Photoregenerable, bifunctional granules of carbon-doped g-C3N4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic

Environmental remediation employing semiconducting materials offer a greener solution for pollution control. Herein, we report the development of high surface area porous architecture of C3N4 nanosheets by a simple aqueous spray drying process. g-C3N4 nanosheets obtained by the thermal decomposition...

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Main Authors: Panneri, S., Ganguly, P., Mohan, M., Nair, Balagopal, Mohamed, A., Warrier, K., Hareesh, U.
Format: Journal Article
Published: American Chemical Society 2017
Online Access:http://hdl.handle.net/20.500.11937/50517
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author Panneri, S.
Ganguly, P.
Mohan, M.
Nair, Balagopal
Mohamed, A.
Warrier, K.
Hareesh, U.
author_facet Panneri, S.
Ganguly, P.
Mohan, M.
Nair, Balagopal
Mohamed, A.
Warrier, K.
Hareesh, U.
author_sort Panneri, S.
building Curtin Institutional Repository
collection Online Access
description Environmental remediation employing semiconducting materials offer a greener solution for pollution control. Herein, we report the development of high surface area porous architecture of C3N4 nanosheets by a simple aqueous spray drying process. g-C3N4 nanosheets obtained by the thermal decomposition of urea-thiourea mixture are spray granulated to microspheres using 2 wt% poly vinyl alcohol (PVA) as binder. The post granulation thermal oxidation treatment resulted in in situ doping of carbon leading to improved photophysical properties compared to pristine g-C3N4. The C3N4 granules with surface area values of 150 m2/g rendered repetitive adsorption of tetracycline antibiotic (~75% in 60 min) and the extended absorption in the visible region facilitated complete photocatalytic degradation upon sunlight irradiation (>95% in 90 min). The delocalized p bonds generated after carbon doping and the macro-meso porous architecture created by the granulation process aided high adsorption capacity (70 mg/g). The photoregenerable, bifunctional materials herein obtained can thus be employed for the adsorption and subsequent degradation of harmful organic pollutants without any secondary remediation processes.
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institution Curtin University Malaysia
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publishDate 2017
publisher American Chemical Society
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spelling curtin-20.500.11937-505172017-09-13T15:41:23Z Photoregenerable, bifunctional granules of carbon-doped g-C3N4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic Panneri, S. Ganguly, P. Mohan, M. Nair, Balagopal Mohamed, A. Warrier, K. Hareesh, U. Environmental remediation employing semiconducting materials offer a greener solution for pollution control. Herein, we report the development of high surface area porous architecture of C3N4 nanosheets by a simple aqueous spray drying process. g-C3N4 nanosheets obtained by the thermal decomposition of urea-thiourea mixture are spray granulated to microspheres using 2 wt% poly vinyl alcohol (PVA) as binder. The post granulation thermal oxidation treatment resulted in in situ doping of carbon leading to improved photophysical properties compared to pristine g-C3N4. The C3N4 granules with surface area values of 150 m2/g rendered repetitive adsorption of tetracycline antibiotic (~75% in 60 min) and the extended absorption in the visible region facilitated complete photocatalytic degradation upon sunlight irradiation (>95% in 90 min). The delocalized p bonds generated after carbon doping and the macro-meso porous architecture created by the granulation process aided high adsorption capacity (70 mg/g). The photoregenerable, bifunctional materials herein obtained can thus be employed for the adsorption and subsequent degradation of harmful organic pollutants without any secondary remediation processes. 2017 Journal Article http://hdl.handle.net/20.500.11937/50517 10.1021/acssuschemeng.6b02383 American Chemical Society restricted
spellingShingle Panneri, S.
Ganguly, P.
Mohan, M.
Nair, Balagopal
Mohamed, A.
Warrier, K.
Hareesh, U.
Photoregenerable, bifunctional granules of carbon-doped g-C3N4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic
title Photoregenerable, bifunctional granules of carbon-doped g-C3N4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic
title_full Photoregenerable, bifunctional granules of carbon-doped g-C3N4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic
title_fullStr Photoregenerable, bifunctional granules of carbon-doped g-C3N4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic
title_full_unstemmed Photoregenerable, bifunctional granules of carbon-doped g-C3N4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic
title_short Photoregenerable, bifunctional granules of carbon-doped g-C3N4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic
title_sort photoregenerable, bifunctional granules of carbon-doped g-c3n4 as adsorptive photocatalyst for the efficient removal of tetracycline antibiotic
url http://hdl.handle.net/20.500.11937/50517