Effect of temperature on the chromium deposition and poisoning of La0.6Sr0.4Co0.2Fe0.8O3-δ cathodes of solid oxide fuel cells

In this study, the effect of the temperature on the surface segregation and Cr deposition on La0.6Sr0.4Co0.2Fe0.8O3-ä(LSCF) cathodes is investigated using confocal laser Raman spectroscopy and electrical conductivity relaxation (ECR) method. The results show that the segregation of SrO phase on the...

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Main Authors: Wang, C., Becker, Thomas, Chen, Kongfa, Zhao, Ling, Wei, Bo, Jiang, San Ping
Format: Journal Article
Published: Pergamon 2014
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/47915
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author Wang, C.
Becker, Thomas
Chen, Kongfa
Zhao, Ling
Wei, Bo
Jiang, San Ping
author_facet Wang, C.
Becker, Thomas
Chen, Kongfa
Zhao, Ling
Wei, Bo
Jiang, San Ping
author_sort Wang, C.
building Curtin Institutional Repository
collection Online Access
description In this study, the effect of the temperature on the surface segregation and Cr deposition on La0.6Sr0.4Co0.2Fe0.8O3-ä(LSCF) cathodes is investigated using confocal laser Raman spectroscopy and electrical conductivity relaxation (ECR) method. The results show that the segregation of SrO phase on the LSCF surface decreases with the decreasing of temperature. Cr deposition takes place on the LSCF surface after the heat-treatment in the presence of Cr2O3at temperature range of 700 to 900°C for 48 h, formingSrCrO4phase. As the temperature decreases, less SrCrO4phase is detected. The surface exchange coefficient of LSCF measured at 900, 800 and 700?C after the heat-treatment in the presence of Cr2O3for 48 his 1.5 × 10-4, 1 × 10-4and 4 × 10-5cm s-1, respectively, which is much lower than that measured on the sample tested in the absence of Cr deposition. Chromium poisoning deteriorates the surface exchange and diffusion processes for the O2reduction reaction on LSCF electrodes. Cr deposition decreases significantly with the decrease of temperature, most likely due to the reduced Sr segregation as well as the decrease of the partial pressure of gaseous Cr species at reduced temperatures.
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spelling curtin-20.500.11937-479152017-09-13T15:58:41Z Effect of temperature on the chromium deposition and poisoning of La0.6Sr0.4Co0.2Fe0.8O3-δ cathodes of solid oxide fuel cells Wang, C. Becker, Thomas Chen, Kongfa Zhao, Ling Wei, Bo Jiang, San Ping chromium deposition and poisoning surface exchange coefficient Solid oxide fuel cells strontium segregation temperature In this study, the effect of the temperature on the surface segregation and Cr deposition on La0.6Sr0.4Co0.2Fe0.8O3-ä(LSCF) cathodes is investigated using confocal laser Raman spectroscopy and electrical conductivity relaxation (ECR) method. The results show that the segregation of SrO phase on the LSCF surface decreases with the decreasing of temperature. Cr deposition takes place on the LSCF surface after the heat-treatment in the presence of Cr2O3at temperature range of 700 to 900°C for 48 h, formingSrCrO4phase. As the temperature decreases, less SrCrO4phase is detected. The surface exchange coefficient of LSCF measured at 900, 800 and 700?C after the heat-treatment in the presence of Cr2O3for 48 his 1.5 × 10-4, 1 × 10-4and 4 × 10-5cm s-1, respectively, which is much lower than that measured on the sample tested in the absence of Cr deposition. Chromium poisoning deteriorates the surface exchange and diffusion processes for the O2reduction reaction on LSCF electrodes. Cr deposition decreases significantly with the decrease of temperature, most likely due to the reduced Sr segregation as well as the decrease of the partial pressure of gaseous Cr species at reduced temperatures. 2014 Journal Article http://hdl.handle.net/20.500.11937/47915 10.1016/j.electacta.2014.07.028 Pergamon restricted
spellingShingle chromium deposition and poisoning
surface exchange coefficient
Solid oxide fuel cells
strontium segregation
temperature
Wang, C.
Becker, Thomas
Chen, Kongfa
Zhao, Ling
Wei, Bo
Jiang, San Ping
Effect of temperature on the chromium deposition and poisoning of La0.6Sr0.4Co0.2Fe0.8O3-δ cathodes of solid oxide fuel cells
title Effect of temperature on the chromium deposition and poisoning of La0.6Sr0.4Co0.2Fe0.8O3-δ cathodes of solid oxide fuel cells
title_full Effect of temperature on the chromium deposition and poisoning of La0.6Sr0.4Co0.2Fe0.8O3-δ cathodes of solid oxide fuel cells
title_fullStr Effect of temperature on the chromium deposition and poisoning of La0.6Sr0.4Co0.2Fe0.8O3-δ cathodes of solid oxide fuel cells
title_full_unstemmed Effect of temperature on the chromium deposition and poisoning of La0.6Sr0.4Co0.2Fe0.8O3-δ cathodes of solid oxide fuel cells
title_short Effect of temperature on the chromium deposition and poisoning of La0.6Sr0.4Co0.2Fe0.8O3-δ cathodes of solid oxide fuel cells
title_sort effect of temperature on the chromium deposition and poisoning of la0.6sr0.4co0.2fe0.8o3-δ cathodes of solid oxide fuel cells
topic chromium deposition and poisoning
surface exchange coefficient
Solid oxide fuel cells
strontium segregation
temperature
url http://hdl.handle.net/20.500.11937/47915