Time and temperature regime of continuous grain coarsening in an ECAP-processed Al(0.1 wt.% Sc) alloy

An equiaxed, submicron grain size distribution was generated in an Al(0.1 wt.% Sc) alloy by processing through equal channel angular pressing followed by a low temperature pre-ageing heat treatment. The alloy was subsequently annealed for various times at 300, 350, 400 and 450 °C for investigating t...

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Main Authors: Bommareddy, A., Quadir, Md Zakaria, Ferry, M.
Format: Journal Article
Published: Elsevier B.V. 2012
Online Access:http://hdl.handle.net/20.500.11937/52681
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author Bommareddy, A.
Quadir, Md Zakaria
Ferry, M.
author_facet Bommareddy, A.
Quadir, Md Zakaria
Ferry, M.
author_sort Bommareddy, A.
building Curtin Institutional Repository
collection Online Access
description An equiaxed, submicron grain size distribution was generated in an Al(0.1 wt.% Sc) alloy by processing through equal channel angular pressing followed by a low temperature pre-ageing heat treatment. The alloy was subsequently annealed for various times at 300, 350, 400 and 450 °C for investigating the thermal stability of the deformation microstructure. It was found that up to 400 °C, the submicron grain structure coarsens slowly and uniformly by a process of continuous recrystallization. Within this temperature range, the uniform dispersion of nano-sized Al 3Sc particles generated by the pre-ageing treatment substantially hinders grain coarsening by Zener pinning of the (sub)grain boundaries. At the higher annealing temperature of 450 °C, certain grains were found to grow discontinuously thereby generating a mixed microstructure consisting of both fine and coarse grains. The data in this study was combined with recent data for a higher solute Al(0.3 wt.% Sc) alloy for furthering our understanding of the time and temperature range in which this family of alloys is resistant to rapid, discontinuous grain coarsening (recrystallization). © 2011 Elsevier Ltd. All rights reserved.
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spelling curtin-20.500.11937-526812017-09-13T15:39:23Z Time and temperature regime of continuous grain coarsening in an ECAP-processed Al(0.1 wt.% Sc) alloy Bommareddy, A. Quadir, Md Zakaria Ferry, M. An equiaxed, submicron grain size distribution was generated in an Al(0.1 wt.% Sc) alloy by processing through equal channel angular pressing followed by a low temperature pre-ageing heat treatment. The alloy was subsequently annealed for various times at 300, 350, 400 and 450 °C for investigating the thermal stability of the deformation microstructure. It was found that up to 400 °C, the submicron grain structure coarsens slowly and uniformly by a process of continuous recrystallization. Within this temperature range, the uniform dispersion of nano-sized Al 3Sc particles generated by the pre-ageing treatment substantially hinders grain coarsening by Zener pinning of the (sub)grain boundaries. At the higher annealing temperature of 450 °C, certain grains were found to grow discontinuously thereby generating a mixed microstructure consisting of both fine and coarse grains. The data in this study was combined with recent data for a higher solute Al(0.3 wt.% Sc) alloy for furthering our understanding of the time and temperature range in which this family of alloys is resistant to rapid, discontinuous grain coarsening (recrystallization). © 2011 Elsevier Ltd. All rights reserved. 2012 Journal Article http://hdl.handle.net/20.500.11937/52681 10.1016/j.jallcom.2012.02.181 Elsevier B.V. restricted
spellingShingle Bommareddy, A.
Quadir, Md Zakaria
Ferry, M.
Time and temperature regime of continuous grain coarsening in an ECAP-processed Al(0.1 wt.% Sc) alloy
title Time and temperature regime of continuous grain coarsening in an ECAP-processed Al(0.1 wt.% Sc) alloy
title_full Time and temperature regime of continuous grain coarsening in an ECAP-processed Al(0.1 wt.% Sc) alloy
title_fullStr Time and temperature regime of continuous grain coarsening in an ECAP-processed Al(0.1 wt.% Sc) alloy
title_full_unstemmed Time and temperature regime of continuous grain coarsening in an ECAP-processed Al(0.1 wt.% Sc) alloy
title_short Time and temperature regime of continuous grain coarsening in an ECAP-processed Al(0.1 wt.% Sc) alloy
title_sort time and temperature regime of continuous grain coarsening in an ecap-processed al(0.1 wt.% sc) alloy
url http://hdl.handle.net/20.500.11937/52681