Improved biosynthesis of silver nanoparticles using keratinase from Stenotrophomonas maltophilia R13: reaction optimization, structural characterization, and biomedical activity

© 2017 Springer-Verlag GmbH Germany, part of Springer Nature In the present study, keratinase from Stenotrophomonas maltophilia R13 was used for the first time as a reducing agent for the eco-friendly synthesis of AgNPs. The keratinase produced by strain R13 was responsible for the reduction of silv...

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Main Authors: Jang, E., Son, Y., Park, S., Yoo, J., Cho, Y., Jeong, S., Liu, Shaomin, Son, H.
Format: Journal Article
Published: 2017
Online Access:http://hdl.handle.net/20.500.11937/66369
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author Jang, E.
Son, Y.
Park, S.
Yoo, J.
Cho, Y.
Jeong, S.
Liu, Shaomin
Son, H.
author_facet Jang, E.
Son, Y.
Park, S.
Yoo, J.
Cho, Y.
Jeong, S.
Liu, Shaomin
Son, H.
author_sort Jang, E.
building Curtin Institutional Repository
collection Online Access
description © 2017 Springer-Verlag GmbH Germany, part of Springer Nature In the present study, keratinase from Stenotrophomonas maltophilia R13 was used for the first time as a reducing agent for the eco-friendly synthesis of AgNPs. The keratinase produced by strain R13 was responsible for the reduction of silver ions and the subsequent formation of AgNPs. Maximum AgNP synthesis was achieved using 2 mM AgNO 3 at pH 9 and 40 °C. Electron microscopy and dynamic light scattering analysis showed AgNPs were spherical and of average diameter ~ 8.4 nm. X-ray diffraction revealed that AgNPs were crystalline. FTIR indicated AgNPs were stabilized by proteins present in the crude enzyme solution of strain R13. AgNPs exhibited a broad antimicrobial spectrum against several pathogenic microorganisms, and the antimicrobial mechanism appeared to involve structural deformation of cells resulting in membrane leakage and subsequent lysis. AgNPs also displayed 1,1-diphenyl-2-picrylhydrazyl (IC 50 = 0.0112 mg/ml), 2,2'-azinobis-3-ethylbenzothiazoline-6-sulfonate radical scavenging (IC 50 = 0.0243 mg/ml), and anti-collagenase (IC 50 = 23.5 mg/ml) activities.
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institution Curtin University Malaysia
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spelling curtin-20.500.11937-663692018-04-30T02:48:45Z Improved biosynthesis of silver nanoparticles using keratinase from Stenotrophomonas maltophilia R13: reaction optimization, structural characterization, and biomedical activity Jang, E. Son, Y. Park, S. Yoo, J. Cho, Y. Jeong, S. Liu, Shaomin Son, H. © 2017 Springer-Verlag GmbH Germany, part of Springer Nature In the present study, keratinase from Stenotrophomonas maltophilia R13 was used for the first time as a reducing agent for the eco-friendly synthesis of AgNPs. The keratinase produced by strain R13 was responsible for the reduction of silver ions and the subsequent formation of AgNPs. Maximum AgNP synthesis was achieved using 2 mM AgNO 3 at pH 9 and 40 °C. Electron microscopy and dynamic light scattering analysis showed AgNPs were spherical and of average diameter ~ 8.4 nm. X-ray diffraction revealed that AgNPs were crystalline. FTIR indicated AgNPs were stabilized by proteins present in the crude enzyme solution of strain R13. AgNPs exhibited a broad antimicrobial spectrum against several pathogenic microorganisms, and the antimicrobial mechanism appeared to involve structural deformation of cells resulting in membrane leakage and subsequent lysis. AgNPs also displayed 1,1-diphenyl-2-picrylhydrazyl (IC 50 = 0.0112 mg/ml), 2,2'-azinobis-3-ethylbenzothiazoline-6-sulfonate radical scavenging (IC 50 = 0.0243 mg/ml), and anti-collagenase (IC 50 = 23.5 mg/ml) activities. 2017 Journal Article http://hdl.handle.net/20.500.11937/66369 10.1007/s00449-017-1873-0 restricted
spellingShingle Jang, E.
Son, Y.
Park, S.
Yoo, J.
Cho, Y.
Jeong, S.
Liu, Shaomin
Son, H.
Improved biosynthesis of silver nanoparticles using keratinase from Stenotrophomonas maltophilia R13: reaction optimization, structural characterization, and biomedical activity
title Improved biosynthesis of silver nanoparticles using keratinase from Stenotrophomonas maltophilia R13: reaction optimization, structural characterization, and biomedical activity
title_full Improved biosynthesis of silver nanoparticles using keratinase from Stenotrophomonas maltophilia R13: reaction optimization, structural characterization, and biomedical activity
title_fullStr Improved biosynthesis of silver nanoparticles using keratinase from Stenotrophomonas maltophilia R13: reaction optimization, structural characterization, and biomedical activity
title_full_unstemmed Improved biosynthesis of silver nanoparticles using keratinase from Stenotrophomonas maltophilia R13: reaction optimization, structural characterization, and biomedical activity
title_short Improved biosynthesis of silver nanoparticles using keratinase from Stenotrophomonas maltophilia R13: reaction optimization, structural characterization, and biomedical activity
title_sort improved biosynthesis of silver nanoparticles using keratinase from stenotrophomonas maltophilia r13: reaction optimization, structural characterization, and biomedical activity
url http://hdl.handle.net/20.500.11937/66369