Atomically Dispersed Transition Metals on Carbon Nanotubes with UltraHigh Loading for Selective Electrochemical Carbon Dioxide Reduction

© 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. Single-atom catalysts (SACs) are the smallest entities for catalytic reactions with projected high atomic efficiency, superior activity, and selectivity; however, practical applications of SACs suffer from a very low metal loading of 1-2 wt%....

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Main Authors: Cheng, Yi, Zhao, S., Johannessen, B., Veder, Jean-Pierre, Saunders, M., Rowles, Matthew, Cheng, M., Liu, C., Chisholm, M., De Marco, Roland, Cheng, H., Yang, S., Jiang, San Ping
Format: Journal Article
Published: Wiley - V C H Verlag GmbH & Co. KGaA 2018
Online Access:http://purl.org/au-research/grants/arc/DP150102025
http://hdl.handle.net/20.500.11937/66522
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author Cheng, Yi
Zhao, S.
Johannessen, B.
Veder, Jean-Pierre
Saunders, M.
Rowles, Matthew
Cheng, M.
Liu, C.
Chisholm, M.
De Marco, Roland
Cheng, H.
Yang, S.
Jiang, San Ping
author_facet Cheng, Yi
Zhao, S.
Johannessen, B.
Veder, Jean-Pierre
Saunders, M.
Rowles, Matthew
Cheng, M.
Liu, C.
Chisholm, M.
De Marco, Roland
Cheng, H.
Yang, S.
Jiang, San Ping
author_sort Cheng, Yi
building Curtin Institutional Repository
collection Online Access
description © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. Single-atom catalysts (SACs) are the smallest entities for catalytic reactions with projected high atomic efficiency, superior activity, and selectivity; however, practical applications of SACs suffer from a very low metal loading of 1-2 wt%. Here, a class of SACs based on atomically dispersed transition metals on nitrogen-doped carbon nanotubes (MSA-N-CNTs, where M = Ni, Co, NiCo, CoFe, and NiPt) is synthesized with an extraordinarily high metal loading, e.g., 20 wt% in the case of NiSA-N-CNTs, using a new multistep pyrolysis process. Among these materials, NiSA-N-CNTs show an excellent selectivity and activity for the electrochemical reduction of CO 2 to CO, achieving a turnover frequency (TOF) of 11.7 s -1 at -0.55 V (vs reversible hydrogen electrode (RHE)), two orders of magnitude higher than Ni nanoparticles supported on CNTs.
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institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T10:30:09Z
publishDate 2018
publisher Wiley - V C H Verlag GmbH & Co. KGaA
recordtype eprints
repository_type Digital Repository
spelling curtin-20.500.11937-665222022-09-06T02:59:15Z Atomically Dispersed Transition Metals on Carbon Nanotubes with UltraHigh Loading for Selective Electrochemical Carbon Dioxide Reduction Cheng, Yi Zhao, S. Johannessen, B. Veder, Jean-Pierre Saunders, M. Rowles, Matthew Cheng, M. Liu, C. Chisholm, M. De Marco, Roland Cheng, H. Yang, S. Jiang, San Ping © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. Single-atom catalysts (SACs) are the smallest entities for catalytic reactions with projected high atomic efficiency, superior activity, and selectivity; however, practical applications of SACs suffer from a very low metal loading of 1-2 wt%. Here, a class of SACs based on atomically dispersed transition metals on nitrogen-doped carbon nanotubes (MSA-N-CNTs, where M = Ni, Co, NiCo, CoFe, and NiPt) is synthesized with an extraordinarily high metal loading, e.g., 20 wt% in the case of NiSA-N-CNTs, using a new multistep pyrolysis process. Among these materials, NiSA-N-CNTs show an excellent selectivity and activity for the electrochemical reduction of CO 2 to CO, achieving a turnover frequency (TOF) of 11.7 s -1 at -0.55 V (vs reversible hydrogen electrode (RHE)), two orders of magnitude higher than Ni nanoparticles supported on CNTs. 2018 Journal Article http://hdl.handle.net/20.500.11937/66522 10.1002/adma.201706287 http://purl.org/au-research/grants/arc/DP150102025 http://purl.org/au-research/grants/arc/DP150102044 http://purl.org/au-research/grants/arc/DP180100568 http://purl.org/au-research/grants/arc/DP180100731 Wiley - V C H Verlag GmbH & Co. KGaA fulltext
spellingShingle Cheng, Yi
Zhao, S.
Johannessen, B.
Veder, Jean-Pierre
Saunders, M.
Rowles, Matthew
Cheng, M.
Liu, C.
Chisholm, M.
De Marco, Roland
Cheng, H.
Yang, S.
Jiang, San Ping
Atomically Dispersed Transition Metals on Carbon Nanotubes with UltraHigh Loading for Selective Electrochemical Carbon Dioxide Reduction
title Atomically Dispersed Transition Metals on Carbon Nanotubes with UltraHigh Loading for Selective Electrochemical Carbon Dioxide Reduction
title_full Atomically Dispersed Transition Metals on Carbon Nanotubes with UltraHigh Loading for Selective Electrochemical Carbon Dioxide Reduction
title_fullStr Atomically Dispersed Transition Metals on Carbon Nanotubes with UltraHigh Loading for Selective Electrochemical Carbon Dioxide Reduction
title_full_unstemmed Atomically Dispersed Transition Metals on Carbon Nanotubes with UltraHigh Loading for Selective Electrochemical Carbon Dioxide Reduction
title_short Atomically Dispersed Transition Metals on Carbon Nanotubes with UltraHigh Loading for Selective Electrochemical Carbon Dioxide Reduction
title_sort atomically dispersed transition metals on carbon nanotubes with ultrahigh loading for selective electrochemical carbon dioxide reduction
url http://purl.org/au-research/grants/arc/DP150102025
http://purl.org/au-research/grants/arc/DP150102025
http://purl.org/au-research/grants/arc/DP150102025
http://purl.org/au-research/grants/arc/DP150102025
http://hdl.handle.net/20.500.11937/66522