Synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants

Novel “sea urchin”-like Ni nanoparticles embedded in N-doped carbon nanotubes (CNTs) supported on porous carbon (Ni@N-C) 3D materials derived from waste biomass were prepared via pyrolysis and employed as an environmentally friendly, easy available and cost-effective catalyst for removal of toxic po...

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Main Authors: Yao, Y., Lian, C., Wu, G., Hu, Y., Wei, F., Yu, M., Wang, Shaobin
Format: Journal Article
Published: Elsevier BV 2017
Online Access:http://purl.org/au-research/grants/arc/DP150103026
http://hdl.handle.net/20.500.11937/56811
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author Yao, Y.
Lian, C.
Wu, G.
Hu, Y.
Wei, F.
Yu, M.
Wang, Shaobin
author_facet Yao, Y.
Lian, C.
Wu, G.
Hu, Y.
Wei, F.
Yu, M.
Wang, Shaobin
author_sort Yao, Y.
building Curtin Institutional Repository
collection Online Access
description Novel “sea urchin”-like Ni nanoparticles embedded in N-doped carbon nanotubes (CNTs) supported on porous carbon (Ni@N-C) 3D materials derived from waste biomass were prepared via pyrolysis and employed as an environmentally friendly, easy available and cost-effective catalyst for removal of toxic pollutants. The characterizations indicated that Ni 0 catalyzed the growth of intertwined CNTs on carbon layers, affording abundant porous structures and larger specific surface area. With the synergistic effect of embedded Ni 0 nanoparticles, nitrogen doping, hierarchical micro-mesopores, and interconnected CNTs, Ni@N-C displayed a superior catalytic capability for the oxidation of organic pollutants using peroxymonosulfate as an oxidant, and catalytic reduction of toxic Cr VI to nontoxic Cr III by formic acid as a reducing agent. It was found that pyrolysis temperatures affected the compositions, morphologies, and catalytic properties of Ni@N-C. Inactive oxidized N species have transformed to the highly active graphitic N, pyridinic-N, and Ni-O-N clusters, thereby improving the catalytic activity. Moreover, Ni@N-C maintained good physicochemical structure and stable activity even after several cycles of reactions. The simple synthetic strategies, 3D structure, and remarkable performance of Ni@N-C composites make them serve as alternative environmentally friendly catalysts for removal of pollutants.
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institution Curtin University Malaysia
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publishDate 2017
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spelling curtin-20.500.11937-568112022-10-26T06:25:44Z Synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants Yao, Y. Lian, C. Wu, G. Hu, Y. Wei, F. Yu, M. Wang, Shaobin Novel “sea urchin”-like Ni nanoparticles embedded in N-doped carbon nanotubes (CNTs) supported on porous carbon (Ni@N-C) 3D materials derived from waste biomass were prepared via pyrolysis and employed as an environmentally friendly, easy available and cost-effective catalyst for removal of toxic pollutants. The characterizations indicated that Ni 0 catalyzed the growth of intertwined CNTs on carbon layers, affording abundant porous structures and larger specific surface area. With the synergistic effect of embedded Ni 0 nanoparticles, nitrogen doping, hierarchical micro-mesopores, and interconnected CNTs, Ni@N-C displayed a superior catalytic capability for the oxidation of organic pollutants using peroxymonosulfate as an oxidant, and catalytic reduction of toxic Cr VI to nontoxic Cr III by formic acid as a reducing agent. It was found that pyrolysis temperatures affected the compositions, morphologies, and catalytic properties of Ni@N-C. Inactive oxidized N species have transformed to the highly active graphitic N, pyridinic-N, and Ni-O-N clusters, thereby improving the catalytic activity. Moreover, Ni@N-C maintained good physicochemical structure and stable activity even after several cycles of reactions. The simple synthetic strategies, 3D structure, and remarkable performance of Ni@N-C composites make them serve as alternative environmentally friendly catalysts for removal of pollutants. 2017 Journal Article http://hdl.handle.net/20.500.11937/56811 10.1016/j.apcatb.2017.07.064 http://purl.org/au-research/grants/arc/DP150103026 Elsevier BV restricted
spellingShingle Yao, Y.
Lian, C.
Wu, G.
Hu, Y.
Wei, F.
Yu, M.
Wang, Shaobin
Synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants
title Synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants
title_full Synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants
title_fullStr Synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants
title_full_unstemmed Synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants
title_short Synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants
title_sort synthesis of “sea urchin”-like carbon nanotubes/porous carbon superstructures derived from waste biomass for treatment of various contaminants
url http://purl.org/au-research/grants/arc/DP150103026
http://hdl.handle.net/20.500.11937/56811