Solar photocatalytic degradation of 4-chlorophenol: Mechanism and kinetic modelling

The present study reports a mechanism and kinetic model of solar photocatalytic degradation of 4-chlorophenol (4-CP) and its intermediates based on the experimental results. Three intermediate compounds hydroquinone (HQ), 4-chlorocatechol (4cCat) and phenol were found during the solar degradation of...

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Main Authors: Abeish, Abdulbasit M., Ang, Ha Ming, Znad, Hussein
Format: Journal Article
Published: Taylor & Francis Ltd. 2013
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/6516
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author Abeish, Abdulbasit M.
Ang, Ha Ming
Znad, Hussein
author_facet Abeish, Abdulbasit M.
Ang, Ha Ming
Znad, Hussein
author_sort Abeish, Abdulbasit M.
building Curtin Institutional Repository
collection Online Access
description The present study reports a mechanism and kinetic model of solar photocatalytic degradation of 4-chlorophenol (4-CP) and its intermediates based on the experimental results. Three intermediate compounds hydroquinone (HQ), 4-chlorocatechol (4cCat) and phenol were found during the solar degradation of different 4-CP concentrations using 0.5 g/L TiO2 as a photocatalyst. In order to obtain more details about the photocatalytic reaction pathway and the kinetic model, set of experiments were carried out using the major intermediates (HQ and 4cCat) as model reactants. To minimise the number of variables and give more accuracy to the kinetic model, the adsorption constants of 4-CPand its intermediates were obtained experimentally. The reaction mechanism for the photocatalytic degradation of 4-CP is proposed. The proposed model predicts well the concentrations of 4-CP and its by-products during the solar photocatalytic degradation at different initial concentrations. The model provides a very good fit of the experimental data and works for a wide range of 4-CP initial concentrations (25–100 mg/L).
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institution Curtin University Malaysia
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publishDate 2013
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spelling curtin-20.500.11937-65162017-09-13T14:41:38Z Solar photocatalytic degradation of 4-chlorophenol: Mechanism and kinetic modelling Abeish, Abdulbasit M. Ang, Ha Ming Znad, Hussein 4-Chlorophenol Mechanism Solar-photocatalytic degradation Kinetic modelling Intermediates The present study reports a mechanism and kinetic model of solar photocatalytic degradation of 4-chlorophenol (4-CP) and its intermediates based on the experimental results. Three intermediate compounds hydroquinone (HQ), 4-chlorocatechol (4cCat) and phenol were found during the solar degradation of different 4-CP concentrations using 0.5 g/L TiO2 as a photocatalyst. In order to obtain more details about the photocatalytic reaction pathway and the kinetic model, set of experiments were carried out using the major intermediates (HQ and 4cCat) as model reactants. To minimise the number of variables and give more accuracy to the kinetic model, the adsorption constants of 4-CPand its intermediates were obtained experimentally. The reaction mechanism for the photocatalytic degradation of 4-CP is proposed. The proposed model predicts well the concentrations of 4-CP and its by-products during the solar photocatalytic degradation at different initial concentrations. The model provides a very good fit of the experimental data and works for a wide range of 4-CP initial concentrations (25–100 mg/L). 2013 Journal Article http://hdl.handle.net/20.500.11937/6516 10.1080/19443994.2013.869665 Taylor & Francis Ltd. fulltext
spellingShingle 4-Chlorophenol
Mechanism
Solar-photocatalytic degradation
Kinetic modelling
Intermediates
Abeish, Abdulbasit M.
Ang, Ha Ming
Znad, Hussein
Solar photocatalytic degradation of 4-chlorophenol: Mechanism and kinetic modelling
title Solar photocatalytic degradation of 4-chlorophenol: Mechanism and kinetic modelling
title_full Solar photocatalytic degradation of 4-chlorophenol: Mechanism and kinetic modelling
title_fullStr Solar photocatalytic degradation of 4-chlorophenol: Mechanism and kinetic modelling
title_full_unstemmed Solar photocatalytic degradation of 4-chlorophenol: Mechanism and kinetic modelling
title_short Solar photocatalytic degradation of 4-chlorophenol: Mechanism and kinetic modelling
title_sort solar photocatalytic degradation of 4-chlorophenol: mechanism and kinetic modelling
topic 4-Chlorophenol
Mechanism
Solar-photocatalytic degradation
Kinetic modelling
Intermediates
url http://hdl.handle.net/20.500.11937/6516