Changes in char structure due to inorganic matters during anthracite pyrolysis

© 2017 Elsevier B.V. To understand effects of inherent mineral matters on the evolution of char structure, the microcrystalline structures of chars from the pyrolysis of raw, HCl-washed (CW) and HCl & HF-washed anthracites (CFW) were investigated by X-ray diffraction (XRD) respectively. Stacking...

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Main Authors: Gong, X., Zhang, Shu
Format: Journal Article
Published: Elsevier 2017
Online Access:http://hdl.handle.net/20.500.11937/58494
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author Gong, X.
Zhang, Shu
author_facet Gong, X.
Zhang, Shu
author_sort Gong, X.
building Curtin Institutional Repository
collection Online Access
description © 2017 Elsevier B.V. To understand effects of inherent mineral matters on the evolution of char structure, the microcrystalline structures of chars from the pyrolysis of raw, HCl-washed (CW) and HCl & HF-washed anthracites (CFW) were investigated by X-ray diffraction (XRD) respectively. Stacking height (Lc), interlayer spacing (d 002 ) and crystallite width (La) were used as parameters for char structure estimation. The results showed that with increasing contents of inherent mineral matters, Lc of char decreased, whereas d 002 and La increased. To study effects of a single inorganic matter, CFW was impregnated with Al 2 O 3 , SiO 2 , and CaO respectively. It was found that all of them (oxides) have resulted in the decrease in Lc and increase in La and d 002 . Differing from Al 2 O 3 , SiO 2 , and CaO, the introduction of Fe 2 O 3 has caused the reduction for both La and Lc values simultaneously, especially when the Fe 2 O 3 contents in the coal were high.
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spelling curtin-20.500.11937-584942017-11-24T05:45:54Z Changes in char structure due to inorganic matters during anthracite pyrolysis Gong, X. Zhang, Shu © 2017 Elsevier B.V. To understand effects of inherent mineral matters on the evolution of char structure, the microcrystalline structures of chars from the pyrolysis of raw, HCl-washed (CW) and HCl & HF-washed anthracites (CFW) were investigated by X-ray diffraction (XRD) respectively. Stacking height (Lc), interlayer spacing (d 002 ) and crystallite width (La) were used as parameters for char structure estimation. The results showed that with increasing contents of inherent mineral matters, Lc of char decreased, whereas d 002 and La increased. To study effects of a single inorganic matter, CFW was impregnated with Al 2 O 3 , SiO 2 , and CaO respectively. It was found that all of them (oxides) have resulted in the decrease in Lc and increase in La and d 002 . Differing from Al 2 O 3 , SiO 2 , and CaO, the introduction of Fe 2 O 3 has caused the reduction for both La and Lc values simultaneously, especially when the Fe 2 O 3 contents in the coal were high. 2017 Journal Article http://hdl.handle.net/20.500.11937/58494 10.1016/j.jaap.2017.08.011 Elsevier restricted
spellingShingle Gong, X.
Zhang, Shu
Changes in char structure due to inorganic matters during anthracite pyrolysis
title Changes in char structure due to inorganic matters during anthracite pyrolysis
title_full Changes in char structure due to inorganic matters during anthracite pyrolysis
title_fullStr Changes in char structure due to inorganic matters during anthracite pyrolysis
title_full_unstemmed Changes in char structure due to inorganic matters during anthracite pyrolysis
title_short Changes in char structure due to inorganic matters during anthracite pyrolysis
title_sort changes in char structure due to inorganic matters during anthracite pyrolysis
url http://hdl.handle.net/20.500.11937/58494