increases from 38.5 mA mg -1 to 45.4 mA mg -1 whilst the peak potential separation (ΔE p ) also increases from 0.176 V to 0.209 V. Overall, a balance between the oxygen functional groups and the defects of CNTs affects the peak current and the reversibility for the VO 2 + /VO 2+ redox. 2018 Journal Article http://hdl.handle.net/20.500.11937/67658 10.1039/c7cp08683k R S C Publications restricted
spellingShingle Lv, Z.
Zhang, J.
Lv, Y.
Cheng, Y.
Jiang, San Ping
Xiang, Y.
Lu, S.
The electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the VO2+/VO2+ redox couple
title The electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the VO2+/VO2+ redox couple
title_full The electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the VO2+/VO2+ redox couple
title_fullStr The electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the VO2+/VO2+ redox couple
title_full_unstemmed The electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the VO2+/VO2+ redox couple
title_short The electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the VO2+/VO2+ redox couple
title_sort electrocatalytic characterization and mechanism of carbon nanotubes with different numbers of walls for the vo2+/vo2+ redox couple
url http://hdl.handle.net/20.500.11937/67658