Worm-like FeS2/TiO2 Nanotubes for Photoelectrocatalytic Reduction of CO2 to Methanol under Visible Light

Photoelectrocatalytic (PEC) reduction of CO 2 to hydrocarbons provides a great technique for CO 2 utilization, renewable energy transformation, and storage. Iron disulfide (FeS 2 ), as an earth-abundant and nontoxic semiconductor, has narrow band gap energy, high photovoltaic conversion efficiency,...

Full description

Bibliographic Details
Main Authors: Han, E., Hu, F., Zhang, S., Luan, B., Li, P., Sun, Hongqi, Wang, Shaobin
Format: Journal Article
Published: American Chemical Society 2018
Online Access:http://hdl.handle.net/20.500.11937/67164
_version_ 1848761492771438592
author Han, E.
Hu, F.
Zhang, S.
Luan, B.
Li, P.
Sun, Hongqi
Wang, Shaobin
author_facet Han, E.
Hu, F.
Zhang, S.
Luan, B.
Li, P.
Sun, Hongqi
Wang, Shaobin
author_sort Han, E.
building Curtin Institutional Repository
collection Online Access
description Photoelectrocatalytic (PEC) reduction of CO 2 to hydrocarbons provides a great technique for CO 2 utilization, renewable energy transformation, and storage. Iron disulfide (FeS 2 ), as an earth-abundant and nontoxic semiconductor, has narrow band gap energy, high photovoltaic conversion efficiency, and light absorption, making it very promising as a photoelectrode in a PEC cell. Herein, novel worm-like FeS 2 /TiO 2 nanotubes (NTs) was prepared by introducing FeS 2 on TiO 2 NTs and exhibited excellent PEC performance for CO 2 reduction to methanol. X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), and high-resolution transmission electron microscopy (HRTEM) showed that worm-like FeS 2 was densely packed on the TiO 2 NT substrate. By introduction of FeS 2 on TiO 2 NTs, the visible light absorption was improved greatly and the energy band gap energy was narrowed to 1.70 eV, which significantly enhanced the photocatalytic performance under visible light. Furthermore, the resistance was reduced with increasing electrocatalytic ability. The major product of PEC reduction of CO 2 was methanol, reaching 91.7 μmol h -1 L -1 .
first_indexed 2025-11-14T10:32:32Z
format Journal Article
id curtin-20.500.11937-67164
institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T10:32:32Z
publishDate 2018
publisher American Chemical Society
recordtype eprints
repository_type Digital Repository
spelling curtin-20.500.11937-671642018-08-29T05:41:04Z Worm-like FeS2/TiO2 Nanotubes for Photoelectrocatalytic Reduction of CO2 to Methanol under Visible Light Han, E. Hu, F. Zhang, S. Luan, B. Li, P. Sun, Hongqi Wang, Shaobin Photoelectrocatalytic (PEC) reduction of CO 2 to hydrocarbons provides a great technique for CO 2 utilization, renewable energy transformation, and storage. Iron disulfide (FeS 2 ), as an earth-abundant and nontoxic semiconductor, has narrow band gap energy, high photovoltaic conversion efficiency, and light absorption, making it very promising as a photoelectrode in a PEC cell. Herein, novel worm-like FeS 2 /TiO 2 nanotubes (NTs) was prepared by introducing FeS 2 on TiO 2 NTs and exhibited excellent PEC performance for CO 2 reduction to methanol. X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), and high-resolution transmission electron microscopy (HRTEM) showed that worm-like FeS 2 was densely packed on the TiO 2 NT substrate. By introduction of FeS 2 on TiO 2 NTs, the visible light absorption was improved greatly and the energy band gap energy was narrowed to 1.70 eV, which significantly enhanced the photocatalytic performance under visible light. Furthermore, the resistance was reduced with increasing electrocatalytic ability. The major product of PEC reduction of CO 2 was methanol, reaching 91.7 μmol h -1 L -1 . 2018 Journal Article http://hdl.handle.net/20.500.11937/67164 10.1021/acs.energyfuels.7b03234 American Chemical Society restricted
spellingShingle Han, E.
Hu, F.
Zhang, S.
Luan, B.
Li, P.
Sun, Hongqi
Wang, Shaobin
Worm-like FeS2/TiO2 Nanotubes for Photoelectrocatalytic Reduction of CO2 to Methanol under Visible Light
title Worm-like FeS2/TiO2 Nanotubes for Photoelectrocatalytic Reduction of CO2 to Methanol under Visible Light
title_full Worm-like FeS2/TiO2 Nanotubes for Photoelectrocatalytic Reduction of CO2 to Methanol under Visible Light
title_fullStr Worm-like FeS2/TiO2 Nanotubes for Photoelectrocatalytic Reduction of CO2 to Methanol under Visible Light
title_full_unstemmed Worm-like FeS2/TiO2 Nanotubes for Photoelectrocatalytic Reduction of CO2 to Methanol under Visible Light
title_short Worm-like FeS2/TiO2 Nanotubes for Photoelectrocatalytic Reduction of CO2 to Methanol under Visible Light
title_sort worm-like fes2/tio2 nanotubes for photoelectrocatalytic reduction of co2 to methanol under visible light
url http://hdl.handle.net/20.500.11937/67164