A hybrid zeolitic imidazolate framework Co-IM-mIM membrane for gas separation

© 2017, Central South University Press and Springer-Verlag GmbH Germany. A zeolitic imidazolate hybrid membrane (Co-IM-mIM) containing two imidazolate ligands deposited on a macroporous a-alumina support was prepared by pre-depositing and secondary growth technique. XRD, TGA and SEM characterization...

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Main Authors: Gao, Z., Li, L., Li, H., Chen, R., Wang, Shaobin, Wang, Y.
Format: Journal Article
Published: 2017
Online Access:http://hdl.handle.net/20.500.11937/58030
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author Gao, Z.
Li, L.
Li, H.
Chen, R.
Wang, Shaobin
Wang, Y.
author_facet Gao, Z.
Li, L.
Li, H.
Chen, R.
Wang, Shaobin
Wang, Y.
author_sort Gao, Z.
building Curtin Institutional Repository
collection Online Access
description © 2017, Central South University Press and Springer-Verlag GmbH Germany. A zeolitic imidazolate hybrid membrane (Co-IM-mIM) containing two imidazolate ligands deposited on a macroporous a-alumina support was prepared by pre-depositing and secondary growth technique. XRD, TGA and SEM characterizations demonstrate that a stable and thin, but dense and pure-phase Co-IM-mIM membrane can be obtained on the macroporous-alumina discs in Teflon-lined autoclave at 120 °C after pre-depositing by dip-coating at room temperature. No visible cracks, pinholes or othe r defects were observed on the membrane layer. The gas separation studies of Co-IM-mIM membrane were carried out at 25 °C and 1×10 5 Pa, showing ideal selectivity of 6.95, 5.25, 3.40 for H 2 /CO 2 , H 2 /N 2 and H 2 /CH 4 , respectively, and a permeance of 17.37× 10 -6 mol/(m 2 ·s·Pa) for H 2 . The influence of temperature and trans-membrane pressure on hydrogen separation and permeation was also carried out. The gas permeation and selectivity demonstrate that this membrane may have potential applications for efficient H 2 separation.
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spelling curtin-20.500.11937-580302017-11-20T08:58:25Z A hybrid zeolitic imidazolate framework Co-IM-mIM membrane for gas separation Gao, Z. Li, L. Li, H. Chen, R. Wang, Shaobin Wang, Y. © 2017, Central South University Press and Springer-Verlag GmbH Germany. A zeolitic imidazolate hybrid membrane (Co-IM-mIM) containing two imidazolate ligands deposited on a macroporous a-alumina support was prepared by pre-depositing and secondary growth technique. XRD, TGA and SEM characterizations demonstrate that a stable and thin, but dense and pure-phase Co-IM-mIM membrane can be obtained on the macroporous-alumina discs in Teflon-lined autoclave at 120 °C after pre-depositing by dip-coating at room temperature. No visible cracks, pinholes or othe r defects were observed on the membrane layer. The gas separation studies of Co-IM-mIM membrane were carried out at 25 °C and 1×10 5 Pa, showing ideal selectivity of 6.95, 5.25, 3.40 for H 2 /CO 2 , H 2 /N 2 and H 2 /CH 4 , respectively, and a permeance of 17.37× 10 -6 mol/(m 2 ·s·Pa) for H 2 . The influence of temperature and trans-membrane pressure on hydrogen separation and permeation was also carried out. The gas permeation and selectivity demonstrate that this membrane may have potential applications for efficient H 2 separation. 2017 Journal Article http://hdl.handle.net/20.500.11937/58030 10.1007/s11771-017-3580-z restricted
spellingShingle Gao, Z.
Li, L.
Li, H.
Chen, R.
Wang, Shaobin
Wang, Y.
A hybrid zeolitic imidazolate framework Co-IM-mIM membrane for gas separation
title A hybrid zeolitic imidazolate framework Co-IM-mIM membrane for gas separation
title_full A hybrid zeolitic imidazolate framework Co-IM-mIM membrane for gas separation
title_fullStr A hybrid zeolitic imidazolate framework Co-IM-mIM membrane for gas separation
title_full_unstemmed A hybrid zeolitic imidazolate framework Co-IM-mIM membrane for gas separation
title_short A hybrid zeolitic imidazolate framework Co-IM-mIM membrane for gas separation
title_sort hybrid zeolitic imidazolate framework co-im-mim membrane for gas separation
url http://hdl.handle.net/20.500.11937/58030