In-situ fabricated gas sensors based on one dimensional core-shell TiO2-Al2O3 nanostructures

A novel in-situ sensor fabrication method consisting of one dimensional (1-D) core-shell TiO2-Al2O3 nanostructures is reported. The 1-D nanostructures were synthesized on Ti-6Al-4V (Ti64) particles by a robust, simple, inexpensive and highly scalable route based on thermal oxidation. The in-situ fab...

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Main Authors: Arafat, M., Haseeb, A., Akbar, S., Quadir, Md Zakaria
Format: Journal Article
Published: Elsevier 2017
Online Access:http://hdl.handle.net/20.500.11937/50051
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author Arafat, M.
Haseeb, A.
Akbar, S.
Quadir, Md Zakaria
author_facet Arafat, M.
Haseeb, A.
Akbar, S.
Quadir, Md Zakaria
author_sort Arafat, M.
building Curtin Institutional Repository
collection Online Access
description A novel in-situ sensor fabrication method consisting of one dimensional (1-D) core-shell TiO2-Al2O3 nanostructures is reported. The 1-D nanostructures were synthesized on Ti-6Al-4V (Ti64) particles by a robust, simple, inexpensive and highly scalable route based on thermal oxidation. The in-situ fabricated sensors were tested in various reducing and oxidizing gases including hydrogen (H2), hydrogen sulfide (H2S), carbon monoxide (CO), methane (CH4), methanol (CH3OH), ethanol (C2H5OH), ethylene (C2H4), nitrogen dioxide (NO2) and oxygen (O2). The selectivity, sensitivity, optimum operating temperature, response time and recovery time of the sensors were examined. Results reveal that the as-grown 1-D nanostructures are 1–5 µm long with diameter of 30–100 nm. The core and shell of the 1-D nanostructures consist of rutile-TiO2 and corundum-Al2O3, respectively. The growth direction of TiO2 and Al2O3 are <002> and <110>, respectively. The sensors consisting of 1-D core-shell TiO2-Al2O3 nanostructures show n-type sensing behavior. Selective sensitivity is seen towards H2S, CH3OH and C2H5OH in N2 background with response values of 38.7, 349.6 and 1108.9, respectively. The response time of the sensors decreases and recovery time increases with increasing the concentration of target gases. An electron tunneling assisted surface depletion model is proposed to explain the sensing mechanism of these sensors. © 2016 Elsevier B.V.
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publishDate 2017
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spelling curtin-20.500.11937-500512017-09-13T15:38:02Z In-situ fabricated gas sensors based on one dimensional core-shell TiO2-Al2O3 nanostructures Arafat, M. Haseeb, A. Akbar, S. Quadir, Md Zakaria A novel in-situ sensor fabrication method consisting of one dimensional (1-D) core-shell TiO2-Al2O3 nanostructures is reported. The 1-D nanostructures were synthesized on Ti-6Al-4V (Ti64) particles by a robust, simple, inexpensive and highly scalable route based on thermal oxidation. The in-situ fabricated sensors were tested in various reducing and oxidizing gases including hydrogen (H2), hydrogen sulfide (H2S), carbon monoxide (CO), methane (CH4), methanol (CH3OH), ethanol (C2H5OH), ethylene (C2H4), nitrogen dioxide (NO2) and oxygen (O2). The selectivity, sensitivity, optimum operating temperature, response time and recovery time of the sensors were examined. Results reveal that the as-grown 1-D nanostructures are 1–5 µm long with diameter of 30–100 nm. The core and shell of the 1-D nanostructures consist of rutile-TiO2 and corundum-Al2O3, respectively. The growth direction of TiO2 and Al2O3 are <002> and <110>, respectively. The sensors consisting of 1-D core-shell TiO2-Al2O3 nanostructures show n-type sensing behavior. Selective sensitivity is seen towards H2S, CH3OH and C2H5OH in N2 background with response values of 38.7, 349.6 and 1108.9, respectively. The response time of the sensors decreases and recovery time increases with increasing the concentration of target gases. An electron tunneling assisted surface depletion model is proposed to explain the sensing mechanism of these sensors. © 2016 Elsevier B.V. 2017 Journal Article http://hdl.handle.net/20.500.11937/50051 10.1016/j.snb.2016.07.135 Elsevier restricted
spellingShingle Arafat, M.
Haseeb, A.
Akbar, S.
Quadir, Md Zakaria
In-situ fabricated gas sensors based on one dimensional core-shell TiO2-Al2O3 nanostructures
title In-situ fabricated gas sensors based on one dimensional core-shell TiO2-Al2O3 nanostructures
title_full In-situ fabricated gas sensors based on one dimensional core-shell TiO2-Al2O3 nanostructures
title_fullStr In-situ fabricated gas sensors based on one dimensional core-shell TiO2-Al2O3 nanostructures
title_full_unstemmed In-situ fabricated gas sensors based on one dimensional core-shell TiO2-Al2O3 nanostructures
title_short In-situ fabricated gas sensors based on one dimensional core-shell TiO2-Al2O3 nanostructures
title_sort in-situ fabricated gas sensors based on one dimensional core-shell tio2-al2o3 nanostructures
url http://hdl.handle.net/20.500.11937/50051