Graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/N-doped carbon nanosheets for oxygen reduction reactions

A metal-organic framework (MOF) seed-mediated deposition route is developed to synthesize MOF/graphene oxide (GO)/MOF nano-sandwiches with core-shell structured MOF (i.e. ZIF-8@ZIF-67) crystals uniformly distributed on GO. Due to the well controllable growth rate, ZIF-8 seeds are first deposited on...

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Main Authors: Wei, J., Hu, Y., Liang, Y., Kong, B., Zheng, Z., Zhang, J., Jiang, San Ping, Zhao, Y., Wang, H.
Format: Journal Article
Published: R S C Publications 2017
Online Access:http://purl.org/au-research/grants/arc/DP150102044
http://hdl.handle.net/20.500.11937/56977
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author Wei, J.
Hu, Y.
Liang, Y.
Kong, B.
Zheng, Z.
Zhang, J.
Jiang, San Ping
Zhao, Y.
Wang, H.
author_facet Wei, J.
Hu, Y.
Liang, Y.
Kong, B.
Zheng, Z.
Zhang, J.
Jiang, San Ping
Zhao, Y.
Wang, H.
author_sort Wei, J.
building Curtin Institutional Repository
collection Online Access
description A metal-organic framework (MOF) seed-mediated deposition route is developed to synthesize MOF/graphene oxide (GO)/MOF nano-sandwiches with core-shell structured MOF (i.e. ZIF-8@ZIF-67) crystals uniformly distributed on GO. Due to the well controllable growth rate, ZIF-8 seeds are first deposited on GO. Then, ZIF-67 species are selectively deposited on the surface of ZIF-8 to form core-shell structures owing to their similar crystal structure and unit cell parameter. Compared with the direct deposition of ZIF-67 crystals on GO, this MOF seed-mediated synthesis can effectively prevent the over-growth and inhomogeneous distribution of ZIF-67 crystals. The GO/core-shell MOF composites are further demonstrated to be an excellent precursor for cobalt/N-doped carbon nanosheets, which are efficient nonprecious metal catalysts for oxygen reduction reactions, and exhibit a high onset potential (~0.93 V versus reversible hydrogen electrode, vs. the RHE) and large kinetic current density (~101 mA mg -1 at 0.80 V vs. the RHE). Such novel carbon materials derived from the core-shell structured MOF also show better catalytic performance than those derived from both GO/ZIF-8 and GO/ZIF-67 prepared under the same conditions. This work offers an alternative strategy to develop MOF-derived carbon-based composites using GO/core-shell structured MOFs as a kind of fresh precursors.
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institution Curtin University Malaysia
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last_indexed 2025-11-14T10:08:34Z
publishDate 2017
publisher R S C Publications
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spelling curtin-20.500.11937-569772022-10-12T07:15:31Z Graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/N-doped carbon nanosheets for oxygen reduction reactions Wei, J. Hu, Y. Liang, Y. Kong, B. Zheng, Z. Zhang, J. Jiang, San Ping Zhao, Y. Wang, H. A metal-organic framework (MOF) seed-mediated deposition route is developed to synthesize MOF/graphene oxide (GO)/MOF nano-sandwiches with core-shell structured MOF (i.e. ZIF-8@ZIF-67) crystals uniformly distributed on GO. Due to the well controllable growth rate, ZIF-8 seeds are first deposited on GO. Then, ZIF-67 species are selectively deposited on the surface of ZIF-8 to form core-shell structures owing to their similar crystal structure and unit cell parameter. Compared with the direct deposition of ZIF-67 crystals on GO, this MOF seed-mediated synthesis can effectively prevent the over-growth and inhomogeneous distribution of ZIF-67 crystals. The GO/core-shell MOF composites are further demonstrated to be an excellent precursor for cobalt/N-doped carbon nanosheets, which are efficient nonprecious metal catalysts for oxygen reduction reactions, and exhibit a high onset potential (~0.93 V versus reversible hydrogen electrode, vs. the RHE) and large kinetic current density (~101 mA mg -1 at 0.80 V vs. the RHE). Such novel carbon materials derived from the core-shell structured MOF also show better catalytic performance than those derived from both GO/ZIF-8 and GO/ZIF-67 prepared under the same conditions. This work offers an alternative strategy to develop MOF-derived carbon-based composites using GO/core-shell structured MOFs as a kind of fresh precursors. 2017 Journal Article http://hdl.handle.net/20.500.11937/56977 10.1039/c7ta00276a http://purl.org/au-research/grants/arc/DP150102044 http://creativecommons.org/licenses/by/3.0/ R S C Publications fulltext
spellingShingle Wei, J.
Hu, Y.
Liang, Y.
Kong, B.
Zheng, Z.
Zhang, J.
Jiang, San Ping
Zhao, Y.
Wang, H.
Graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/N-doped carbon nanosheets for oxygen reduction reactions
title Graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/N-doped carbon nanosheets for oxygen reduction reactions
title_full Graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/N-doped carbon nanosheets for oxygen reduction reactions
title_fullStr Graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/N-doped carbon nanosheets for oxygen reduction reactions
title_full_unstemmed Graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/N-doped carbon nanosheets for oxygen reduction reactions
title_short Graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/N-doped carbon nanosheets for oxygen reduction reactions
title_sort graphene oxide/core-shell structured metal-organic framework nano-sandwiches and their derived cobalt/n-doped carbon nanosheets for oxygen reduction reactions
url http://purl.org/au-research/grants/arc/DP150102044
http://hdl.handle.net/20.500.11937/56977