Effect of Pd doping on the activity and stability of directly assembled La0.95Co0.19Fe0.76Pd0.05O3-δ cathodes of solid oxide fuel cells

Sr doping is a common strategy to enhance the electrocatalytic activity of perovskite cathode materials of solid oxide fuel cells (SOFCs), but the tendency of Sr surface segregation, chemical incompatibility with yttria-stabilized zirconia (YSZ) and interaction with volatile contaminants such as chr...

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Main Authors: Li, N., Ai, N., He, S., Cheng, Y., Rickard, William, Chen, K., Zhang, T., Jiang, S.
Format: Journal Article
Published: Elsevier BV * North-Holland 2018
Online Access:http://purl.org/au-research/grants/arc/DP150102025
http://hdl.handle.net/20.500.11937/61207
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author Li, N.
Ai, N.
He, S.
Cheng, Y.
Rickard, William
Chen, K.
Zhang, T.
Jiang, S.
author_facet Li, N.
Ai, N.
He, S.
Cheng, Y.
Rickard, William
Chen, K.
Zhang, T.
Jiang, S.
author_sort Li, N.
building Curtin Institutional Repository
collection Online Access
description Sr doping is a common strategy to enhance the electrocatalytic activity of perovskite cathode materials of solid oxide fuel cells (SOFCs), but the tendency of Sr surface segregation, chemical incompatibility with yttria-stabilized zirconia (YSZ) and interaction with volatile contaminants such as chromium in SOFC stacks lead to a loss of long-term cell performance. Herein, a Sr-free and Pd-doped La 0.95 Co 0.19 Fe 0.76 Pd 0.05 O 3-d (LCFPd) cathode is directly assembled on a barrier-layer-free YSZ electrolyte cell without conventional high temperature pre-sintering. The cell with the directly assembled LCFPd-GDC (gadolinium-doped ceria) composite cathode exhibits a peak power density of 1035 mW cm - 2 and excellent operation stability at 750 °C for 200 h. Cathodic polarization significantly enhances the electrode/electrolyte interface contact, indicated by the substantial decrease of cell ohmic resistance from 0.28 O cm 2 to 0.14 O cm 2 after polarization at 500 mA cm - 2 and 750 °C for 120 h. Detailed elemental analysis indicates that doped Pd could be segregated on the electrode surface under fuel cell operation conditions, which significantly enhances the electrocatalytic activity for the O 2 reduction reaction. This study provides new strategy to develop cobaltite based perovskite materials directly on YSZ electrolyte.
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publishDate 2018
publisher Elsevier BV * North-Holland
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spelling curtin-20.500.11937-612072022-10-12T07:08:31Z Effect of Pd doping on the activity and stability of directly assembled La0.95Co0.19Fe0.76Pd0.05O3-δ cathodes of solid oxide fuel cells Li, N. Ai, N. He, S. Cheng, Y. Rickard, William Chen, K. Zhang, T. Jiang, S. Sr doping is a common strategy to enhance the electrocatalytic activity of perovskite cathode materials of solid oxide fuel cells (SOFCs), but the tendency of Sr surface segregation, chemical incompatibility with yttria-stabilized zirconia (YSZ) and interaction with volatile contaminants such as chromium in SOFC stacks lead to a loss of long-term cell performance. Herein, a Sr-free and Pd-doped La 0.95 Co 0.19 Fe 0.76 Pd 0.05 O 3-d (LCFPd) cathode is directly assembled on a barrier-layer-free YSZ electrolyte cell without conventional high temperature pre-sintering. The cell with the directly assembled LCFPd-GDC (gadolinium-doped ceria) composite cathode exhibits a peak power density of 1035 mW cm - 2 and excellent operation stability at 750 °C for 200 h. Cathodic polarization significantly enhances the electrode/electrolyte interface contact, indicated by the substantial decrease of cell ohmic resistance from 0.28 O cm 2 to 0.14 O cm 2 after polarization at 500 mA cm - 2 and 750 °C for 120 h. Detailed elemental analysis indicates that doped Pd could be segregated on the electrode surface under fuel cell operation conditions, which significantly enhances the electrocatalytic activity for the O 2 reduction reaction. This study provides new strategy to develop cobaltite based perovskite materials directly on YSZ electrolyte. 2018 Journal Article http://hdl.handle.net/20.500.11937/61207 10.1016/j.ssi.2017.12.020 http://purl.org/au-research/grants/arc/DP150102025 http://purl.org/au-research/grants/arc/DP150102044 Elsevier BV * North-Holland restricted
spellingShingle Li, N.
Ai, N.
He, S.
Cheng, Y.
Rickard, William
Chen, K.
Zhang, T.
Jiang, S.
Effect of Pd doping on the activity and stability of directly assembled La0.95Co0.19Fe0.76Pd0.05O3-δ cathodes of solid oxide fuel cells
title Effect of Pd doping on the activity and stability of directly assembled La0.95Co0.19Fe0.76Pd0.05O3-δ cathodes of solid oxide fuel cells
title_full Effect of Pd doping on the activity and stability of directly assembled La0.95Co0.19Fe0.76Pd0.05O3-δ cathodes of solid oxide fuel cells
title_fullStr Effect of Pd doping on the activity and stability of directly assembled La0.95Co0.19Fe0.76Pd0.05O3-δ cathodes of solid oxide fuel cells
title_full_unstemmed Effect of Pd doping on the activity and stability of directly assembled La0.95Co0.19Fe0.76Pd0.05O3-δ cathodes of solid oxide fuel cells
title_short Effect of Pd doping on the activity and stability of directly assembled La0.95Co0.19Fe0.76Pd0.05O3-δ cathodes of solid oxide fuel cells
title_sort effect of pd doping on the activity and stability of directly assembled la0.95co0.19fe0.76pd0.05o3-δ cathodes of solid oxide fuel cells
url http://purl.org/au-research/grants/arc/DP150102025
http://purl.org/au-research/grants/arc/DP150102025
http://hdl.handle.net/20.500.11937/61207