3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification

3,4-(Hydroxymethyl-ethylenedioxy)thiophene (4) and 3,4-(2'-hydroxypropylenedioxy)thiophene (4'') were synthesized from dimethyl 3,4-dihydroxythiophene-2,5-dicarboxylate (1), which were isomers and difficult to separate. When they were esterified with tetrathiafulvalene carried carboxy...

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Main Authors: Zhang, L., Wu, Changzhi, Wang, C., Zuo, H., Shen, Y.
Format: Journal Article
Published: John Wiley & Sons 2015
Online Access:http://hdl.handle.net/20.500.11937/53921
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author Zhang, L.
Wu, Changzhi
Wang, C.
Zuo, H.
Shen, Y.
author_facet Zhang, L.
Wu, Changzhi
Wang, C.
Zuo, H.
Shen, Y.
author_sort Zhang, L.
building Curtin Institutional Repository
collection Online Access
description 3,4-(Hydroxymethyl-ethylenedioxy)thiophene (4) and 3,4-(2'-hydroxypropylenedioxy)thiophene (4'') were synthesized from dimethyl 3,4-dihydroxythiophene-2,5-dicarboxylate (1), which were isomers and difficult to separate. When they were esterified with tetrathiafulvalene carried carboxylic acid group, only 3,4-(hydroxymethyl-ethylenedioxy)thiophene (4) could be esterified. No such selectivity was observed when the isomers were esterified by lauric acid and benzoic acid, respectively.
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institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T09:57:03Z
publishDate 2015
publisher John Wiley & Sons
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spelling curtin-20.500.11937-539212017-10-23T01:46:59Z 3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification Zhang, L. Wu, Changzhi Wang, C. Zuo, H. Shen, Y. 3,4-(Hydroxymethyl-ethylenedioxy)thiophene (4) and 3,4-(2'-hydroxypropylenedioxy)thiophene (4'') were synthesized from dimethyl 3,4-dihydroxythiophene-2,5-dicarboxylate (1), which were isomers and difficult to separate. When they were esterified with tetrathiafulvalene carried carboxylic acid group, only 3,4-(hydroxymethyl-ethylenedioxy)thiophene (4) could be esterified. No such selectivity was observed when the isomers were esterified by lauric acid and benzoic acid, respectively. 2015 Journal Article http://hdl.handle.net/20.500.11937/53921 10.1002/jhet.1834 John Wiley & Sons restricted
spellingShingle Zhang, L.
Wu, Changzhi
Wang, C.
Zuo, H.
Shen, Y.
3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification
title 3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification
title_full 3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification
title_fullStr 3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification
title_full_unstemmed 3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification
title_short 3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification
title_sort 3,4-ethylenedioxythiophene functionalizationed with tetrathiafulvalene: synthesis and selective esterification
url http://hdl.handle.net/20.500.11937/53921