Mass production of carbon nanofibers using microwave technology

Copyright © 2015 American Scientific Publishers All rights reserved.Carbon nanotubes (CNFs) were produced by gas phase single stage microwave assisted chemical vapour deposition (MA-CVD) using ferrocene as a catalyst and acetylene (C2H2) and hydrogen (H2) as precursor gases. The effect of the proces...

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Bibliographic Details
Main Authors: Mujawar, Mubarak, Abdullah, E., Sahu, J., Jayakumar, N., Ganesan, P.
Format: Journal Article
Published: American Scientific Publishers 2015
Online Access:http://hdl.handle.net/20.500.11937/51591
Description
Summary:Copyright © 2015 American Scientific Publishers All rights reserved.Carbon nanotubes (CNFs) were produced by gas phase single stage microwave assisted chemical vapour deposition (MA-CVD) using ferrocene as a catalyst and acetylene (C2H2) and hydrogen (H2) as precursor gases. The effect of the process parameters such as microwave power, radiation time, and gas ratio of C2H2/H2 was investigated. The CNFs were characterized using scanning and transmission electron microscopy (TEM), and by thermogravimetric analysis (TGA). Results reveal that the optimized conditions for CNF production were 1000 W reaction power, 35 min radiation time, and 0.8 gas ratio of C2H2/H2. TEM analyses revealed that the uniformly dispersed CNFs diameters ranging from 115-131 nm. The TGA analysis showed that the purity of CNF produced was 93%.