Optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using Taguchi design of experiments
This article aims to study the effects of material formulation and processing parameters on mechanical properties of bioepoxy/clay nanocomposites based on epoxidized soybean oil (ESO) via Taguchi design of experiments (DoEs). A mixed-level DoE with an L16 orthogonal array was constructed to achieve...
| Main Authors: | , , , |
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| Format: | Journal Article |
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John Wiley and Sons Inc
2018
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| Online Access: | http://hdl.handle.net/20.500.11937/62964 |
| _version_ | 1848760957073883136 |
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| author | Salam, H. Dong, Yu Davies, Ian Pramanik, Alokesh |
| author_facet | Salam, H. Dong, Yu Davies, Ian Pramanik, Alokesh |
| author_sort | Salam, H. |
| building | Curtin Institutional Repository |
| collection | Online Access |
| description | This article aims to study the effects of material formulation and processing parameters on mechanical properties of bioepoxy/clay nanocomposites based on epoxidized soybean oil (ESO) via Taguchi design of experiments (DoEs). A mixed-level DoE with an L16 orthogonal array was constructed to achieve maximum levels of tensile strength, tensile modulus, and impact strength for corresponding bionanocomposites. Pareto analysis of variance (ANOVA) was used to identify significant factors and preferred formulations in the manufacture of bioepoxy/clay nanocomposites. The ESO content was found to have the most significant effect with regards to bionanocomposite mechanical properties with contribution percentages of 66.63, 72.96, and 40.14% for their tensile strength, tensile modulus, and impact strength, respectively. With regards to material processing parameters, mechanical mixing speed was identified as a critical factor to achieve optimal tensile and impact properties. Nonetheless, the results also indicated clay content to be a significant factor for tensile strength, whereas curing agent type was vital for the improvement of tensile modulus and impact strength. Clay type and sonication time were also found to be significant factors for impact strength. In contrast to this, manufacturing parameters such as mechanical mixing temperature, mixing time, and sonication frequency were considered to be non-significant factors due to their low cumulative contribution percentages of <10%. Finally, experimental confirmation tests based on the preferred combination of factors demonstrated good agreement with statistically predicted results. |
| first_indexed | 2025-11-14T10:24:01Z |
| format | Journal Article |
| id | curtin-20.500.11937-62964 |
| institution | Curtin University Malaysia |
| institution_category | Local University |
| last_indexed | 2025-11-14T10:24:01Z |
| publishDate | 2018 |
| publisher | John Wiley and Sons Inc |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | curtin-20.500.11937-629642018-04-17T08:59:33Z Optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using Taguchi design of experiments Salam, H. Dong, Yu Davies, Ian Pramanik, Alokesh clay structure–property relationships biopolymers and renewable polymers mechanical properties nanocomposites design of experiments (DoEs) This article aims to study the effects of material formulation and processing parameters on mechanical properties of bioepoxy/clay nanocomposites based on epoxidized soybean oil (ESO) via Taguchi design of experiments (DoEs). A mixed-level DoE with an L16 orthogonal array was constructed to achieve maximum levels of tensile strength, tensile modulus, and impact strength for corresponding bionanocomposites. Pareto analysis of variance (ANOVA) was used to identify significant factors and preferred formulations in the manufacture of bioepoxy/clay nanocomposites. The ESO content was found to have the most significant effect with regards to bionanocomposite mechanical properties with contribution percentages of 66.63, 72.96, and 40.14% for their tensile strength, tensile modulus, and impact strength, respectively. With regards to material processing parameters, mechanical mixing speed was identified as a critical factor to achieve optimal tensile and impact properties. Nonetheless, the results also indicated clay content to be a significant factor for tensile strength, whereas curing agent type was vital for the improvement of tensile modulus and impact strength. Clay type and sonication time were also found to be significant factors for impact strength. In contrast to this, manufacturing parameters such as mechanical mixing temperature, mixing time, and sonication frequency were considered to be non-significant factors due to their low cumulative contribution percentages of <10%. Finally, experimental confirmation tests based on the preferred combination of factors demonstrated good agreement with statistically predicted results. 2018 Journal Article http://hdl.handle.net/20.500.11937/62964 10.1002/APP.45769 John Wiley and Sons Inc restricted |
| spellingShingle | clay structure–property relationships biopolymers and renewable polymers mechanical properties nanocomposites design of experiments (DoEs) Salam, H. Dong, Yu Davies, Ian Pramanik, Alokesh Optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using Taguchi design of experiments |
| title | Optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using Taguchi design of experiments |
| title_full | Optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using Taguchi design of experiments |
| title_fullStr | Optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using Taguchi design of experiments |
| title_full_unstemmed | Optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using Taguchi design of experiments |
| title_short | Optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using Taguchi design of experiments |
| title_sort | optimization of material formulation and processing parameters in relation to mechanical properties of bioepoxy/clay nanocomposites using taguchi design of experiments |
| topic | clay structure–property relationships biopolymers and renewable polymers mechanical properties nanocomposites design of experiments (DoEs) |
| url | http://hdl.handle.net/20.500.11937/62964 |