Crystallinity, surface morphology, and chemical composition of the recast layer and rutile-TiO2 formation on Ti-6Al-4V ELI by wire-EDM to enhance biocompatibility

© 2017 Springer-Verlag London Ltd. In this study, the surface morphology, chemical composition, and crystallography of the recast layer on wire electrical discharge machining (wire-EDM) modified Ti-6Al-4V ELI were investigated through scanning electron microscopy, backscattered electron imaging, ene...

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Main Authors: Rahman, S., Ashraf, M., Bashar, M., Kamruzzaman, M., Nurul Amin, A., Hossain, Mofazzal
Format: Journal Article
Published: Springer 2017
Online Access:http://hdl.handle.net/20.500.11937/55897
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author Rahman, S.
Ashraf, M.
Bashar, M.
Kamruzzaman, M.
Nurul Amin, A.
Hossain, Mofazzal
author_facet Rahman, S.
Ashraf, M.
Bashar, M.
Kamruzzaman, M.
Nurul Amin, A.
Hossain, Mofazzal
author_sort Rahman, S.
building Curtin Institutional Repository
collection Online Access
description © 2017 Springer-Verlag London Ltd. In this study, the surface morphology, chemical composition, and crystallography of the recast layer on wire electrical discharge machining (wire-EDM) modified Ti-6Al-4V ELI were investigated through scanning electron microscopy, backscattered electron imaging, energy-dispersive x-ray spectroscopy, and x-ray diffraction. The characteristics of the two tailored cutting strategies, namely, main cut and finish trim cut, were evaluated in terms of micro-cracks, micro-pores, recast layer thickness (RLT), surface roughness (SR), phase transition, and micro-hardness. In addition, the relative changes of the SR, RLT, and kerf width were demonstrated with regard to peak current and pulse spacing. Noticeably fewer amounts of micro-cracks, micro-voids, remarkable truncation of RLT and SR, and nanoporous structure were attained at finish trim cut mode. It was also found out that an a ? a' + rutile-TiO 2 phase transition occurred on the recast layer of wire-EDM modified sample at finish trim cut. Furthermore, recast layer showed higher micro-hardness compared to that of the heat-affected zone and bulk material. In essence, the wire-EDM finish trim cut treatment is a potential technology to feasibly enhance the biocompatibility for Ti-6Al-4V ELI alloy through the formation of rutile-TiO 2 and amelioration of the surface morphology.
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spelling curtin-20.500.11937-558972023-08-02T06:39:09Z Crystallinity, surface morphology, and chemical composition of the recast layer and rutile-TiO2 formation on Ti-6Al-4V ELI by wire-EDM to enhance biocompatibility Rahman, S. Ashraf, M. Bashar, M. Kamruzzaman, M. Nurul Amin, A. Hossain, Mofazzal © 2017 Springer-Verlag London Ltd. In this study, the surface morphology, chemical composition, and crystallography of the recast layer on wire electrical discharge machining (wire-EDM) modified Ti-6Al-4V ELI were investigated through scanning electron microscopy, backscattered electron imaging, energy-dispersive x-ray spectroscopy, and x-ray diffraction. The characteristics of the two tailored cutting strategies, namely, main cut and finish trim cut, were evaluated in terms of micro-cracks, micro-pores, recast layer thickness (RLT), surface roughness (SR), phase transition, and micro-hardness. In addition, the relative changes of the SR, RLT, and kerf width were demonstrated with regard to peak current and pulse spacing. Noticeably fewer amounts of micro-cracks, micro-voids, remarkable truncation of RLT and SR, and nanoporous structure were attained at finish trim cut mode. It was also found out that an a ? a' + rutile-TiO 2 phase transition occurred on the recast layer of wire-EDM modified sample at finish trim cut. Furthermore, recast layer showed higher micro-hardness compared to that of the heat-affected zone and bulk material. In essence, the wire-EDM finish trim cut treatment is a potential technology to feasibly enhance the biocompatibility for Ti-6Al-4V ELI alloy through the formation of rutile-TiO 2 and amelioration of the surface morphology. 2017 Journal Article http://hdl.handle.net/20.500.11937/55897 10.1007/s00170-017-0772-5 Springer restricted
spellingShingle Rahman, S.
Ashraf, M.
Bashar, M.
Kamruzzaman, M.
Nurul Amin, A.
Hossain, Mofazzal
Crystallinity, surface morphology, and chemical composition of the recast layer and rutile-TiO2 formation on Ti-6Al-4V ELI by wire-EDM to enhance biocompatibility
title Crystallinity, surface morphology, and chemical composition of the recast layer and rutile-TiO2 formation on Ti-6Al-4V ELI by wire-EDM to enhance biocompatibility
title_full Crystallinity, surface morphology, and chemical composition of the recast layer and rutile-TiO2 formation on Ti-6Al-4V ELI by wire-EDM to enhance biocompatibility
title_fullStr Crystallinity, surface morphology, and chemical composition of the recast layer and rutile-TiO2 formation on Ti-6Al-4V ELI by wire-EDM to enhance biocompatibility
title_full_unstemmed Crystallinity, surface morphology, and chemical composition of the recast layer and rutile-TiO2 formation on Ti-6Al-4V ELI by wire-EDM to enhance biocompatibility
title_short Crystallinity, surface morphology, and chemical composition of the recast layer and rutile-TiO2 formation on Ti-6Al-4V ELI by wire-EDM to enhance biocompatibility
title_sort crystallinity, surface morphology, and chemical composition of the recast layer and rutile-tio2 formation on ti-6al-4v eli by wire-edm to enhance biocompatibility
url http://hdl.handle.net/20.500.11937/55897